CN101484257A - Strip casting method and device - Google Patents
Strip casting method and device Download PDFInfo
- Publication number
- CN101484257A CN101484257A CNA2007800131190A CN200780013119A CN101484257A CN 101484257 A CN101484257 A CN 101484257A CN A2007800131190 A CNA2007800131190 A CN A2007800131190A CN 200780013119 A CN200780013119 A CN 200780013119A CN 101484257 A CN101484257 A CN 101484257A
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- CN
- China
- Prior art keywords
- cooling agent
- cooling
- casting method
- casting
- strip
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/06—Continuous casting of metals, i.e. casting in indefinite lengths into moulds with travelling walls, e.g. with rolls, plates, belts, caterpillars
- B22D11/0637—Accessories therefor
- B22D11/068—Accessories therefor for cooling the cast product during its passage through the mould surfaces
- B22D11/0682—Accessories therefor for cooling the cast product during its passage through the mould surfaces by cooling the casting wheel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/06—Continuous casting of metals, i.e. casting in indefinite lengths into moulds with travelling walls, e.g. with rolls, plates, belts, caterpillars
- B22D11/0602—Continuous casting of metals, i.e. casting in indefinite lengths into moulds with travelling walls, e.g. with rolls, plates, belts, caterpillars formed by a casting wheel and belt, e.g. Properzi-process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/06—Continuous casting of metals, i.e. casting in indefinite lengths into moulds with travelling walls, e.g. with rolls, plates, belts, caterpillars
- B22D11/0622—Continuous casting of metals, i.e. casting in indefinite lengths into moulds with travelling walls, e.g. with rolls, plates, belts, caterpillars formed by two casting wheels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/06—Continuous casting of metals, i.e. casting in indefinite lengths into moulds with travelling walls, e.g. with rolls, plates, belts, caterpillars
- B22D11/0637—Accessories therefor
- B22D11/068—Accessories therefor for cooling the cast product during its passage through the mould surfaces
- B22D11/0685—Accessories therefor for cooling the cast product during its passage through the mould surfaces by cooling the casting belts
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Continuous Casting (AREA)
- Moulds For Moulding Plastics Or The Like (AREA)
- Molds, Cores, And Manufacturing Methods Thereof (AREA)
Abstract
The invention relates to a process and a device for strip casting using a travelling mould which is cooled by a liquid coolant. The invention is characterised in that the coolant is liquid metal or ionic liquid. Preferably, the coolant flows with turbulent flow through the cooling device attributed to the travelling mould.
Description
Technical field
The present invention relates to a kind of casting method and device of metal sheet band, especially a kind of the liquid coolant casting method and device of the metal sheet band of cooling indirectly of adopting.
Background technology
The casting method of metal sheet band and device are disclosed by patent documentations such as FR 2 289 271 A, GB 2 310 155 A, US 5 411075 A, US 4 671 340 A, JP 63 192 541 A, all adopt water as cooling agent in the technology that above-mentioned patent documentation discloses.Other patent documentation, casting method and device as EP 1 452252 A of the applicant's application have also disclosed strip have then adopted liquid metal and ionic liquid as cooling agent.
The casting device of strip can have various ways usually, as: be provided with one or two conveyer belt, do not establish conveyer belt and be provided with and form a slit between the opposite face of two rotation rollers, two rotation rollers, be provided with a rotation roller and a conveyer belt, a rotation roller perhaps only is set.All be provided with the mold of advancing in these casting devices, in the application's specification and claims, be referred to as " thin strip casting ".
When casting machine was provided with two rollers, the cast metal entered the gap by a special feed arrangement and solidifies in the gap or surface solidification at least, so that the metal sheet band of moulding can be handled.The general employing indirectly cooled off, and promptly water is sprayed directly on the opposite face inboard of the afterbody or the roller of conveyer belt, rather than is sprayed directly on the strip.Except said apparatus, can also adopt roller and a casting machine of being provided with a cavity to cast near the conveyer belt of cavity, the inboard of roller is by the water spray cooling, and the outside of conveyer belt is also by the water spray cooling.In single roll caster, the casting melt is positioned on the single roller that is not provided with cavity, and roller is from inner cooling, and cooling is only from a side of strip.Except twin-roll caster, single roll caster also may obtain extensive use in future.
In general, adopting thin strip casting is a kind of effective way that obtains semi-finished product and finished product as continuous casing, product can be in the form of sheets, thin ribbon shaped, wire or shaft-like, and founding materials can be ferrous metal and non-ferrous metals such as copper, aluminium, magnesium, nickel or its alloy such as steel.
The general mold of advancing that adopts in the continuous casing of strip to obtain almost zero friction, improves casting speed, saves cost.
The continuous casing of strip generally adopts water as cooling agent, and still, water has following significant disadvantages as cooling agent: by the low operating temperature of low evaporating temperature decision, and directly set off an explosion easily when hot cast metal contacts.Be cooled fast to low temperature by high temperature and on the mold of advancing, produce very big thermograde easily, and cause after certain operating time, forming crackle, reduce the service life of the mold of advancing.
In some thin strip casting machines (as rotation thin strip casting machine), the strong cooling that conveyer belt one side is caused by water can cause the contraction of strip, and forms a gas gap between strip and mold.Gas gap can hinder the transmission of heat, causes the defectives such as casting speed reduction, segregation, the bending of roller shell, face crack and cell size variation that cast continuously.High casting speed needs strong cooling, but is not to be cooled to low-down temperature.
Adopt water as cooling agent technology instability,,, influence the metallurgical performance of product even the very little change of cast metal charging rate all may cause the significant change of cooling velocity because the low evaporating temperature of water can cause to be cooled heat transfer marked change.
When adopting water as cooling agent, the thermograde on the mold of advancing is very big, has limited the service life of mold.If the formation face crack, even can on cast article, see face crack, therefore to adopt water to differ and obtain desirable product quality surely as cooling agent, the service life of the mold of perhaps advancing is not long.
Above defective is to adopt water as inherent shortcoming that cooling agent caused, therefore, necessaryly provide a kind of casting method and device simple, strip reliably, overcoming the defective in the existing thin strip casting method and apparatus, and keep the advantage of existing thin strip casting method and apparatus.
Summary of the invention
Therefore, the objective of the invention is to: a kind of casting method and device simple, strip reliably are provided.
In order to realize the foregoing invention purpose, the casting method of strip of the present invention adopts liquid metal or ionic liquid as cooling agent, and cooling agent is with the turbulent form cooling device of flowing through, and is controlled to guarantee cooling characteristics.
Ionic liquid is the name of one group of salt, comprises organic cation and most inorganic anions, and fusing point is below 100 ℃.Ionic liquid is not decomposed under the highest operating temperature, does not react with casting device under given environmental condition.In addition, need to prove, though water and other liquid also contain a spot of ion, is not the alleged ionic liquid of the present invention.
In order to distinguish metal to be cast and as the metal of cooling agent, this specification is called the former " cast metal ", the latter is called " liquid metal ".
Under the effect of cooling indirectly, cast metal or alloy solidify.According to an embodiment of the invention, liquid metal is used in cooling indirectly, as lead, tin, bismuth, gallium, indium or its alloy, and other metal or alloy that below the setting temperature of cast metal or alloy, are in a liquid state.
Adopt the indirect cooling of liquid metal can guarantee that cooling down operation is continuous, controlled in the thin strip casting, intensity of cooling can be adjusted by the flow velocity of adjusting cooling agent and the feeding temperature of cooling agent, thereby improve mold cold side temperature and reduce the thermograde of mold, the gas gap of avoiding being created in strip in rotational casting and the casting of single roller and advancing and form between the mould.
Can obtain the cross section quality like this and cast strip more uniformly, higher casting speed, and prevent the formation of face crack.By the temperature of adjusting cooling agent and the flow velocity of cooling agent, may be controlled to the grainiess of type strip product.Therefore, when using liquid metal, also can obtain good castability even in process of setting and cooling procedure subsequently, be easy to generate the alloy of crackle as cooling agent.In addition, can also avoid the blast of adopting water may cause fully as cooling agent.
Usually, the existing mould system of advancing that is used for thin strip casting also can adopt liquid metal as cooling agent.At this moment, this system comprises: one use the liquid metal cooling to advance the device, of mold is heated to operating temperature with cooling agent and after distributing the heat of strip the device of cooling cooling agent, and the loop device of a cooling agent.
The Celsius temperature fusing point of cooling agent be preferably lower than or equal the cast metal the Celsius temperature fusing point 60%.
According to a preferred embodiment of the present invention, in the mold zone of advancing, the flow direction of cooling agent is opposite with the traffic direction of casting strip.
In order to realize the foregoing invention purpose, the present invention also provides a kind of cooling device that is used for the inventive method, it comprises that one is used to contain the reservoir vessel that carries cooling agent, heater, one and connects reservoir vessel and the cooling device pump with indirect cooling casting metal sheet band by pipeline, and one is arranged on and is used for the cooling agent self-cooling set is delivered to heat exchanger on the return duct of reservoir vessel.
According to a preferred embodiment of the present invention, cooling device preferably can be provided with built-ins such as the runner of the built-in wing, cross sectional dimensions and/or shape variable or biasing dish, so that cooling agent is in turbulent condition and forms desirable fluid flow pattern.
Description of drawings
Below in conjunction with accompanying drawing, describe the specific embodiment of the present invention and corresponding useful technique effect thereof in detail, wherein:
Fig. 1 is the schematic diagram of twin-roll caster of the present invention.
Fig. 2 is the partial schematic diagram of sealing coolant circuit.
Fig. 3 is the cross-sectional schematic of III-III line in Fig. 4.
Fig. 4 is the cross-sectional schematic of IV-IV line in Fig. 3.
The specific embodiment
Figure 1 shows that the schematic diagram of the vertical thin strip casting of the present invention with twin-roll caster, comprise the cooling device that chill roll is required, the difference of itself and existing twin-roll caster is: the support of roller is opened, and preferably all open at the two ends of Zhi Chenging, so that support 9 is parallel to the rotating shaft extension of roller.Support 9 is fixed on the supporting base 10 of roller both sides, and casting machine also is provided with a coolant feed 2 and a cooling agent return duct 6.
Figure 2 shows that the feedway of cooling agent, it comprises a cooling agent reservoir vessel 12, a pump 13 that connects feed pipe 2 shown in Figure 1, and a cooling agent return duct 6.Cooling agent refluxes through an external heat exchangers 14, and after the heat that distributes on the heat exchanger 14 was reached one second cool cycles, cooling agent was got back to cooling agent reservoir vessel 12.
Fig. 3 be among Fig. 4 along the cross-sectional schematic of III-III line, it is depicted as the cross-sectional schematic at right roller middle part among Fig. 1, with the cooling device of detailed demonstration double-roller continuous casting machine.Cooling device comprises a feed pipe 2 that is connected on the proportioning room 3, and proportioning room 3 is guaranteed the pressure loss of being scheduled to and made cooling agent evenly distribute along the length direction of roller.Through after the proportioning room 3, the cooling agent heat exchanger 4 of upwards flowing through, heat exchanger 4 will be cast the heat that strip distributes and take away from roller shell 1.As shown in Figure 2, leave heat exchanger 4 after, cooling agent flows into collecting chamber 5, cooling agent is collected and sends into return duct 6 in collecting chamber 5, return duct 6 extends to external heat exchangers 14 from roller.
In heat exchanger 14, the heat that distributes is reached one second cooling recirculation system, to realize other heating purposes.Certainly, for the different parts at roller, conveyer belt provides enough coolings, two or more main cooling systems and/or inferior cooling system can be set also.
Cooling agent is stored in the reservoir vessel 12, and is transported to feed pipe 2 by pump 13.Pump 13 can be immersed in the cooling agent reservoir vessel 12, also can be connected to the outside of reservoir vessel 12 by pipeline, as shown in Figure 2.The kind of institute's use pump 13 and required coolant flow speed are depended in the installation of pump 13, and pump 13 can be a mechanical pump, can be electromagnetic pumps also, depend on the self attributes of required coolant flow speed, pump efficiency, cost of investment and cooling agent.For the those skilled in the art that know the technology of the present invention, the selection of pump and installation can realize easily.
Please refer to Fig. 3, embedded heat exchanger 4 is pressed on the roller shell 1 by hydraulic piston 7, and support 8 and 9 can prevent that embedded heat exchanger 4 from rotating, and hydraulic piston 7 is supported by support 9.Consider the thermal expansion in different operating stage, can also use other settings.
Embedded heat exchanger 4 is provided with the device that can make cooling agent produce strong turbulent flow, so that near each parts the cooling surface have desirable rate of heat dissipation, and provides desirable fluid flow pattern.
Fig. 4 is the vertical profile schematic diagram of right roller shown in Figure 3 along the IV-IV line, and as can be seen, roller shell 1 is fixed on the hollow shaft 11, and the fixed-site of roller is on support member 16.In order to ensure the rotation of roller, casting machine also is provided with gear 17, and certainly, the drive unit of roller also can otherwise be installed.
The roller shell can be made by Elbrodur B 95 copper alloys, or be set to the shell of two-layer hollow, wherein shell can distribute on the strip copper alloy of heat fast by Elbrodur B 95 copper alloys or other and makes, and inner casing is for providing the thin box hat of necessary intensity for roller.The outside of shell and inboard superficial layer are respectively equipped with one deck high-abrasive material, to prolong the service life of shell.
The reservoir vessel 12 of cooling agent can be provided with an inert gas entrance 15, and inert gas can 15 enter reservoir vessel 12 by entering the mouth.Inert gas can be helium or argon gas, according to the chemical attribute of cooling agent, also can use the air in the nitrogen discharge line sometimes and cools off before circulate coolant.The cooling agent after using in addition, can also be provided with a cooling agent regenerating unit, so that can be regenerated.
Cooling system of the present invention can be used for the casting of vertical casting, horizontal casting or other angles, and the present invention can be used for the casting of ferrous metal such as steel, also can be used for the casting of non-ferrous metals such as copper, aluminium or its alloy.The present invention can be used for existing workshop, and can not run into too big problem.For this reason, only need to install and can prevent that cooling agent from get final product along the device that the inner surface of roller or conveyer belt leaks, the material require that is adopted can bear the temperature, chemical action of cooling agent and by the density and the mobile power that causes of cooling agent.For the those skilled in the art that know metal casting of the present invention, the selection of material is conspicuous.
In order to ensure the desirable fluid flow pattern and the turbulent flow of liquid metal, cooling device of the present invention can be provided with built-in, as the runner of inner wing, cross sectional dimensions and/or shape variable and biasing dish etc.For the technical staff in thermodynamic fluid of the present invention field, be provided with built-in arrange and design is conspicuous.
According to employed cooling agent,, preferably can heat pipeline and device that all or most at least cooling agent are flowed through in order to prevent to freeze.In addition, pipeline and device preferably can tilt be installed, to guarantee that when pump 13 cisco unity malfunctions, cooling agent can be back to the reservoir vessel 12 that is provided with heater under the effect of self gravitation.
The invention has the advantages that: because the number of the quantity of heat transmitter and the heat transmitter when making water as cooling agent Amount is consistent, can realize easier, better cooling control; Can prolong the service life of the mold of advancing; Can improve casting speed; Can obtain continuous casting surface smooth, that do not have blemish; Continuously casting The face of making a list does not have or only has negligible uneven surface layer; Temperature that can be by regulating cooling agent and Structure and the size of the flow control crystal grain of cooling agent; Can realize the sloping casting of strip foundry goods, save again Energy consumption during heating.
Claims (8)
1, a kind of casting method of strip adopts a mold of advancing with coolant cools, and it is characterized in that: described cooling agent is liquid metal or ionic liquid.
2, casting method according to claim 1 is characterized in that: described cooling agent is selected from lead, tin, bismuth, gallium, indium or its alloy.
3. casting method according to claim 1 and 2 is characterized in that: the Celsius temperature fusing point of described cooling agent is less than or equal to 60% of founding materials Celsius temperature fusing point.
4. according to each described casting method in the claim 1 to 3, it is characterized in that: in the mold zone of advancing, the flow direction of described cooling agent is opposite with the direction of motion of described casting strip.
5, according to each described casting method in the claim 1 to 4, it is characterized in that: the described cooling agent of near surface to be cooled is turbulent flow.
6, casting method according to claim 5 is characterized in that: the described cooling agent of near surface to be cooled is strong turbulent flow.
7. cooling device that is used in each described casting method of claim 1 to 6, it comprises: reservoir vessel (12) that is used to accommodate cooling medium, heater, one are provided with and connect reservoir vessel and cooling device (4) pump (13) with indirect cooling casting metal sheet band, and one is positioned at and is used for cooling agent is transported to heat exchanger (14) on the return duct (6) of reservoir vessel from cooling device.
8. cooling device according to claim 7, it is characterized in that: described cooling device (4) is provided with the runner of inner wing, cross sectional dimensions and/or shape variable, and built-in such as biasing dish, so that the cooling agent of near surface to be cooled is turbulent condition and/or forms desirable fluidised form.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP06450056A EP1844880A1 (en) | 2006-04-12 | 2006-04-12 | Strip casting |
EP06450056.4 | 2006-04-12 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN101484257A true CN101484257A (en) | 2009-07-15 |
Family
ID=37076205
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNA2007800131190A Pending CN101484257A (en) | 2006-04-12 | 2007-04-11 | Strip casting method and device |
Country Status (8)
Country | Link |
---|---|
US (1) | US20090314460A1 (en) |
EP (2) | EP1844880A1 (en) |
JP (1) | JP2009533225A (en) |
CN (1) | CN101484257A (en) |
BR (1) | BRPI0711537A2 (en) |
CA (1) | CA2647894A1 (en) |
NO (1) | NO20084271L (en) |
WO (1) | WO2007115827A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114406215A (en) * | 2021-12-15 | 2022-04-29 | 钢铁研究总院 | Vacuum rapid quenching cooling system for forced cooling by liquid metal |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ITRM20070150A1 (en) * | 2007-03-21 | 2008-09-22 | Danieli Off Mecc | PROCESS AND PLANT FOR THE PRODUCTION OF METAL TAPES |
CN101265516B (en) * | 2008-04-23 | 2010-06-02 | 浙江佰耐钢带有限公司 | Steel band quenching technique and cooling medium used for the same |
AT508292B1 (en) * | 2009-05-28 | 2011-03-15 | Mettop Gmbh | METHOD FOR COOLING A METALURGIC OVEN AND COOLING SYSTEM FOR METALURGICAL OVENS |
PE20142105A1 (en) | 2012-02-02 | 2014-12-20 | Vtu Holding Gmbh | IONIC LIQUIDS FOR COOLING IN HIGH TEMPERATURE ENVIRONMENTS |
EP3599037A1 (en) | 2018-07-25 | 2020-01-29 | Primetals Technologies Germany GmbH | Cooling section with adjustment of the cooling agent flow by means of pumping |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1098541A (en) * | 1964-03-05 | 1968-01-10 | Leonard Gordon Charles Tuck | Method for the continuous casting of metal |
FR2289271A1 (en) * | 1974-10-29 | 1976-05-28 | Socometal | Spiral water channel for cooling rolls - used in continuous casting, made of wire welded round mild steel tube |
FR2587247B1 (en) * | 1985-09-17 | 1988-08-12 | Siderurgie Fse Inst Rech | CYLINDER FOR CONTINUOUS CASTING BETWEEN CYLINDERS, WITH COOLING FLUID CIRCULATION |
JPS62101353A (en) * | 1985-10-25 | 1987-05-11 | Kawasaki Steel Corp | Continuous casting method for hollow ingot |
JPS6330157A (en) * | 1986-07-24 | 1988-02-08 | Mitsubishi Heavy Ind Ltd | Cooling drum type strip continuous casting method |
JPS63183759A (en) * | 1987-01-26 | 1988-07-29 | Ishikawajima Harima Heavy Ind Co Ltd | Nozzle for shift mold type continuous casting machine |
JPS63192541A (en) * | 1987-02-05 | 1988-08-09 | Kawasaki Steel Corp | Internal water cooled sleeve type roll for producing rapidly cooled strip |
US5411075A (en) * | 1993-08-31 | 1995-05-02 | Aluminum Company Of America | Roll for use in casting metal products and an associated method |
FR2723014B1 (en) * | 1994-07-29 | 1996-09-20 | Pechiney Rhenalu | METHOD AND DEVICE FOR CORRECTING THE OVALIZATION OF CONTINUOUS CASTING CYLINDERS OF METAL STRIP |
JPH091295A (en) * | 1995-06-13 | 1997-01-07 | Hitachi Cable Ltd | Dam block guide of continuous casting equipment |
AUPN811396A0 (en) * | 1996-02-16 | 1996-03-07 | Bhp Steel (Jla) Pty Limited | Roll cooling structure for twin roll continuous caster |
DE10042078A1 (en) * | 2000-08-26 | 2002-03-07 | Sms Demag Ag | Method and device for the continuous casting of steel strip from molten steel |
JP2002086254A (en) * | 2001-07-02 | 2002-03-26 | Toshiba Corp | Method and apparatus for treating metallic material |
JP4726385B2 (en) * | 2002-09-25 | 2011-07-20 | シンフォニアテクノロジー株式会社 | Rapid casting equipment |
EP1452252A1 (en) * | 2003-02-28 | 2004-09-01 | Hubert Dipl.-Ing. Sommerhofer | Continuous casting method |
-
2006
- 2006-04-12 EP EP06450056A patent/EP1844880A1/en not_active Withdrawn
-
2007
- 2007-04-11 BR BRPI0711537-7A patent/BRPI0711537A2/en not_active IP Right Cessation
- 2007-04-11 JP JP2009504636A patent/JP2009533225A/en active Pending
- 2007-04-11 US US12/226,261 patent/US20090314460A1/en not_active Abandoned
- 2007-04-11 CA CA002647894A patent/CA2647894A1/en not_active Abandoned
- 2007-04-11 CN CNA2007800131190A patent/CN101484257A/en active Pending
- 2007-04-11 EP EP07724151A patent/EP2010345A1/en not_active Withdrawn
- 2007-04-11 WO PCT/EP2007/003210 patent/WO2007115827A1/en active Application Filing
-
2008
- 2008-10-13 NO NO20084271A patent/NO20084271L/en not_active Application Discontinuation
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114406215A (en) * | 2021-12-15 | 2022-04-29 | 钢铁研究总院 | Vacuum rapid quenching cooling system for forced cooling by liquid metal |
Also Published As
Publication number | Publication date |
---|---|
US20090314460A1 (en) | 2009-12-24 |
NO20084271L (en) | 2009-01-09 |
BRPI0711537A2 (en) | 2011-11-01 |
EP2010345A1 (en) | 2009-01-07 |
WO2007115827A1 (en) | 2007-10-18 |
CA2647894A1 (en) | 2007-10-18 |
EP1844880A1 (en) | 2007-10-17 |
JP2009533225A (en) | 2009-09-17 |
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Application publication date: 20090715 |