CN101423219A - Polycrystalline silicon purification or silicon liquid leakage defense device of ingot furnace - Google Patents

Polycrystalline silicon purification or silicon liquid leakage defense device of ingot furnace Download PDF

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Publication number
CN101423219A
CN101423219A CNA2008102028190A CN200810202819A CN101423219A CN 101423219 A CN101423219 A CN 101423219A CN A2008102028190 A CNA2008102028190 A CN A2008102028190A CN 200810202819 A CN200810202819 A CN 200810202819A CN 101423219 A CN101423219 A CN 101423219A
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CN
China
Prior art keywords
platform
silicon liquid
diversion trench
liquid leakage
ingot furnace
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Granted
Application number
CNA2008102028190A
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Chinese (zh)
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CN101423219B (en
Inventor
史珺
宗卫峰
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SHANGHAI PRO ENTERGY TECHNOLOGY Co Ltd
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SHANGHAI PRO ENTERGY TECHNOLOGY Co Ltd
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Priority to CN2008102028190A priority Critical patent/CN101423219B/en
Publication of CN101423219A publication Critical patent/CN101423219A/en
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Publication of CN101423219B publication Critical patent/CN101423219B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention provides a silicon liquid leakage protection device used for a polysilicon purification or ingot furnace, comprising a crucible and a platform; the crucible is arranged on the upper surface of the platform; the silicon liquid leakage protection device is characterized in that the device also comprises a chamfer and a coagulating basin; the upper surface of the platform is provided with a plurality of radial diversion troughs and a plurality of axial diversion troughs; the chamfer is arranged at the periphery of the bottom of the platform; the coagulating basin is arranged on the lower surface of the platform and surrounds the platform by one cycle; the internal circumference of the coagulating basin is arranged inside the chamfer and the external circumference thereof extends to the external surface of the platform; when the silicon liquid leakage protection device used for the polysilicon purification or ingot furnace is adopted, the leaked silicon liquid can completely flow into the coagulating basin by the diversion trough on the platform no matter where the leakage occurs on the crucible, thus preventing the occurrence of equipment damage and explosion and protecting the safety of operators in front of the furnace.

Description

The silicon liquid leakage defense device of a kind of polysilicon purification or ingot furnace
Technical field
The invention belongs to polysilicon and purify or the ingot casting field, the silicon liquid leakage defense device of particularly a kind of polysilicon purification or ingot furnace.
Background technology
At vacuum melting purifying solar energy polysilicon or when carrying out polycrystalline silicon ingot casting, because a variety of causes, the crucible of carrying silicon material can break unavoidably, and causes silicon liquid to leak, and silicon liquid is in case leak, can damage the mechanism's (normally graphite) and the body of heater of support crucible, serious, can cause furnace bottom by burn through, and the water coolant of furnace wall and high temperature silicon liquid are come in contact, and cause exploding, even personal injury.
Silicon liquid leaks and to be caused as crucible itself invisible defect being arranged by multiple reason, and silicon liquid and crucible or its top coat generation chemical reaction cause crucible to corrode, and expansion caused crucible to rise splitting when silicon liquid solidified, or the like.Although take all measures, in polycrystalline silicon ingot casting and purification, silicon liquid leaks and still is difficult to avoid.
Summary of the invention
Main purpose of the present invention is in order to address the above problem; the silicon liquid leakage defense device of a kind of polysilicon purification or ingot furnace is provided; when silicon liquid contingency takes place to leak; this device can be protected the equipment in body of heater and the stove; prevent the generation of structure deteriorate and blast, protection flushing and casting workman's personnel safety.
In order to achieve the above object, technical scheme provided by the invention is: the silicon liquid leakage defense device of a kind of polysilicon purification or ingot furnace comprises crucible, platform, graphite support and stainless steel platform; Graphite props up and is set up in above the stainless steel platform; Platform is located at above the graphite support; Crucible is located at above the platform; Also comprise chamfering and coagulating pan; The platform upper surface has a plurality of radially diversion trenchs and a plurality of broadwise diversion trench; Chamfering is located at the periphery of platform bottom; Coagulating pan is located at the following of platform and around one week of platform; The inside of being located at chamfering interior week of coagulating pan, periphery extends to the outside of platform.
The thickness of platform is at least 50mm.
Radially diversion trench prolongs radially outward from the center of platform and disperses; The broadwise diversion trench is around the center of platform, and is similar to the peripheral shape of platform; Radially diversion trench and described broadwise diversion trench intersect netted.
Radially the quantity of diversion trench is at least 1; The quantity of broadwise diversion trench is at least 1.
Radially the degree of depth of diversion trench and broadwise diversion trench and width are 5mm~40mm; Radially therefrom mind-set is more and more darker outward for diversion trench; It is identical with the degree of depth of its radially diversion trench that intersects that the degree of depth of broadwise diversion trench is followed.
Broadwise diversion trench in outmost turns is opened at least one flow-guiding mouth.
Silicon liquid transmitter is equipped with in the bottom of flow-guiding mouth, and this silicon liquid transmitter is linear transmitter.
The thickness of coagulating pan exceeds with the weight that can carry whole silicon liquid in the crucible; The capacity of coagulating pan exceeds can load silicon liquid whole in the crucible.
Coagulating pan is made up of high-temperature refractory, and this high-temperature refractory is the combination of high alumina, carbon fibre or above-mentioned materials.
Platform is made up of high-temperature refractory, and this refractory materials is the combination of graphite, quartz, miramint or above-mentioned materials.
Positively effect of the present invention is as follows: because platform is provided with diversion trench, be provided with chamfering and coagulating pan below the platform, no matter crucible leaks from any orientation, and the silicon liquid of leakage all can flow in the coagulating pan by the diversion trench on the platform, so thoroughly avoided the generation of various hazardous conditions.
Description of drawings:
Fig. 1: structural representation of the present invention;
Fig. 2: platform vertical view of the present invention.
Embodiment:
As shown in Figure 1, the silicon liquid leakage defense device of a kind of polysilicon purification or ingot furnace comprises crucible 1, platform 2, graphite support 8 and stainless steel platform 9, and graphite support 8 is located at above the stainless steel platform 9; Platform 2 is located at above the graphite support 8; Crucible 1 is located at above the platform 2, and the thickness of platform is at least 50mm, also comprises chamfering 6 and coagulating pan 7, has at least 1 radially diversion trench 3 and at least 1 broadwise diversion trench 4 at platform 2 upper surfaces, and radially diversion trench 3 prolongs radially outward from the center of platform 2 and disperses; Broadwise diversion trench 4 is around the center of platform 2, and is similar to the peripheral shape of platform 2; Radially diversion trench 3 and broadwise diversion trench 4 intersect netted; Radially the degree of depth of diversion trench 3 and broadwise diversion trench 4 and width are 5mm~40mm, and radially therefrom mind-set is more and more darker outward for diversion trench 3, and it is identical with the degree of depth of its radially diversion trench 3 that intersects that the degree of depth of broadwise diversion trench 4 is followed; Open at least one flow-guiding mouth 5 at the broadwise diversion trench 4 of outmost turns, the silicon liquid that flows on the platform 2 from crucible 1 is flowed away by flow-guiding mouth 5, in the bottom of flow-guiding mouth 5 silicon liquid transmitter 10 is installed, this silicon liquid transmitter 10 is linear transmitter, flow down when running into this silicon liquid transmitter 10 at silicon liquid, promptly provide a switch signal, when silicon liquid did not leak, this silicon liquid transmitter 10 provided a reverse switch signal.
Periphery in platform 2 bottoms is provided with chamfering 6, to prevent that silicon liquid from flowing to platform 2 bottom surfaces, one coagulating pan 7 is installed below platform 2, coagulating pan 7 is around 2 one weeks of platform, and interior week is located at the inside of chamfering 6, and periphery extends to the outside of platform 2, and no matter silicon liquid flows out from any orientation, all can flow directly in the coagulating pan 7, the silicon liquid that drips from chamfering 6 also can fall in the coagulating pan 7; The thickness of coagulating pan 7 exceeds with the weight that can carry whole silicon liquid in the crucible 1, and whole silicon liquid exceeds the capacity of coagulating pan 7 in the crucible 1 loading; Coagulating pan 7 is made up of high-temperature refractory, and this high-temperature refractory is the combination of high alumina, carbon fibre or above-mentioned materials, and the speed of response of this material and silicon is slower, can carry out passivation, makes platform 2 surfaces more and more be difficult for reacting with silicon; Platform 2 is made up of refractory materials, and this refractory materials is the combination of graphite, quartz, miramint or above-mentioned materials, and these materials should be able to be high temperature resistant, and do not contain the volatile additive of high temperature.

Claims (10)

1, the silicon liquid leakage defense device of a kind of polysilicon purification or ingot furnace comprises crucible, platform, graphite support and stainless steel platform; Graphite props up and is set up in above the stainless steel platform; Platform is located at above the graphite support; Crucible is located at above the platform, it is characterized in that: also comprise chamfering and coagulating pan; Described platform upper surface has a plurality of radially diversion trenchs and a plurality of broadwise diversion trench; Described chamfering is located at the periphery of platform bottom; Described coagulating pan is located at the following of platform and around one week of platform; The inside of being located at chamfering interior week of described coagulating pan, periphery extends to the outside of platform.
2, the silicon liquid leakage defense device of polysilicon purification according to claim 1 or ingot furnace, it is characterized in that: the thickness of described platform is at least 50mm.
3, the silicon liquid leakage defense device of polysilicon purification according to claim 1 or ingot furnace, it is characterized in that: described radially diversion trench prolongs radially outward from the center of platform to be dispersed; Described broadwise diversion trench is around the center of platform, and is similar to the peripheral shape of platform; Described radially diversion trench and described broadwise diversion trench intersect netted.
4, according to the silicon liquid leakage defense device of claim 1 or 3 described polysilicons purifications or ingot furnace, it is characterized in that: the quantity of described radially diversion trench is at least 1; The quantity of described broadwise diversion trench is at least 1.
5, according to the silicon liquid leakage defense device of claim 1 or 3 described polysilicons purifications or ingot furnace, it is characterized in that: the degree of depth of described radially diversion trench and broadwise diversion trench and width are 5mm~40mm; Therefrom mind-set is more and more darker outward for described radially diversion trench, and it is identical with the degree of depth of its radially diversion trench that intersects that the degree of depth of described broadwise diversion trench is followed.
6, according to the silicon liquid leakage defense device of claim 1 or 3 described polysilicons purifications or ingot furnace, it is characterized in that: the broadwise diversion trench in outmost turns is opened at least one flow-guiding mouth.
7, the silicon liquid leakage defense device of polysilicon purification according to claim 6 and ingot furnace, it is characterized in that: silicon liquid transmitter is equipped with in the bottom of described flow-guiding mouth; This silicon liquid transmitter is linear transmitter.
8, the silicon liquid leakage defense device of polysilicon purification according to claim 1 or ingot furnace, it is characterized in that: the thickness of described coagulating pan exceeds with the weight that can carry whole silicon liquid in the crucible, and the capacity of described coagulating pan exceeds can load silicon liquid whole in the crucible.
9, the silicon liquid leakage defense device of polysilicon purification according to claim 1 or ingot furnace, it is characterized in that: described coagulating pan is made up of high-temperature refractory, and this high-temperature refractory is the combination of high alumina, carbon fibre or above-mentioned materials.
10, the silicon liquid leakage defense device of polysilicon purification according to claim 1 or ingot furnace, it is characterized in that: described platform is made up of refractory materials, and this refractory materials is the combination of graphite, quartz, miramint or above-mentioned materials.
CN2008102028190A 2008-11-17 2008-11-17 Polycrystalline silicon purification or silicon liquid leakage defense device of ingot furnace Expired - Fee Related CN101423219B (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN2008102028190A CN101423219B (en) 2008-11-17 2008-11-17 Polycrystalline silicon purification or silicon liquid leakage defense device of ingot furnace

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CN101423219A true CN101423219A (en) 2009-05-06
CN101423219B CN101423219B (en) 2010-12-08

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101592440B (en) * 2009-07-17 2011-03-16 龙岩市龙创硅业有限公司 Leak-proof protection device of vacuum furnace and formula and preparation process thereof
CN102383183A (en) * 2011-11-04 2012-03-21 湖南顶立科技有限公司 Crystalline silicon ingot casting furnace
CN103370451A (en) * 2011-02-07 2013-10-23 信越半导体股份有限公司 Single crystal production apparatus and single crystal production method

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101592440B (en) * 2009-07-17 2011-03-16 龙岩市龙创硅业有限公司 Leak-proof protection device of vacuum furnace and formula and preparation process thereof
CN103370451A (en) * 2011-02-07 2013-10-23 信越半导体股份有限公司 Single crystal production apparatus and single crystal production method
CN103370451B (en) * 2011-02-07 2016-04-27 信越半导体股份有限公司 Single-crystal manufacturing apparatus and monocrystalline manufacture method
US9422635B2 (en) 2011-02-07 2016-08-23 Shin-Etsu Handotai Co., Ltd. Single crystal production apparatus and single crystal production method having pedestal with grooves
CN102383183A (en) * 2011-11-04 2012-03-21 湖南顶立科技有限公司 Crystalline silicon ingot casting furnace

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C06 Publication
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SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
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EE01 Entry into force of recordation of patent licensing contract

Assignee: Jiangsu strong Photovoltaic Technology Co., Ltd.

Assignor: Shanghai Pro Entergy Technology Co., Ltd.

Contract record no.: 2012320000363

Denomination of invention: Polycrystalline silicon purification or silicon liquid leakage defense device of ingot furnace

Granted publication date: 20101208

License type: Exclusive License

Open date: 20090506

Record date: 20120330

C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20101208

Termination date: 20131117