CN101475857A - Liquid fuel and preparation thereof - Google Patents
Liquid fuel and preparation thereof Download PDFInfo
- Publication number
- CN101475857A CN101475857A CNA200910036740XA CN200910036740A CN101475857A CN 101475857 A CN101475857 A CN 101475857A CN A200910036740X A CNA200910036740X A CN A200910036740XA CN 200910036740 A CN200910036740 A CN 200910036740A CN 101475857 A CN101475857 A CN 101475857A
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- CN
- China
- Prior art keywords
- solution
- liquid fuel
- portions
- parts
- dissolving
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000446 fuel Substances 0.000 title claims abstract description 33
- 239000007788 liquid Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 42
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 39
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 26
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000010299 hexamethylene tetramine Nutrition 0.000 claims abstract description 13
- 239000004312 hexamethylene tetramine Substances 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 6
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 5
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 40
- DCKVNWZUADLDEH-UHFFFAOYSA-N sec-butyl acetate Chemical class CCC(C)OC(C)=O DCKVNWZUADLDEH-UHFFFAOYSA-N 0.000 claims description 7
- 239000000654 additive Substances 0.000 claims description 6
- 230000000996 additive effect Effects 0.000 claims description 6
- 229940043232 butyl acetate Drugs 0.000 claims description 4
- 239000007789 gas Substances 0.000 abstract description 10
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract description 9
- 238000002485 combustion reaction Methods 0.000 abstract description 5
- 239000002283 diesel fuel Substances 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052799 carbon Inorganic materials 0.000 abstract description 2
- 238000004880 explosion Methods 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 230000003749 cleanliness Effects 0.000 abstract 1
- 230000008021 deposition Effects 0.000 abstract 1
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 239000000779 smoke Substances 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 2
- 125000003158 alcohol group Chemical group 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000009615 deamination Effects 0.000 description 1
- 238000006481 deamination reaction Methods 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
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- Liquid Carbonaceous Fuels (AREA)
Abstract
The invention relates to a liquid fuel and a preparation method thereof. The liquid fuel is mainly prepared from the following raw materials in portion by mass: 150 to 300 portions of water, 650 to 850 portions of methanol, 5 to 20 portions of butyl acetate, 5 to 20 portions of sodium hydroxide, 2 to 10 portions of hexamethylenetetramine, 10 to 30 portions of hydrogen peroxide with a mass concentration of 30 percent, and 50 to 150 portions of ethanol. The liquid fuel has low volatility and steady performance, is safe during the transportation and storage when being distributed to users due to the high temperature resistance, is difficult to ignite if no open flame exists, does not splash liquids and fumigate eyes during the use, can completely burn, is difficult to generate harmful gas such as formaldehyde and the like, has no smoke, no toxicity, no carbon deposition, no pot blackening, violent fire, high heat energy, no pressure, and no explosion danger, has a combustion calorie more than 9,500kcal/kg, can be extinguished by water during the fire extinguishing, and has the characteristics of cleanliness, environment protection, safety, simple and convenient production, and low production cost. The liquid fuel can substitute diesel oil and liquefied gas, and is suitable to be used by diesel furnaces, liquefied gas furnaces, boilers and the like.
Description
Technical field
The present invention relates to a kind of liquid fuel and preparation method thereof.
Background technology
Existing alcohol-group fuel and civil synthetic fuel, because incomplete combustion is thorough, can give out the gas of smoked eye, this is that fuel does not have thorough perfect combustion and the formaldehyde and the carbon dioxide that produce, human and environment there is certain hazardness, residual liquid is arranged after the fuel combustion, and the raw material that uses is the higher inflammable explosive article of purity, gives transportation like this, store in a warehouse and bring unsafe factor.
Summary of the invention
Purpose of the present invention just provides liquid fuel of a kind of cleaning, environmental protection, safety and preparation method thereof.
The technical solution adopted in the present invention is: a kind of liquid fuel mainly is to be made by the raw material of following mass parts: 10～30 parts of the hydrogen peroxide of 150～300 parts in water, 650～850 parts of methyl alcohol, 5～20 parts of butylacetates, 5～20 parts in sodium hydroxide, 2～10 parts of hexamethylenetetramines, mass concentration 30%, 50～150 parts of ethanol.Its preparation method: (1) adds stirring and dissolving in the entry with sodium hydroxide, adds the hexamethylenetetramine stirring and dissolving then, adds the hydrogen peroxide stirring and dissolving of mass concentration 30% again, obtains A solution; (2) A solution is slowly poured in the water stirred, obtain B solution; (3) butylacetate is added in the ethanol stir, obtain C solution; (4) C solution is slowly poured in the methyl alcohol stirred, obtain D solution; (5) B solution is slowly poured in the D solution, placed 40～120 minutes, obtain liquid fuel.
A kind of liquid fuel can be to be made by the raw material of following mass parts: 150～300 parts in water, 650～850 parts of methyl alcohol, 5～20 parts of butylacetates, 5～20 parts in sodium hydroxide, 2～10 parts of hexamethylenetetramines, 10～30 parts of the hydrogen peroxide of mass concentration 30%, 50～150 parts of ethanol, 3～10 parts of foodstuff additive, light green 0.2～0.5 part.Its preparation method: (1) adds stirring and dissolving in the entry with sodium hydroxide, adds the hexamethylenetetramine stirring and dissolving then, adds the hydrogen peroxide stirring and dissolving of mass concentration 30% again, obtains A solution after adding light green and foodstuff additive; (2) A solution is slowly poured in the water stirred, obtain B solution; (3) butylacetate is added in the ethanol stir, obtain C solution; (4) C solution is slowly poured in the methyl alcohol stirred, obtain D solution; (5) B solution is slowly poured in the D solution, placed 40～120 minutes, obtain liquid fuel.
Liquid fuel volatility of the present invention is low, stable performance, because liquid fuel heatproof height, be distributed to the user in transportation, safety during storage, the flames of anger is difficult for lighting, do not fly liquid during use, not smoked eye, obnoxious flavoures such as being difficult for producing formaldehyde can thoroughly burn, smokelessly, nontoxic, no carbon distribution, no blacking pan, firepower is violent, the heat energy height, no pressure, no explosion hazard, reach more than 9500 kcal/kg at burning calorie on the alcohol-group fuel stove, water can put out during fire extinguishing, has cleaning, environmental protection, safety, simple for production, the characteristics that production cost is low, the present invention can substitute diesel oil and liquefied gas, is applicable to diesel oil stove, liquefied gas furnace, uses such as boiler, just the burner or the nozzle of stove and accessory will be changed a little.
Embodiment
Below in conjunction with embodiment, the invention will be further described, but it is not represented as unique embodiment of the present invention.
Embodiment one
5 gram sodium hydroxide are added stirring and dissolving in the 50 gram water, add 2 gram hexamethylenetetramine stirring and dissolving then, add the hydrogen peroxide 10 gram stirring and dissolving of mass concentration 30% again, obtain A solution; Slowly pour A solution into 100 grams and stir in the water, obtain B solution; 5 gram butylacetates are added stirring in ethanol 50 grams, obtain C solution; C solution is slowly poured into 650 grams stir in the methyl alcohol, obtain D solution; B solution is slowly poured in the D solution, placed 40 minutes, obtain liquid fuel.Deamination and desulfurization when methyl alcohol CHOH makes, basically do not have harmful substances, burning back expellant gas does not constitute pollution to environment, adds and plays flash burn and combustion-supporting effect in the entry, water can be stablized the volatility and the liveness of methyl alcohol, and is the mixed agent of good chemical molecular dissolving.Sodium hydroxide, hydrogen peroxide, hexamethylenetetramine are used for strengthening the oxygen molecule of fuel, when making after the flash burn to certain temperature because the hydrogen-oxygen chain in chemical reaction self effusion oxygen molecule and the parallel off water outlet makes fuel fiercely burning under the oxygen-enriched environment in the stove of certain temperature.Ethyl acetate is an ignition dope, makes the color and the diesel combustion shape of flame, can effectively make flare higher.
Embodiment two
20 gram sodium hydroxide are added stirring and dissolving in the 100 gram water, add 10 gram hexamethylenetetramines then and stir constantly dissolving, hydrogen peroxide 30 grams that add mass concentration 30% again stir constantly dissolving, obtain A solution; Slowly pour A solution into 300 grams and stir in the water, obtain B solution; 20 gram butylacetates are added stirring in ethanol 150 grams, obtain C solution; C solution is slowly poured into 850 grams stir in the methyl alcohol, obtain D solution; B solution is slowly poured in the D solution, placed 120 minutes, obtain liquid fuel.
Embodiment three
5 gram sodium hydroxide are added stirring and dissolving in the 50 gram water, add 2 gram hexamethylenetetramine stirring and dissolving then, add the hydrogen peroxide 10 gram stirring and dissolving of mass concentration 30% again, obtain A solution behind foodstuff additive 3 grams, light green 0.2 gram; Slowly pour A solution into 100 grams and stir in the water, obtain B solution; 5 gram butylacetates are added stirring in ethanol 50 grams, obtain C solution; C solution is slowly poured into 650 grams stir in the methyl alcohol, obtain D solution; B solution is slowly poured in the D solution, placed 60 minutes, obtain liquid fuel.
Embodiment four
20 gram sodium hydroxide are added stirring and dissolving in the 100 gram water, add 10 gram hexamethylenetetramine stirring and dissolving then, add the hydrogen peroxide 30 gram stirring and dissolving of mass concentration 30% again, obtain A solution behind foodstuff additive 10 grams, light green 0.5 gram; Slowly pour A solution into 300 grams and stir in the water, obtain B solution; 20 gram butylacetates are added stirring in ethanol 150 grams, obtain C solution; C solution is slowly poured into 850 grams stir in the methyl alcohol, obtain D solution; B solution is slowly poured in the D solution, placed 120 minutes, obtain liquid fuel.
Liquid fuel of the present invention after tested, the contrast of every index and liquefied gas, diesel oil sees the following form:
| The contrast project | Liquid fuel | Liquefied gas | Diesel oil |
| Sulfur monoxide | <1.4mg/m 3 | 4.02mg/m 3 | 26.9mg/m 3 |
| Oxynitride | 1.58mg/m 3 | 7.48mg/m 3 | 11mg/m 3 |
| Carbonic acid gas | 3.025mg/m 3 | 178.74mg/m 3 | 721.24mg/m 3 |
| Calorific value | 11000 kcal/kg | 7800 kcal/kg | 12000 kcal/kg |
| Pressure | No pressure | Steel cylinder 1-1.2MPa | No pressure |
| Level of safety | Leaking is liquid, finds that easily water one is pounced on and promptly gone out, environmental protection | Leaking is gas, is difficult for finding, poisonous, is difficult for putting out | Leaking is liquid, and easily not environmental protection is easily put out in discovery |
Claims (4)
1, a kind of liquid fuel is characterized in that it mainly being that raw material by following mass parts is made: 10～30 parts of the hydrogen peroxide of 150～300 parts in water, 650～850 parts of methyl alcohol, 5～20 parts of butylacetates, 5～20 parts in sodium hydroxide, 2～10 parts of hexamethylenetetramines, mass concentration 30%, 50～150 parts of ethanol.
2, liquid fuel according to claim 1 is characterized in that the raw material that also adds has: 3～10 parts of foodstuff additive, light green 0.2～0.5 part.
3, the preparation method of liquid fuel according to claim 1 is characterized in that:
(1) sodium hydroxide is added stirring and dissolving in the entry, add the hexamethylenetetramine stirring and dissolving then, add the hydrogen peroxide stirring and dissolving of mass concentration 30%, obtain A solution;
(2) A solution is slowly poured in the water stirred, obtain B solution;
(3) butylacetate is added in the ethanol stir, obtain C solution;
(4) C solution is slowly poured in the methyl alcohol stirred, obtain D solution;
(5) B solution is slowly poured in the D solution, placed 40～120 minutes, obtain liquid fuel.
4, the preparation method of liquid fuel according to claim 2 is characterized in that:
(1) sodium hydroxide is added stirring and dissolving in the entry, add the hexamethylenetetramine stirring and dissolving then, add mass concentration 30% hydrogen peroxide stirring and dissolving again, obtain A solution after adding light green and foodstuff additive;
(2) A solution is slowly poured in the water stirred, obtain B solution;
(3) butylacetate is added in the ethanol stir, obtain C solution;
(4) C solution is slowly poured in the methyl alcohol stirred, obtain D solution;
(5) B solution is slowly poured in the D solution, placed 40～120 minutes, obtain liquid fuel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910036740XA CN101475857B (en) | 2009-01-16 | 2009-01-16 | Liquid fuel and preparation thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910036740XA CN101475857B (en) | 2009-01-16 | 2009-01-16 | Liquid fuel and preparation thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101475857A true CN101475857A (en) | 2009-07-08 |
| CN101475857B CN101475857B (en) | 2010-12-08 |
Family
ID=40836634
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910036740XA Expired - Fee Related CN101475857B (en) | 2009-01-16 | 2009-01-16 | Liquid fuel and preparation thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101475857B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101875868A (en) * | 2010-04-19 | 2010-11-03 | 宋贵中 | Civil liquid fuel and preparation method thereof |
| CN102408924A (en) * | 2011-10-12 | 2012-04-11 | 陈金城 | Double-base liquid fuel and preparation method thereof |
| CN103396844A (en) * | 2013-08-12 | 2013-11-20 | 廖新明 | Alcohol oil and preparation method thereof |
| CN104357099A (en) * | 2014-11-10 | 2015-02-18 | 湖北德美科技有限公司 | Alcohol-based fuel and preparation method thereof |
| US9447724B2 (en) | 2010-11-25 | 2016-09-20 | Gane Energy & Resources Pty Ltd. | Fuel and process for powering a compression ignition engine |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101338226A (en) * | 2008-08-08 | 2009-01-07 | 高三林 | Environment protection type liquid fuel and method for preparing same |
-
2009
- 2009-01-16 CN CN200910036740XA patent/CN101475857B/en not_active Expired - Fee Related
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101875868A (en) * | 2010-04-19 | 2010-11-03 | 宋贵中 | Civil liquid fuel and preparation method thereof |
| CN101875868B (en) * | 2010-04-19 | 2012-05-23 | 廖新明 | Civil liquid fuel |
| US9447724B2 (en) | 2010-11-25 | 2016-09-20 | Gane Energy & Resources Pty Ltd. | Fuel and process for powering a compression ignition engine |
| US10023818B2 (en) | 2010-11-25 | 2018-07-17 | Gane Energy & Resources Pty Ltd. | Process for powering a compression ignition engine and fuel therefor |
| US10815441B2 (en) | 2010-11-25 | 2020-10-27 | Gane Energy & Resources Pty Ltd. | Fuel and process for powering a compression ignition engine |
| CN102408924A (en) * | 2011-10-12 | 2012-04-11 | 陈金城 | Double-base liquid fuel and preparation method thereof |
| CN102408924B (en) * | 2011-10-12 | 2014-05-07 | 陈金城 | Double-base liquid fuel and preparation method thereof |
| CN103396844A (en) * | 2013-08-12 | 2013-11-20 | 廖新明 | Alcohol oil and preparation method thereof |
| CN103396844B (en) * | 2013-08-12 | 2015-05-27 | 上海源圭能源有限公司 | Alcohol oil and preparation method thereof |
| CN104357099A (en) * | 2014-11-10 | 2015-02-18 | 湖北德美科技有限公司 | Alcohol-based fuel and preparation method thereof |
| CN104357099B (en) * | 2014-11-10 | 2016-04-13 | 湖北德美科技有限公司 | A kind of alcohol-group fuel and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101475857B (en) | 2010-12-08 |
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Application publication date: 20090708 Assignee: Huizhou Kesheng Energy Co. Ltd. Assignor: Li Yaosu|Liao Xinming Contract record no.: 2012440000639 Denomination of invention: Liquid fuel and preparation method thereof Granted publication date: 20101208 License type: Exclusive License Record date: 20121206 |
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Assignee: Huizhou Kesheng Energy Co. Ltd. Assignor: Li Yaosu|Liao Xinming Contract record no.: 2012440000639 Date of cancellation: 20130822 |
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Application publication date: 20090708 Assignee: Shanghai Yuangui Energy Co., Ltd. Assignor: Li Yaosu|Liao Xinming Contract record no.: 2013440000480 Denomination of invention: Liquid fuel and preparation method thereof Granted publication date: 20101208 License type: Exclusive License Record date: 20131017 |
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