CN101387584A - Fibre sample auto arranging method based on high voltage electrostatic technique - Google Patents

Fibre sample auto arranging method based on high voltage electrostatic technique Download PDF

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Publication number
CN101387584A
CN101387584A CNA200810042687XA CN200810042687A CN101387584A CN 101387584 A CN101387584 A CN 101387584A CN A200810042687X A CNA200810042687X A CN A200810042687XA CN 200810042687 A CN200810042687 A CN 200810042687A CN 101387584 A CN101387584 A CN 101387584A
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China
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voltage electrostatic
fiber
microslide
sample
fibre
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CNA200810042687XA
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Chinese (zh)
Inventor
赵奕
储晓露
高天琪
邱晓丹
杨若绮
邱夷平
纪峰
张迎晨
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Guangzhou Fibre Product Testing Institute
Donghua University
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Donghua University
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  • Sampling And Sample Adjustment (AREA)

Abstract

The invention relates to a method for utilizing high voltage electrostatic technique to realize fiber sample automatic arrangement, which comprises: cutting an object sample into short segments and dispersing them into dispersed fibers; according to the theory that the fibers can be oriented in a high voltage electrostatic field along the direction of the field direction, parallel and vertically adhering the object short segments of the fiber samples on a glass slide precoated with strip adhesives; combing the fibers to parallel lodging the fibers on the glass slide to produce a glass slide capable of being detected under a microscope. The invention can realize the automatic arrangement of the fiber samples of large number, to improve the efficiency and result accuracy in the process of checking fibers and yarns via microscopic method. The method has simple process, no pollution, easy spread and easy application.

Description

Fibre sample auto arranging method based on high voltage electrostatic technique
Technical field
The invention belongs to textile technology field, particularly relate to a kind of fibre sample auto arranging method based on high voltage electrostatic technique.
Background technology
Yarn constituent comprises that scientific research, trade, criminal investigation, archaeology etc. all are important test items in detecting in a lot of fields.Comparatively the Yarn constituent quantitative detecting method of widespread usage mainly contains microscopy analytic approach (optical microscopy, microscopic projector method and polarization microscope analytic approach) and chemical analysis at present.
Chemical analysis method is according to the dissolution characteristics difference of different types of fiber in certain solution, by sample to be tested being carried out a series of experiments such as weigh-dissolve-dry-weigh to analyze each component content, this method is applicable to the situation that each fibre fractionation chemical component difference is bigger, as hair/cotton, wash/cotton, hair/nitrile mixed yarn etc.; , difficultly detect as cotton/fiber crops, cashmere/wool etc. for the close raw material of chemical constitution with chemical method.For cotton fibriia, also there is chemical method in being dissolved in the finite concentration sulfuric acid solution, to cause the solution absorbency difference to carry out that blending ratio detects according to two kinds of fibers, it is 200510045527.7 that on June 21st, 2006 disclosed application number, publication number is the national inventing patent " method of testing of fiber crops/cotton blending ratio " of CN 1789977A, but this method need have cotton, the fibrilia raw material consistent with blending sample to be measured, so only be fit to the inside plants calibrating, not strong for the detection operability of commodity inspection department.Above-mentioned all chemical methodes all have low, the defect of high cost of detection efficiency, and owing to need the chemical reagent of configuration higher concentration, use in examination of fibers department at present, will produce a large amount of discarded chemical solvent, very easily contaminated environment, hazard detection personnel healths every day.
The microscopy analytic approach comprises optical microscopy, microscopic projector method and polarization microscope method.Optical microscopy is differentiated fiber according to different types of fiber difference vertical, laterally morphological feature; The microscopic projector method is mainly used in the detection that detects the tangible fiber of cross-sectional diameter difference in size and carry out fibre finenesses such as wool; The polarization microscope method is according to the birefraction difference of different types of fiber, or carries out fiber according to the phenomenon of fiber expression characteristics color under polarization microscope and differentiate.Above-mentioned three kinds of microscopy methods are extracted the sample of some and it are separated into staple in bulk from blending product, and each fibre fractionation is differentiated, counted, and the diameter of each component fibre of test some, thereby calculate blending ratio.Close for composition, be difficult to each fibre fractionation with the chemical method discriminating, as cotton/fiber crops, wool/cashmere, Tencel/ viscose glue or the like, adopt above-mentioned microscopy method to carry out qualitative analysis and detection by quantitative to blending product more exactly, simultaneously, because of said method all is the physical detection process, do not relate to pollution problem, so the microscopy analytic approach is considered to the most promising yarn qualities detection method, representing the developing direction of modern textile product detection technique, use more prevalent.
Yet, although the microscopy method has advance and application prospect preferably,, also need survey the diameter of up to a hundred fibers because need to reach thousands of by root discriminating and counting fiber, workload is very big, and this has limited the popularization and application of this method.The main cause that causes this problem is fiber to be measured stochastic distribution in field of view, and orientation is mixed and disorderly, makes testing staff's fatiguability in to the discriminating of a large amount of fibers, counting process, and inefficiency reduces accuracy of detection.The best approach that addresses this problem is to realize the auto arrangement of fiber samples to be measured.At present, still adopt the mode of hand carding fiber arranged in fibre inspection department and universities and colleges, factory, laboratory, as using microscopic projector to carry out in fibre diameter and the composition detection, the fiber arranged sample of mode by hand always.
Summary of the invention
Technical matters to be solved by this invention provides a kind of employing high voltage electrostatic technique, can be in the high-voltage electrostatic field according to fibrous material along the principle of direction of an electric field orientations, realize fiber samples automatically, a kind of fibre sample auto arranging method of proper alignment based on high voltage electrostatic technique.
The technical solution adopted for the present invention to solve the technical problems is: a kind of fibre sample auto arranging method based on high voltage electrostatic technique is provided, comprises the following steps:
(1) sampling: cut the short-movie section sample of isometric fiber to be measured or yarn, sample is dispersed into discrete fibre;
(2) gluing: coat the bar glue that is arranged in parallel on microslide (4) surface and be used for adhering fibre; Microslide (4) coated face is placed electric field down;
(3) stock layout: fiber samples to be measured is placed the high-voltage electrostatic field, and fiber is arranged in parallel and sticks on the bar glue of microslide along direction of an electric field after the energized;
(4) film-making: adopt the method for air-flow combing or mechanical carding to make the parallel lodging of the fiber that vertically adheres on the microslide, make the microslide sample that to examine under a microscope.
Described step (1) cuts rolled state and the obvolvent situation of length according to different fibre compositions, generally between 1~4mm; With fine needle sample is disperseed to be the staple in bulk shape.
The microslide of described step (2) has many finedraws side by side, and stitching wide is 0.2mm, and nip clearance is 3mm or 5mm, and Flock Adhesive is coated on the microslide (4), and bar glue (5) scope of coating accounts for 2/3 of slide.
The high-voltage electrostatic field of described step (3) is the high-voltage electrostatic field of 30~50kV.
Beneficial effect
1. can realize the auto-paralleling arrangement of fiber samples to be measured, be convenient to adopt optical microscope to carry out each fibre composition discriminating, diameter detection, counting experiment.
2. can realize the auto-paralleling arrangement of fiber samples to be measured, composition discriminating, the diameter of fiber samples detect, counting is tested thereby can realize adopting the polarization microscope analytic approach to carry out in batches.
3. can realize the auto-paralleling arrangement of fiber samples to be measured, experiment etc. is differentiated and counted to diameter detection, the composition being convenient to adopt microscopic projector to carry out each fibre fractionation.
4. be physical process, can realize pollution-free detection, meet the fundamental state policy of energy-saving and emission-reduction.
5. being used in combination of high voltage electrostatic technique, computer image processing technology and microscopy method can be realized automatic nesting, counted fiber automatically, thereby realizes that high precision, high efficiency yarn detect, and it is low to detect cost, is beneficial to and applies.
6. can carry out the detection and the analysis of small amount of sample, not destroy original sample, therefore can preserve former state preferably, be beneficial to the precious textile historical relic of protection.
Description of drawings
Fig. 1 adopts high voltage electrostatic technique to realize the device synoptic diagram of fiber samples proper alignment among the present invention.
Fig. 2 is the partial devices synoptic diagram that fiber samples vertically adheres to microslide among the present invention under high voltage electrostatic field.
Fig. 3 is that fiber is vertically being arranged on the microslide and the synoptic diagram of parallel lodging after combing among the present invention.
Fig. 4 adopts the photo (part) that (100 *) are detected under polarization microscope after the method for the invention sample preparation to fiber samples to be measured.
Fig. 5 adopts the photo (part) that (40 *) are detected under polarization microscope after the method for the invention sample preparation to cotton/nitrile blending composition sample.
Among the figure: 1-battery lead plate, 2-electrostatic field, 3-sample, 4-microslide, 5-bar glue
Embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only to be used to the present invention is described and be not used in and limit the scope of the invention.Should be understood that in addition those skilled in the art can make various changes or modifications the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
Fig. 1,2,3 reaches each main operating process synoptic diagram for adopting high voltage electrostatic technique to realize the device synoptic diagram of fiber samples proper alignment among the present invention, and the present invention mainly may further comprise the steps:
(1) sampling: will extract some in fiber to be measured or the yarn samples, cut the neat short-movie section sample of plurality of sections length and place (see figure 1) on the bottom crown 1 of electrostatic field 2 from the different parts of sample with the Ha Shi food slicer, intercepted length is according to the rolled state and the obvolvent situation of different fibre compositions, generally between 1~4mm.With fine needle sample 3 is scatter, be the staple in bulk shape.
(2) gluing: get a clean slide, use special paddle (paddle has many finedraws side by side, and stitching wide is 0.2mm, and nip clearance is two kinds of 3mm, 5mm) that Flock Adhesive is coated on the microslide 4, bar glue 5 scopes of coating account for 2/3 of slide.Microslide 4 coated faces are placed electric field (Fig. 1,2) down.
(3) stock layout: fiber 3 flies to top crown 1 after the energized under the high voltage electrostatic field of 30~50kV, is arranged in parallel and sticks on the bar glue of microslide 4 (Fig. 2,3) along direction of an electric field, and whole process was finished in 1~2 second.Disconnect the electric field power supply, the remaining static on the leadout electrode 1 takes out microslide 4, performs mark on the microslide.Repeat (2)~(3) operating process, adhere on the microslide up to the fiber samples of sufficient amount.
(4) film-making: the method that adopts gentle air-flow combing, make the fiber 3 even parallel lodging (Fig. 3) that vertically are arranged on the microslide 4, also available toothcomb combing makes the fiber 3 of lodging more parallel (during combing, fiber can be coated transparent thick thing such as a little pure glycerin to improve carding effect), covered drips degree of adhesion and the raising degree of getting a clear view of distilled water to increase slide at one jiao of end of cover glass.The slide that makes is placed on microscopically carries out test experience.
Above-mentioned fiber auto arranging method, be applicable to the composition detection of pure fiber textile, and composite fibre textile such as yarn, fabric and non-fibre composition qualitative detection and quantitative test of knitting product etc., can fiber arranged type comprise common natural fiber and man-made fiber, as cotton, wool, cashmere, the rabbit hair, silk, bast-fibre, viscose glue, vinegar ester, terylene, nylon, tygon, polypropylene, polyvinyl etc.

Claims (4)

1. the fibre sample auto arranging method based on high voltage electrostatic technique comprises the following steps:
(1) sampling: cut the short-movie section sample of isometric fiber to be measured or yarn, sample is dispersed into discrete fibre;
(2) gluing: coat the bar glue that is arranged in parallel on microslide (4) surface and be used for adhering fibre; Microslide (4) coated face is placed electric field down;
(3) stock layout: fiber samples to be measured is placed the high-voltage electrostatic field, and fiber is arranged in parallel and sticks on the bar glue of microslide along direction of an electric field after the energized;
(4) film-making: adopt the method for air-flow combing or mechanical carding to make the parallel lodging of the fiber that vertically adheres on the microslide, make the microslide sample that to examine under a microscope.
2. a kind of fibre sample auto arranging method based on high voltage electrostatic technique according to claim 1 is characterized in that: described step (1) cuts rolled state and the obvolvent situation of length according to different fibre compositions, generally between 1~4mm; With fine needle sample is disperseed to be the staple in bulk shape.
3. a kind of fibre sample auto arranging method according to claim 1 based on high voltage electrostatic technique, it is characterized in that: the microslide of described step (2) has many finedraws side by side, stitching wide is 0.2mm, nip clearance is 3mm or 5mm, Flock Adhesive is coated on the microslide (4), and bar glue (5) scope of coating accounts for 2/3 of slide.
4. a kind of fibre sample auto arranging method based on high voltage electrostatic technique according to claim 1 is characterized in that: the high-voltage electrostatic field of described step (3) is the high-voltage electrostatic field of 30~50kV.
CNA200810042687XA 2008-09-09 2008-09-09 Fibre sample auto arranging method based on high voltage electrostatic technique Pending CN101387584A (en)

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Application Number Priority Date Filing Date Title
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CN101387584A true CN101387584A (en) 2009-03-18

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106767439A (en) * 2017-02-13 2017-05-31 北京和众视野科技有限公司 Natural textile fiber length-measuring appliance and its measuring method
CN107345868A (en) * 2016-05-06 2017-11-14 株洲时代新材料科技股份有限公司 Light microscope print apparatus for preparation and light microscope print preparation method
CN108007930A (en) * 2017-12-08 2018-05-08 五邑大学 A kind of textile component analysis method
CN114833043A (en) * 2022-04-24 2022-08-02 浙江大学 Preparation method of high-density high-orientation carbon fiber short fiber array and heat conducting pad

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107345868A (en) * 2016-05-06 2017-11-14 株洲时代新材料科技股份有限公司 Light microscope print apparatus for preparation and light microscope print preparation method
CN106767439A (en) * 2017-02-13 2017-05-31 北京和众视野科技有限公司 Natural textile fiber length-measuring appliance and its measuring method
CN108007930A (en) * 2017-12-08 2018-05-08 五邑大学 A kind of textile component analysis method
CN108007930B (en) * 2017-12-08 2020-11-03 五邑大学 Textile component analysis method
CN114833043A (en) * 2022-04-24 2022-08-02 浙江大学 Preparation method of high-density high-orientation carbon fiber short fiber array and heat conducting pad
CN114833043B (en) * 2022-04-24 2023-09-19 浙江大学 Preparation method of high-density high-orientation carbon fiber short fiber array and heat conducting pad

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Address after: 201620 Shanghai, Songjiang new town, North Road, No. 2999 people

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Open date: 20090318