CN101423561A - Method for reducing fresh water dosage during carrageenan extraction by eucheuma - Google Patents
Method for reducing fresh water dosage during carrageenan extraction by eucheuma Download PDFInfo
- Publication number
- CN101423561A CN101423561A CNA2008102186692A CN200810218669A CN101423561A CN 101423561 A CN101423561 A CN 101423561A CN A2008102186692 A CNA2008102186692 A CN A2008102186692A CN 200810218669 A CN200810218669 A CN 200810218669A CN 101423561 A CN101423561 A CN 101423561A
- Authority
- CN
- China
- Prior art keywords
- eucheuma
- seawater
- gmel
- fresh water
- web
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Landscapes
- Processing Of Solid Wastes (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention relates to a method for reducing the fresh water use amount when carrageenan is extracted by using eucheuma. According to the production process flow when the carrageenan is extracted by the eucheuma, the water use amount characteristic of each working procedure and the requirement on the production water, after the sea water is subjected to sand filtration, coagulation treatment and pH value adjustment, sea water is used to replace fresh water to perform production in the processes of eucheuma base process and bleaching so as to reduce the use amount of the fresh water. The method has apparent effect on reducing the fresh water use amount. When the powder carrageenan product is produced, the fresh water use amount can be reduced to 42.9 percent. The method has great significance to build a water-saving and environment-friendly society, improve the enterprise economic benefits, and guarantee the sustainable development of the enterprise and the society.
Description
Technical field
The seawater that the invention belongs in the chemical treatment is used, and particularly reduces the method for fresh water dosage with carrageenan extraction by eucheuma.
Background technology
Carrageenin is widely used in food, medicine, group training, various microorganism detection and the scientific experiment.In producing with carrageenan extraction by eucheuma, need to consume a large amount of fresh water, 1 ton of Eucheuma muricatum (Gmel.) Web dry product of every processing needs about 110 tons of water consumptions.Freshwater resources are limited irreplaceable strategic resources, according to statistics, China per capita the fresh water amount only be the whole world per capita the fresh water amount about 1/4, become one of country of lack of water, especially China's Coastal Areas economy is comparatively flourishing, the density of population is high, and the situation of its lack of water is more severe; Most of maritime nations are actively accelerating the development and use seawater resources.Carrageenin manufacturing enterprise is owing to the reason of raw material is located at the coastland substantially, and the China's Coastal Areas seawater resources are very abundant, and the usage quantity of as far as possible using seawater, minimizing fresh water on producing just seems extremely important.Therefore, can consider to use seawater to come instead of part fresh water to produce according to the production technique and the water characteristics of carrageenan extraction by eucheuma, water-saving to building, environment-friendly type is social, improve the business economic benefit, Sustainable Development of Enterprises is significant.
Summary of the invention
The purpose of this invention is to provide a kind of method with reducing fresh water dosage during carrageenan extraction by eucheuma, the water characteristics of the technological process of production during according to carrageenan extraction by eucheuma and each operation reach the requirement to water of productive use, in alkaline purification, bleaching process, use seawater to replace fresh water to produce, reduce the usage quantity of fresh water effectively.
The present invention includes following steps:
(1) processing of seawater
With drawing up after the seawater that comes carries out sand filtration, coagulating treatment, add the hydrochloric acid adjust pH and between 6.0-6.5, be stored in the pond, standby;
(2) alkaline purification
Sodium hydroxide is added to the alkali lye that is made into 10-15% concentration in the seawater, in alkali lye, adds 1%KCl then, be heated to 60-65 ℃, add Eucheuma muricatum (Gmel.) Web and handled 12-16 hours;
(3) lixiviating
After the alkaline purification, clean to the pH6.5,, use freshwater soaking then instead 3-5 times, when pH is stabilized in 6.0-6.5, Eucheuma muricatum (Gmel.) Web is pulled out with sea water immersion 2 times with seawater;
(4) carry glue
With carrying glue in the Eucheuma muricatum (Gmel.) Web input boiling water of handling well, put forward the glue water consumption about 40-50 times, 30-40 minutes time; Glue filters, cools off, pushes away bar, and powder-like product is produced in press dewatering, drying, pulverizing, or produces the strip product in freezing 24-36 hours down at-18 ℃, thaws, puts bar then and dry.
It is apparent in view that the present invention reduces the fresh water dosage effect, when producing powdery carrageenin product, can reduce the fresh water usage quantity and reach 42.9%, water-saving to building, environment-friendly type is social, improves the business economic benefit, and enterprise and social sustainable development are significant.
Description of drawings
Fig. 1 is a production scheme of the present invention.
Embodiment
As shown in Figure 1,
To draw up after the seawater that comes carries out sand filtration, coagulating treatment, add hydrochloric acid and adjust the pH value of seawater between 6.0-6.5, inject the seawater after handling in the alkaline purification pond, sodium hydroxide is added the alkali lye that is made into 10---15%, in alkali lye, add 1%KCl then, be heated to 60-65 ℃, drop into Eucheuma muricatum (Gmel.) Web and handle after 12-16 hours, drain alkali lye.The seawater (with the fragrant plant mentioned in ancient texts dry weight basis, below identical) that adds 7 times soaks a little, draining after the stirring and washing, cleans to the pH6.5 with seawater, uses sea water immersion again 2 times, soaks about 1 hour at every turn, uses freshwater soaking then instead.When pH is stabilized in 6.0-6.5, finish the alkaline purification of Eucheuma muricatum (Gmel.) Web, it is pulled out, drop in 40 times the boiling water and carry glue, 30-40 minutes time; The glue that extracts filters, cools off, pushes away bar, press dewatering, drying, pulverizing (production powder-like product); Or descend to thaw, put in freezing 24-36 hours bar at-18 ℃ and dry (producing the strip product).
Carry out concrete test with Eucheuma muricatum (Gmel.) Web below
To draw up after the seawater that comes carries out sand filtration, coagulating treatment, add hydrochloric acid and adjust the pH value of seawater between 6.0-6.5, in the alkaline purification pond, inject 1.0 cubic metres of seawater after handling, sodium hydroxide is added the alkali lye that is made into 10---15%, in alkali lye, add 1%KCl then, be heated to 60-65 ℃, after handling 14 hours in 150 kilograms of Eucheuma muricatum (Gmel.) Webs input alkaline purification ponds, drain alkali lye.Add seawater and soak, stir the back draining a little,, to pH6.5, use sea water immersion again 2 times, soak about 1 hour at every turn, use freshwater soaking then instead through repeated washing.When pH is stabilized in 6.0-6.5, Eucheuma muricatum (Gmel.) Web is pulled out, drop in 6 cubic metres of boiling water and carry glue, 35 minutes time; Glue filters, cools off, pushes away bar, and powdered carrageenin product is produced in press dewatering, drying, pulverizing; Or at-18 ℃ times freezing 30 hours, thaw, put bar then to dry, produce the carrageenin product of strip.
The water consumption situation that seawater replaces fresh water processing to produce
*
Calculate to handle 1 ton of Eucheuma muricatum (Gmel.) Web dry product, produce powder-like product.
In the whole production flow process, the water consumption production powder-like product that replaces fresh water processing to handle 1 ton of Eucheuma muricatum (Gmel.) Web dry product with seawater utilizes 48 cubic metres in seawater, reduces the fresh water usage quantity and reaches 42.9%.Add enterprise with the production of China's Coastal Areas carrageenan extraction by eucheuma and calculate, can save a large amount of fresh water every year, and business economic benefit and social benefit are all very outstanding, and enterprise and social Sustainable development are significant.
Claims (1)
1, a kind of method with reducing fresh water dosage during carrageenan extraction by eucheuma is characterized in that comprising the steps:
(1) processing of seawater
After seawater carried out sand filtration, coagulating treatment, add hydrochloric acid and adjust the pH value, pH is stablized between 6.0-6.5;
(2) utilize seawater that Eucheuma muricatum (Gmel.) Web is carried out alkaline purification
Sodium hydroxide is added to is made into alkali lye in the seawater, concentration adds KCl then in alkali lye between 10-15%, and consumption is heated to 60-65 ℃ in 0.8～1.2% scope, adds Eucheuma muricatum (Gmel.) Web and handles 12-16 hours;
(3) utilizing seawater to carry out lixiviating cleans
After Eucheuma muricatum (Gmel.) Web carries out alkaline purification, clean pH to the Eucheuma muricatum (Gmel.) Web scavenging solution about 6.5,, use freshwater soaking then instead 3-5 times, make pH be stabilized in 6.0-6.5, Eucheuma muricatum (Gmel.) Web is pulled out with sea water immersion 2 times with seawater;
(4) carry glue
With carrying glue in the Eucheuma muricatum (Gmel.) Web input boiling water of handling well, put forward the glue water consumption about 40-50 times, 30-40 minutes time; Glue filters, cools off, pushes away bar, and powder-like product is produced in press dewatering, drying, pulverizing, or produces the strip product in freezing 24-36 hours down at-18 ℃, thaws, puts bar then and dry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102186692A CN101423561B (en) | 2008-10-22 | 2008-10-22 | Method for reducing fresh water dosage during carrageenan extraction by eucheuma |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102186692A CN101423561B (en) | 2008-10-22 | 2008-10-22 | Method for reducing fresh water dosage during carrageenan extraction by eucheuma |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101423561A true CN101423561A (en) | 2009-05-06 |
| CN101423561B CN101423561B (en) | 2011-04-13 |
Family
ID=40614462
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008102186692A Expired - Fee Related CN101423561B (en) | 2008-10-22 | 2008-10-22 | Method for reducing fresh water dosage during carrageenan extraction by eucheuma |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101423561B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101983973A (en) * | 2010-10-08 | 2011-03-09 | 青岛聚大洋海藻工业有限公司 | Extracting and processing technique of carrageen |
| CN102180988A (en) * | 2011-04-15 | 2011-09-14 | 江南大学 | Method for preparing k-carrageenan with high gel strength from eucheuma |
| CN102344499A (en) * | 2010-07-30 | 2012-02-08 | 中国科学院海洋研究所 | Method for preparing Iota-carrageenan |
| CN102633902A (en) * | 2012-05-03 | 2012-08-15 | 临沂艾德森生物科技有限公司 | Carrageenan liquid/jelly, and preparation method and use method thereof |
-
2008
- 2008-10-22 CN CN2008102186692A patent/CN101423561B/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102344499A (en) * | 2010-07-30 | 2012-02-08 | 中国科学院海洋研究所 | Method for preparing Iota-carrageenan |
| CN102344499B (en) * | 2010-07-30 | 2013-03-20 | 中国科学院海洋研究所 | Method for preparing Iota-carrageenan |
| CN101983973A (en) * | 2010-10-08 | 2011-03-09 | 青岛聚大洋海藻工业有限公司 | Extracting and processing technique of carrageen |
| CN102180988A (en) * | 2011-04-15 | 2011-09-14 | 江南大学 | Method for preparing k-carrageenan with high gel strength from eucheuma |
| CN102180988B (en) * | 2011-04-15 | 2012-12-05 | 江南大学 | Method for preparing k-carrageenan with high gel strength from eucheuma |
| CN102633902A (en) * | 2012-05-03 | 2012-08-15 | 临沂艾德森生物科技有限公司 | Carrageenan liquid/jelly, and preparation method and use method thereof |
| CN102633902B (en) * | 2012-05-03 | 2013-01-30 | 临沂艾德森生物科技有限公司 | Carrageenan liquid/jelly, and preparation method and use method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101423561B (en) | 2011-04-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107177996B (en) | A kind of preprocess method of bleached pulp | |
| CN101423561B (en) | Method for reducing fresh water dosage during carrageenan extraction by eucheuma | |
| CN101407832B (en) | Method for producing chitin, calcium citrate and protein powder | |
| CN1943453B (en) | Method for removing orange skin by enzyme | |
| CN100441693C (en) | Process for preparing chitin and chitosan | |
| CN103360509B (en) | Alginic acid and the method for alginic acid salt is prepared for raw material with fresh sargassum | |
| CN104789792B (en) | A kind of technique of nickel citrate catalysis Leaching of Gold Using Thiosulfate | |
| CN103878385B (en) | A kind of method and application thereof that utilizes the green synthesizing water-solubility Nanoscale Iron of mangosteen peel | |
| CN101560270A (en) | Chitin production method with energy-saving and emission-reduction | |
| CN106146687A (en) | A kind of extract the method for pectin in citrus peel residue | |
| CN105800996B (en) | A kind of method that utilization waste wool keratin prepares cement blowing agent | |
| CN103665195B (en) | A kind of method utilizing agar in Enzymatic Extraction fragrant plant mentioned in ancient texts | |
| CN101428841A (en) | Process for producing basic copper carbonate | |
| CN101134786A (en) | Method for producing chitosan-shitosan | |
| CN103689609B (en) | A kind of method adopting enzyme-chemically method to extract food fibre in fresh cassava slag | |
| CN102154867B (en) | Pretreatment method of household paper pulp | |
| CN105639209B (en) | A kind of enteromorpha stichopus japonicus biological feedstuff and preparation method thereof | |
| CN107119477A (en) | A kind of sinocalamus latiflorus true qualities paper pulp and its preparation technology | |
| CN101289380A (en) | Process for preparing calcium propionate by using japanese pearl oyster conch | |
| CN105130224A (en) | Neutral sodium salt alkali-activation low-calcium fly ash cement and use method of same | |
| CN106140084A (en) | A kind of charing stalk/diatomite molecular sieve demanganization filtrate blending nano-manganese dioxide | |
| CN101899583A (en) | Integrative method of two-stage acid leaching, washing and filter pressing for manganese powder pickle liquor | |
| CN102174629A (en) | Method for extracting protein for feed from bowel residue by enzyme hydrolysis method | |
| CN109970163A (en) | A kind of recycling processing method of azo dye wastewater | |
| CN110203957B (en) | Method for preparing nano calcium carbonate based on subcritical hydrolysis method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110413 Termination date: 20121022 |