CN101343512A - Solid fuel adhesive agent and preparation method - Google Patents
Solid fuel adhesive agent and preparation method Download PDFInfo
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- CN101343512A CN101343512A CNA2008100129430A CN200810012943A CN101343512A CN 101343512 A CN101343512 A CN 101343512A CN A2008100129430 A CNA2008100129430 A CN A2008100129430A CN 200810012943 A CN200810012943 A CN 200810012943A CN 101343512 A CN101343512 A CN 101343512A
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- agent
- solid fuel
- adhesive agent
- catalysis
- oxygenant
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
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- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention relates to an adhesive agent, in particular to a solid fuel adhesive agent formed by cold pressing biomaterial solid honeycomb-shaped fuel and the preparation method. The solid fuel adhesive agent is mainly composed of the components according to the weight parts as the following: the ratio between waste paper pulp and corn flour and catalyzing and pasting agent and oxidizing agent and complexing agent is 800 to 900;70 to 150;5 to 15;0.5 to 1.5;0.5 to 1.5. The adhesive agent has the advantages that the process is simple, the reaction temperature is low, the energy consumption and the device investment are low, the operating process is easy to master, the adhesive agent is odorless, and no three wastes are discharged; the initial viscous force is strong, the viscosity is high, the adhesive agent has a certain storage period, the source of the raw material is wide, and the cost is low.
Description
Technical field
The present invention relates to a kind of tackiness agent, relate in particular to the solid fuel adhesive agent and the preparation method of the cellular fuel coldmoulding of a kind of biomass solid.
Background technology
Because the fossil oil crisis, the Chinese government calls energy-saving and emission-reduction, and the while is according to the needs of new socialist countryside construction, rural energy structural reform, development and utilization biomass fuel energetically.The cellular shaped fuel of biomass on the market in recent years because volume is bigger, all over the body honeycomb, is difficult for adopting hot-forming, must take coldmoulding.Therefore need make its bonding jail with tackiness agent, but currently marketed tackiness agent costs an arm and a leg, make the cellular shaped fuel cost of the biomass height of production, be unfavorable for promoting the use of, therefore be badly in need of the tackiness agent that a kind of viscosity is good, price is very cheap.
Summary of the invention
The invention provides a kind of solid fuel adhesive agent and preparation method for solving the problems of the technologies described above, purpose reduces to generate gives birth to this, simplifies production technique.
For reaching above-mentioned purpose solid fuel adhesive agent of the present invention, mainly form by ratio of weight and the number of copies: paper waste: Semen Maydis powder: catalysis paste agent: oxygenant: complexing agent=800-900: 70-150: 5-15: 0.5-1.5: 0.5-1.5 by following component.
Solid fuel adhesive agent mainly is made of by ratio of weight and the number of copies following component: paper waste: Semen Maydis powder: catalysis paste agent: oxygenant: complexing agent=800-900: 90-120: 8-12: 0.8-1.2: 0.8-1.2.
Solid fuel adhesive agent also comprises defoamer, and the ratio of weight and number of paper waste, Semen Maydis powder, catalysis paste agent, oxygenant, complexing agent and defoamer is 800-900: 70-150: 5-15: 0.5-1.5: 0.5-1.5: 0.1-0.5.
Solid fuel adhesive agent, the ratio of weight and number of paper waste, Semen Maydis powder, catalysis paste agent, oxygenant, complexing agent and defoamer is 800-900: 90-120: 8-12: 0.8-1.2: 0.8-1.2: 0.2-0.3.
Described catalysis paste agent is a sodium hydroxide; Oxygenant is hydrogen peroxide, tetrachloric acid's sodium or sodium peroxide; Complexing agent is a sodium tetraborate; Defoamer is a tbp.
The preparation method of solid fuel adhesive agent is made of following component: paper waste: Semen Maydis powder by ratio of weight and the number of copies: catalysis paste agent: oxygenant: complexing agent: defoamer=800-900: 70-150: 5-15: 0.5-1.5: 0.5-1.5: 0.1-0.5; Its preparation method comprise the steps: with the paper waste of above-mentioned parts by weight drop into after the retort beautiful charge level dropped into jar in; Starting agitator stirs; Add oxygenant and catalysis paste agent after the stirring successively and continue at normal temperatures to stir after 0.5-2 hour and be warmed up to 40-50 ℃, be incubated and stop temperature after 0.5-2 hour; Measure the qualified adding complexing agent of viscosity, stir and get final product discharging after 3-10 minute.
The described agitator that starts stirs and is 5-20 minute.
Described beautiful charge level is greater than 80 orders.
Describedly add and to add defoamer after clear water stirs 5-20 minute stopping Wen Houzai, and then viscosimetric; Defoamer is a tbp.
Described catalysis paste agent is a sodium hydroxide; Oxygenant is hydrogen peroxide, tetrachloric acid's sodium or sodium peroxide; Complexing agent is a sodium tetraborate.
Advantageous effect of the present invention: technology is simple, temperature of reaction is low, power consumption less, facility investment is few; Operating procedure is easy to grasp, tasteless, no waste discharge; Initial bonding strength is strong, viscosity fastness is high, certain staging life is arranged; Raw material sources are wide, cost is low.
Embodiment
Embodiment 1
Solid fuel adhesive agent of the present invention will drop into the beautiful charge level of 70kg80 order in the jar after the 800kg paper waste input retort; Starting agitator stirred 5 minutes; After the stirring successively 0.5kg add oxidants hydrogen peroxide and 5kg catalysis paste agent sodium hydroxide and continue at normal temperatures to stir after 0.5 hour and be warmed up to 40 ℃, be incubated and stop temperature after 0.5 hour; Measure the qualified adding of viscosity 0.5kg complexing agent sodium tetraborate, stir and get final product discharging after 3 minutes.
Embodiment 2
Solid fuel adhesive agent of the present invention will drop into the beautiful charge level of 150kg200 order in the jar after the 900kg paper waste input retort; Starting agitator stirred 20 minutes; After the stirring successively 1.5kg add oxygenant sodium peroxide and 15kg catalysis paste agent sodium hydroxide and continue at normal temperatures to stir after 2 hours and be warmed up to 50 ℃, be incubated and stop temperature after 2 hours; Measure the qualified adding of viscosity 1.5kg complexing agent sodium tetraborate, stir and get final product discharging after 10 minutes.
Embodiment 3
Solid fuel adhesive agent of the present invention will drop into the beautiful charge level of 100kg100 order in the jar after the 900kg paper waste input retort; Starting agitator stirred 10 minutes; After the stirring successively 1kg add oxygenant four sodium-chlor and 10kg catalysis paste agent sodium hydroxide and continue at normal temperatures to stir after 1 hour and be warmed up to 45 ℃, be incubated and stop temperature after 1 hour; Measure the qualified adding of viscosity 1kg complexing agent sodium tetraborate, stir and get final product discharging after 5 minutes.
Embodiment 4
Solid fuel adhesive agent of the present invention will drop into the beautiful charge level of 120kg300 order in the jar after the 850kg paper waste input retort; Starting agitator stirred 20 minutes; After the stirring successively 1.2kg add oxygenant sodium peroxide and 8kg catalysis paste agent sodium hydroxide and continue at normal temperatures to stir after 1.5 hours and be warmed up to 48 ℃, be incubated and stop temperature after 0.8 hour; Measure the qualified adding of viscosity 1.2kg complexing agent sodium tetraborate, stir and get final product discharging after 10 minutes.
Embodiment 5
Solid fuel adhesive agent of the present invention will drop into the beautiful charge level of 90kg300 order in the jar after the 800kg paper waste input retort; Starting agitator stirred 15 minutes; After the stirring successively 0.8kg add oxygenant sodium peroxide and 12kg catalysis paste agent sodium hydroxide and continue at normal temperatures to stir after 0.8 hour and be warmed up to 50 ℃, be incubated and stop temperature after 1.2 hours; Measure the qualified adding of viscosity 0.8kg complexing agent sodium tetraborate, stir and get final product discharging after 8 minutes.
Embodiment 6
Add and to add 0.1kg defoamer tbp after clear water stirs 5 minutes stopping Wen Houzai among the embodiment 1, spend 5 minutes after viscosimetric again.Other is with embodiment 1.
Embodiment 7
Add and to add 0.5kg defoamer tbp after clear water stirs 20 minutes stopping Wen Houzai among the embodiment 1, spend 10 minutes after viscosimetric again.Other is with embodiment 1.
Embodiment 8
Add and to add 0.3kg defoamer tbp after clear water stirs 10 minutes stopping Wen Houzai among the embodiment 1, spend 15 minutes after viscosimetric again.Other is with embodiment 1.
Embodiment 9
Add and to add 0.2kg defoamer tbp after clear water stirs 6 minutes stopping Wen Houzai among the embodiment 1, spend 7 minutes after viscosimetric again.Other is with embodiment 1.
Embodiment 10
Add and to add 0.4kg defoamer tbp after clear water stirs 18 minutes stopping Wen Houzai among the embodiment 1, spend 5 minutes after viscosimetric again.Other is with embodiment 1.
Claims (10)
1, solid fuel adhesive agent is characterized in that mainly being made up of by ratio of weight and the number of copies following component: paper waste: Semen Maydis powder: catalysis paste agent: oxygenant: complexing agent=800-900: 70-150: 5-15: 0.5-1.5: 0.5-1.5.
2, solid fuel adhesive agent according to claim 1 is characterized in that mainly being made up of by ratio of weight and the number of copies following component: paper waste: Semen Maydis powder: catalysis paste agent: oxygenant: complexing agent=800-900: 90-120: 8-12: 0.8-1.2: 0.8-1.2.
3, solid fuel adhesive agent according to claim 1, it is characterized in that also comprising defoamer, the ratio of weight and number of paper waste, Semen Maydis powder, catalysis paste agent, oxygenant, complexing agent and defoamer is 800-900: 70-150: 5-15: 0.5-1.5: 0.5-1.5: 0.1-0.5.
4, solid fuel adhesive agent according to claim 3, the ratio of weight and number that it is characterized in that paper waste, Semen Maydis powder, catalysis paste agent, oxygenant, complexing agent and defoamer is 800-900: 90-120: 8-12: 0.8-1.2: 0.8-1.2: 0.2-0.3.
5,, it is characterized in that described catalysis paste agent is a sodium hydroxide according to claim 3 or 4 described solid fuel adhesive agents; Oxygenant is hydrogen peroxide, tetrachloric acid's sodium or sodium peroxide; Complexing agent is a sodium tetraborate; Defoamer is a tbp.
6, the preparation method of solid fuel adhesive agent is characterized in that following component constitutes by ratio of weight and the number of copies: paper waste: Semen Maydis powder: catalysis paste agent: oxygenant: complexing agent: defoamer=800-900: 70-150: 5-15: 0.5-1.5: 0.5-1.5: 0.1-0.5;
Its preparation method comprises the steps:
After the paper waste input retort with above-mentioned parts by weight beautiful charge level is dropped in the jar; Starting agitator stirs; Add oxygenant and catalysis paste agent after the stirring successively and continue at normal temperatures to stir after 0.5-2 hour and be warmed up to 40-50 ℃, be incubated and stop temperature after 0.5-2 hour; Measure the qualified adding complexing agent of viscosity, stir and get final product discharging after 3-10 minute.
7, solid fuel adhesive agent according to claim 6 is characterized in that the described agitator that starts stirs and is 5-20 minute.
8, solid fuel adhesive agent according to claim 6 is characterized in that described beautiful charge level is greater than 80 orders.
9, solid fuel adhesive agent according to claim 6 is characterized in that describedly adding and adding defoamer after clear water stirs 5-20 minute stopping Wen Houzai, and then viscosimetric; Defoamer is a tbp.
10, solid fuel adhesive agent according to claim 6 is characterized in that described catalysis paste agent is a sodium hydroxide; Oxygenant is hydrogen peroxide, tetrachloric acid's sodium or sodium peroxide; Complexing agent is a sodium tetraborate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100129430A CN101343512B (en) | 2008-08-26 | 2008-08-26 | Solid fuel adhesive agent and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100129430A CN101343512B (en) | 2008-08-26 | 2008-08-26 | Solid fuel adhesive agent and preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101343512A true CN101343512A (en) | 2009-01-14 |
| CN101343512B CN101343512B (en) | 2010-09-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2008100129430A Expired - Fee Related CN101343512B (en) | 2008-08-26 | 2008-08-26 | Solid fuel adhesive agent and preparation method |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106520243A (en) * | 2016-12-15 | 2017-03-22 | 榆林学院 | Compound adhesive, briquette coal containing compound adhesive, and briquette coal preparation method |
| CN107298952A (en) * | 2017-06-27 | 2017-10-27 | 南开大学 | A kind of preparation method and its usage of the biomass solid formed fuel adhesive of novel environment friendly |
| CN108003957A (en) * | 2017-11-23 | 2018-05-08 | 莫祖勇 | A kind of biomass solid fuel and preparation method thereof |
-
2008
- 2008-08-26 CN CN2008100129430A patent/CN101343512B/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106520243A (en) * | 2016-12-15 | 2017-03-22 | 榆林学院 | Compound adhesive, briquette coal containing compound adhesive, and briquette coal preparation method |
| CN107298952A (en) * | 2017-06-27 | 2017-10-27 | 南开大学 | A kind of preparation method and its usage of the biomass solid formed fuel adhesive of novel environment friendly |
| CN107298952B (en) * | 2017-06-27 | 2019-02-22 | 南开大学 | A kind of preparation method and its usage of the biomass solid formed fuel adhesive of environmental protection |
| CN108003957A (en) * | 2017-11-23 | 2018-05-08 | 莫祖勇 | A kind of biomass solid fuel and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN101343512B (en) | 2010-09-08 |
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Granted publication date: 20100908 Termination date: 20110826 |