CN101338098A - Method for producing chlorosulfonated polyethylene paint - Google Patents
Method for producing chlorosulfonated polyethylene paint Download PDFInfo
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- CN101338098A CN101338098A CNA2008100123523A CN200810012352A CN101338098A CN 101338098 A CN101338098 A CN 101338098A CN A2008100123523 A CNA2008100123523 A CN A2008100123523A CN 200810012352 A CN200810012352 A CN 200810012352A CN 101338098 A CN101338098 A CN 101338098A
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- paint
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- chlorosulfonated polyethylene
- lacquer
- lacquer bar
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Abstract
The invention provides a production method of chloro-sulfonated polyethylene paint in the field of coatings. The production method comprises the following steps: batching, stirring and mixing, hot compounding, paint strip preparation, paint strip dissolution and paint homogenation. The production method of chloro-sulfonated polyethylene paint has the advantages of high production efficiency, even paint, good dispersivity and no sediment, and is suitable to be used in paint production with chloro-sulfonated polyethylene as membrane.
Description
Technical field
What the present invention proposed is the production method of a kind of chlorosulfonated polyethylene paint of paint field.
Background technology
Before the present invention proposes, have with the chlorosulfonated polyethylene be film forming matter two-pack and single component lacquer arranged, wherein two-pack is to be made of membrane-forming agent and solidifying agent, the mixing through component during use forms the paint vehicle with self cure.Owing to two-pack need be used, the difficult again control of cooperation ratio so cause solidifying excessive or the curing deficiency, directly influences quality and the degree of adhesion and the work-ing life of paint film.And compounding practice is loaded down with trivial details, needs after the cooperation to use at once, and overstand then paint vehicle solidifies, and can't use, and causes the waste of paint vehicle and abandons pollution to environment.
Though the single component chlorosulfonated polyethylene paint need not cooperate the curing paint vehicle separately, the film curing time is long, and hardness is low, also influences the quality of paint vehicle.
Through retrieval, someone has proposed the patent application of single component polyethylene paint, its technology contents is: by chlorosulfonated polyethylene liquid, petroleum resin liquid, titanium dioxide, pigment carbon ink, sulfate precipitate dam, talcum powder, dispersion agent, lubricant, flow agent and thinner composition are formed in the protective system of the present invention.
Implementing product manufacture method of the present invention is:
1, to join content be to form reserve liquid A behind the dissolution filter in 16% the chlorosulfonated polyethylene resin to, 90: 10 mixed solvents of ring ethyl ketone stupid with diformazan;
2, be to form reserve liquid B behind the 50% petroleum resin dissolution filter with the stupid solution of diformazan with content;
3, with A liquid with after B liquid mixes, add after dispersion agent, wetting agent stir, add pigment, filler, thinner again, will be dispersed into the resin that can grind particle diameter after the mixed with resin at last.
4, above-mentioned slip mesh-of-grind qualified after, pour into and be finished product in the paint mixing tank.
Its concentration 16% of described chlorosulfonated polyethylene liquid, be a kind of caking agent, the content during preparation is 40%, caking agent: petroleum resin liquid concentration 50%, content 16%, pigment: titanium dioxide is 10%, colour black 0.1%, filler: process white 16%, talcum powder 6%, auxiliary agent: IFKA-4010 is 0-3%, lubricant IFKA-5065 is 0.2%, auxiliary agent: flow agent IFKA-3777 is 0.4%, thinner: dimethylbenzene: the ring ethyl ketone is 3% at 90: 10.
Though aforesaid method can be made paint, liquid organic solvent and solid-state filler add respectively and blended, are unfavorable for the thorough mixing and the dispersion of raw material, and are difficult to make the paint vehicle of physique uniform and smooth.Because A and B prepare respectively, necessary operate continuously is not easy to interim production, has also limited the raising of throughput.
Also have a kind ofly about the chlorosulfonated polyethylene antifouling paste, it what is claimed is:
1, wet spraying chloro sulfonated polyvinyl anti-corrosion paint is a kind of supporting chlorosulfonated polyethylene antifouling paste, it is characterized in that being made up of chlorosulfonated polyethylene finish paint, intermediary's lacquer, putty.
2, wet spraying chloro sulfonated polyvinyl anti-corrosion paint according to claim 1 is brushed intermediary's lacquer earlier when it is characterized in that constructing, back brush finish lacquer is used for directly brushing on two kinds of situation faces of non-metallic material drying and humidity.
3, chlorosulfonated polyethylene finish paint according to claim 1, it is characterized in that comprising varnish, enamel paint and clay.Be the main body macromolecular material by chlorosulfonated polyethylene rubber, formulated through chemical modification.
4, intermediary according to claim 1 coats with lacquer, and it is characterized in that it is a kind of moisture-hardening varnish.Comprise by a kind of in Resins, epoxy, the NCO performed polymer or two kinds or they again with chlorosulfonated polyethylene rubber, chlorinated rubber, sulfonated elastomer, HTPB, TPS, chlorinatedpolyethylene ether resin, poly-enzyme resin in the moisture-hardening varnish formed for the main body macromolecular material of one or more materials.
5, non-metallic material according to claim 2, it is characterized in that comprising grout, sand-cement slurry, Cement Concrete, acidproof concrete, resin concrete, timber, brick, watt, stone, magnesia goods, plastering etc.
6, chlorosulfonated polyethylene finish paint according to claim 3 is characterized in that can adding strongtheners such as fiber, scale in case of necessity in paint film.
7, chlorosulfonated polyethylene finish paint according to claim 3 is characterized in that not high-order bit of appearance requirement, and available chlorosulfonated polyethylene rubber, NCO performed polymer are that intermediary's lacquer that main body and macromolecular material are formed is made finish paint.
8, putty according to claim 1 is characterized in that, comprises two kinds of putty of the lacquer A.B of chloro-sulfonated polyethylene putty and intermediary.
9, according to claim 1,2 described wet spraying chloro sulfonated polyvinyl anti-corrosion paints, it is characterized in that, form by chlorosulfonated polyethylene finish paint, intermediary's lacquer, intermediary's lacquer B putty or intermediary's lacquer A putty, be used for directly brushing on dry and moist two kinds of situation grouts, sand-cement slurry, the Cement Concrete face.
Summary of the invention
In order to overcome the shortcoming of existing chlorosulfonated polyethylene paint production process, the present invention proposes a kind of production method of chlorosulfonated polyethylene paint.This method solves the technical problem of paint vehicle homogeneous and dispersion and production efficiency by batching, hot milling, compacting slivering, dissolved mode again.
The scheme that technical solution problem of the present invention is adopted is:
1, batching
Chlorosulfonated polyethylene resin is joined in the organic solvent, form bating liquor, in bating liquor, add physique material, color material, auxiliary agent then, in container, mix, become compound by design flow.
2, mix
Compound is stirred, make it further thorough mixing, form raw materials for varnish.
3, hot milling
Raw materials for varnish is joined in the mixing roll, roll under heating condition, mixing, melting temperature is controlled at 80～100 ℃, becomes mixing materials.
4, make the lacquer bar
Mixing materials by plodder, is suppressed into the lacquer bar, becomes the dried lacquer bar, length 3～5cm, diameter 0.5～2cm.
5, lacquer bar dissolving
The dried lacquer bar is put in the dissolution kettle, is added organic solvent, under the state that stirs with dried lacquer bar dissolving becoming dispersive paint vehicle.
6, paint vehicle homogeneous
Paint vehicle is joined in the clarifixator, carry out homogeneous after, become finished product paint.
The inventive method system of employing chlorosulfonated polyethylene paint production efficiency height, paint vehicle is even, and good dispersity does not precipitate.Suit in the paint vehicle that with the chlorosulfonated polyethylene is film forming matter is produced, to use.
Embodiment
1, batching
Chlorosulfonated polyethylene resin is joined in the organic solvent, form bating liquor, in bating liquor, add physique material, color material, auxiliary agent then, in container, mix, become compound by design flow.
2, mix
Compound is stirred, make it further thorough mixing, form raw materials for varnish.
3, hot milling
Raw materials for varnish is joined in the mixing roll, roll under heating condition, mixing, melting temperature is controlled at 80～100 ℃, becomes mixing materials.
4, make the lacquer bar
Mixing materials by plodder, is suppressed into the lacquer bar, becomes the dried lacquer bar, length 3～5cm, diameter 0.5～2cm.
5, lacquer bar dissolving
The dried lacquer bar is put in the dissolution kettle, is added organic solvent, under the state that stirs with dried lacquer bar dissolving becoming dispersive paint vehicle.
6, paint vehicle homogeneous
Paint vehicle is joined in the clarifixator, carry out homogeneous after, become finished product paint.
Because paint vehicle is by the mixing physique material and the full and uniform mixing of filler that can make in the paint vehicle.Because paint vehicle is made the dried lacquer bar, help transportation and keeping, enhance productivity, and made lacquer bar is convenient to dissolve lacquering.
The prepared paint of the present invention is solvent evaporates air curing resin type lacquer class, and spreadability is strong, and paint suitable anticorrosion, that isolate, decorate uses.
The character of chlorosulfonated polyethylene
Chlorosulfonated polyethylene is white or yellow elastomerics, general character with rubber, has self distinctive performance simultaneously, can be dissolved in aromatic hydrocarbon and hydrochloric ether is insoluble in fat and the alcohol, in ketone and ether, can only swelling can not dissolve, excellent ozone resistance, resistance to weathering, chemical resistance etc. are arranged, better physical mechanical property, ageing-resistant performance, heat-resisting and lower temperature resistance, oil-proofness, flame resistivity, wear resistance, and anti-electrical insulating property.
Claims (1)
1, a kind of production method of chlorosulfonated polyethylene paint is characterized in that:
1. prepare burden: chlorosulfonated polyethylene resin is joined in the organic solvent, form bating liquor, in bating liquor, add physique material, color material, auxiliary agent then, in container, mix, become compound by design flow;
2. mix: compound is stirred, make it further thorough mixing, form raw materials for varnish;
3. hot milling: raw materials for varnish is joined in the mixing roll, roll under heating condition, mixing, melting temperature is controlled at 80～100 ℃, becomes mixing materials;
4. make the lacquer bar: mixing materials by plodder, is suppressed into the lacquer bar, becomes the dried lacquer bar, length 3～5cm, diameter 0.5～2cm;
5. coat with lacquer bar dissolving: the dried lacquer bar is put in the dissolution kettle, is added organic solvent, under the state that stirs with dried lacquer bar dissolving becoming dispersive paint vehicle;
6. paint vehicle homogeneous: paint vehicle is joined in the clarifixator, carry out homogeneous after, become finished product paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100123523A CN101338098B (en) | 2008-07-14 | 2008-07-14 | Method for producing chlorosulfonated polyethylene paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100123523A CN101338098B (en) | 2008-07-14 | 2008-07-14 | Method for producing chlorosulfonated polyethylene paint |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101338098A true CN101338098A (en) | 2009-01-07 |
| CN101338098B CN101338098B (en) | 2011-02-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100123523A Expired - Fee Related CN101338098B (en) | 2008-07-14 | 2008-07-14 | Method for producing chlorosulfonated polyethylene paint |
Country Status (1)
| Country | Link |
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| CN (1) | CN101338098B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101942153A (en) * | 2010-10-22 | 2011-01-12 | 南京长江涂料有限公司 | Single-component chlorosulfonated polyethylene anticorrosive paint and preparation method thereof |
| CN102977692A (en) * | 2012-12-12 | 2013-03-20 | 辽宁啄木鸟漆业发展有限公司 | Method for preparing anion bowlder paint |
| CN103013235A (en) * | 2012-12-09 | 2013-04-03 | 葫芦岛市恒通特种漆有限公司 | Chlorosulfonated polyethylene voltage-resistance and high-performance special anticorrosive paint and production method thereof |
| CN103073991A (en) * | 2013-01-06 | 2013-05-01 | 葫芦岛市恒通特种漆有限公司 | Method for preparing low temperature resistant and corrosion proof coating |
| CN104673000A (en) * | 2014-10-25 | 2015-06-03 | 青岛中天信达生物技术研发有限公司 | Preparation method of anticorrosive coating |
-
2008
- 2008-07-14 CN CN2008100123523A patent/CN101338098B/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101942153A (en) * | 2010-10-22 | 2011-01-12 | 南京长江涂料有限公司 | Single-component chlorosulfonated polyethylene anticorrosive paint and preparation method thereof |
| CN101942153B (en) * | 2010-10-22 | 2012-07-04 | 南京长江涂料有限公司 | Single-component chlorosulfonated polyethylene anticorrosive paint and preparation method thereof |
| CN103013235A (en) * | 2012-12-09 | 2013-04-03 | 葫芦岛市恒通特种漆有限公司 | Chlorosulfonated polyethylene voltage-resistance and high-performance special anticorrosive paint and production method thereof |
| CN103013235B (en) * | 2012-12-09 | 2015-01-21 | 葫芦岛市恒通特种漆有限公司 | Chlorosulfonated polyethylene voltage-resistance and high-performance special anticorrosive paint and production method thereof |
| CN102977692A (en) * | 2012-12-12 | 2013-03-20 | 辽宁啄木鸟漆业发展有限公司 | Method for preparing anion bowlder paint |
| CN102977692B (en) * | 2012-12-12 | 2015-11-04 | 啄木鸟漆业集团有限公司 | A kind of anion bowlder paint preparation method |
| CN103073991A (en) * | 2013-01-06 | 2013-05-01 | 葫芦岛市恒通特种漆有限公司 | Method for preparing low temperature resistant and corrosion proof coating |
| CN103073991B (en) * | 2013-01-06 | 2016-06-01 | 葫芦岛市恒通特种漆有限公司 | The production method of a kind of coating of resistance to low-temperature corrosion protection |
| CN104673000A (en) * | 2014-10-25 | 2015-06-03 | 青岛中天信达生物技术研发有限公司 | Preparation method of anticorrosive coating |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101338098B (en) | 2011-02-16 |
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Effective date of registration: 20170808 Address after: 125003 Liaoning province Huludao City Peikang Industrial Zone Patentee after: Huludao industry and Trade Co. Ltd. and anti-corrosion through Bo ship Address before: Huludao City, Liaoning Province, 125003 North Road, Longgang District No. 123 Patentee before: Huludao Hengtong Special Paint Co., Ltd. |
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Granted publication date: 20110216 Termination date: 20200714 |
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