CN101279893B - High-efficient extraction equipment of natural borneol - Google Patents
High-efficient extraction equipment of natural borneol Download PDFInfo
- Publication number
- CN101279893B CN101279893B CN2008100313852A CN200810031385A CN101279893B CN 101279893 B CN101279893 B CN 101279893B CN 2008100313852 A CN2008100313852 A CN 2008100313852A CN 200810031385 A CN200810031385 A CN 200810031385A CN 101279893 B CN101279893 B CN 101279893B
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- CN
- China
- Prior art keywords
- retort
- charging basket
- distillation
- natural borneol
- condensation collector
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 229940116229 borneol Drugs 0.000 title claims abstract description 23
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 title claims abstract description 22
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 title claims abstract description 22
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 title claims abstract description 22
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 238000000605 extraction Methods 0.000 title abstract description 7
- 238000009833 condensation Methods 0.000 claims abstract description 19
- 230000005494 condensation Effects 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000004821 distillation Methods 0.000 claims abstract description 15
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 11
- 238000007599 discharging Methods 0.000 claims abstract description 5
- 239000000945 filler Substances 0.000 claims description 6
- 239000010865 sewage Substances 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 3
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 claims description 2
- 230000002093 peripheral effect Effects 0.000 claims 1
- 230000007306 turnover Effects 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 2
- 241000723346 Cinnamomum camphora Species 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 4
- 241000907904 Dipterocarpus Species 0.000 description 2
- 240000005636 Dryobalanops aromatica Species 0.000 description 2
- 229960000846 camphor Drugs 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000035924 thermogenesis Effects 0.000 description 2
- DTGKSKDOIYIVQL-NQMVMOMDSA-N (+)-Borneol Natural products C1C[C@]2(C)[C@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-NQMVMOMDSA-N 0.000 description 1
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
- 244000080208 Canella winterana Species 0.000 description 1
- 235000008499 Canella winterana Nutrition 0.000 description 1
- 241000201295 Euphrasia Species 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 125000002604 borneol group Chemical group 0.000 description 1
- 229930008380 camphor Natural products 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000017074 necrotic cell death Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a high-efficiency extraction device for natural borneol, which comprises a charging basket with a plurality of vent holes, a distillation retort, a water adding pipe, a feed liquid steam pipe and a condensation collector; the side surface of the distillation tank is provided with a charging basket access and a drain outlet at the bottom, a heating coil is arranged at the bottom in the distillation tank, a guide rail is arranged above the heating coil, and the charging basket is positioned on the guide rail and can extend out of the distillation tank from the access for charging or discharging; the water adding pipe extends into the distillation retort to add the water required by distillation, one end of the feed liquid steam pipe is communicated with the distillation retort from the top of the distillation retort, the other end of the feed liquid steam pipe is communicated with the condenser from the lower end of the condenser, and the condensation collector comprises a barrel body, a circulating water jacket on the periphery of the barrel body and an electric scraper in the barrel body. The invention adopts mechanical automation, so that the extraction rate of the natural borneol reaches up to 1.0 percent, and the invention has the advantages of low extraction cost, simple process and convenient operation, thereby being capable of industrially producing the natural borneol in large batch and meeting the market requirement.
Description
Technical field
The present invention relates to a kind of natural Broneolum Syntheticum and extract equipment.
Technical background
Natural Broneolum Syntheticum (Borneolum) original name " Dipterocarpus pilosus " claims natural d-Bomeol again, is commonly called as the plum sheet, and molecular formula is C
10H
18O.It originates in the archipelago, Sumatera of Indonesia, is from the trunk of Dipterocarpus pilosus [Dryobalanopsaromatica Gaertmer] crystallized product through steam distillation.Its gas delicate fragrance, bitter, Xin Liang have logical all keys, loose stagnated fire, swelling and pain relieving, heat reliving and toxin-eliminating, remove the screen medicinal functions such as inducing resuscitation, removing necrosis, promoting granulation, anticancer that make eye bright, have one's ideas straightened out, and are a kind of famous and precious rare medicinal material and senior spices.
At present, the borneo camphor tree of processing natural Broneolum Syntheticum is closely exhausted.For solving the present situation of natural Broneolum Syntheticum shortage of resources, the scientific research personnel of Chinese forest-science academy is seeking the resource of preparation natural Broneolum Syntheticum always.Up to the beginning of the nineties in last century, the applicant has found a kind of canella of extracting natural Broneolum Syntheticum--borneol camphor tree in the virgin forest in township falls in the step head of 800 meters of the domestic height above sea level of the new rolling in Hunan.Through research in a few years, invented a kind of " extract d-Bomeol technology " and obtained national inventing patent in 1994 from camphor leaf.Developed some production units subsequently, because borneol camphor tree branches and leaves proportion is little, shared volume is bigger, and present equipment can not feed intake in a large number, and the finished product generally adopt manual the collection to cause output lower, and the natural Broneolum Syntheticum extraction yield is relatively low.Along with some international and domestic cosmetics of super quality, medicine, food, essence and flavoring agent grow with each passing day to the demand of natural Broneolum Syntheticum, make that the natural Broneolum Syntheticum suitability for industrialized production is extremely urgent, therefore how making natural Broneolum Syntheticum can mass industrialized production be present problem demanding prompt solution.
Summary of the invention
The object of the present invention is to provide a kind of efficient extracting device for natural borneol that can make natural Broneolum Syntheticum carry out large-scale industrial production.
This efficient extracting device for natural borneol provided by the invention comprises charging basket, retort, filler pipe, feed liquid vapour pipe, condensation collector with many ventilating pits; The retort side has the charging basket gangway, sewage draining exit is arranged at the bottom, and in retort, heating coil is arranged at the bottom, and this heating coil top has guide rail, charging basket to be located in can stretch out retort charging or discharging from the gangway on the described guide rail; Filler pipe puts in and adds distillation time institute's water requirement in the retort, one end of feed liquid vapour pipe is communicated with retort from the top of retort, the other end is communicated with the condensation collector from the lower end of condensation collector, the condensation collector comprises staving, the recirculated water water jacket of staving periphery, bucket intravital one electronic scraper plate.
The present invention is because charging basket can debouch retort under exogenetic process, therefore can feed fast automatically and discharging by travelling belt, and electronic scraper plate has been adopted in the collection of the finished product of the present invention, can directly will scrape down attached to the borneol on the borneol collector staving inwall.The present invention adopts mechanical automation, make the natural Broneolum Syntheticum extraction yield up to 1.0%, and extraction cost is low, and technology is simple, and is easy to operate, so energy mass industrialized production natural Broneolum Syntheticum satisfies the needs in market.
Description of drawings
Fig. 1 is a structural representation of the present invention.
Fig. 2 is the borneol collector synoptic diagram of one embodiment of the present invention.
Embodiment
From Fig. 1 and Fig. 2 as can be seen, efficient extracting device for natural borneol of the present invention mainly is made up of charging basket 1, retort 2, feed liquid vapour pipe 3, condensation collector 4, electronic scraper plate 5.The side of retort 2 has charging basket gangway 21, and sewage draining exit 22 is arranged at the bottom, and wash tube 9 is arranged at the top.In retort 2, heating coil 10 is arranged at the bottom, there is guide rail 6 this heating coil top, charging basket 1 is located on the guide rail 6, and can move along guide rail 6, after charging basket 1 entered retort 2, its end cap 11 can be buckled on the retort 2 21 sealings of charging basket gangway, charging basket 1 can stretch out under the drive of power cylinder 8 that retort is feeded or discharging from the gangway, and power cylinder 8 can be that cylinder also can be an oil cylinder.Filler 7 is to be used to add distillation time institute's water requirement, has been covered with ventilating pit 12 on the charging basket 1, and when heating coil 10 adds thermogenesis steam with the water in the retort, steam will enter charging basket by ventilating pit 12 the borneol Leaf of Camphortree is carried out boiling.The distiller top is connected with feed liquid vapour pipe 3, and this pipe is sent feed liquid steam into condensation collector 4 by valve 31 controls from the bottom.Condensation collector 4 comprises watercooling jacket 43, the cleaning valve 49 at staving top, the filtering net 44 of staving 41 bottoms, products export 45, the wash water valve 46 of staving 41, visor 42, staving periphery, electronic scraper plate 5 in the staving 41, electronic scraper plate 5 is made up of explosion-proof reducing motor 51, axle 52, scraper plate 53.Cold water inlet 47 is in water jacket 43 bottoms, and rising pipe 48 is on the top of water jacket 43, for water jacket 43 provides recirculated cooling water.
During the present device operation, clean by 9 pairs of distiller inwalls of wash tube earlier, the needed water yield when replenishing distillation by filler pipe again, then drive slowly outer 2/3rds places that move to charging basket of charging basket by cylinder, then borneol camphor tree branches and leaves (raw material) are filled head tank, and then by cylinder charging basket is advanced in the distiller, begin to add thermogenesis steam by heating coil 10, the borneol camphor tree branches and leaves in the charging basket are added thermal distillation.After 20 minutes to be distilled, open valve 31, steam is imported in the condensation collector 4 by feed liquid vapour pipe 3.When borneol camphor tree branches and leaves are heated to certain temperature in distiller after, make the natural Broneolum Syntheticum distillation in the borneol camphor tree branches and leaves, sublimate enters condensation-crystallization in the condensation collector with steam then, feed cold water in the water jacket of condensation this moment collector, when distillation finishes, closed heating coil 10 and valve 31 earlier, start cylinder, drive charging basket by cylinder and move outward, distilled branches and leaves are discharged on the conveying belt, be delivered to again between the waste material storage.Meanwhile open electronic scraper plate 5, close electronic scraper plate 5 after moving 5 minutes approximately, will scrape, open products export 45 again, collect natural Broneolum Syntheticum attached to the crystal on the condensation collector wall.After product has been collected, open cleaning valve, the condensation collector is cleaned, it is that task is prepared down that sewage is got rid of from wash water valve 46.
Claims (4)
1. an efficient extracting device for natural borneol is characterized in that comprising charging basket (1), retort (2), filler pipe (7), feed liquid vapour pipe (3), condensation collector (4) with many ventilating pits; The retort side has charging basket gangway (21), the bottom has sewage draining exit (22), top that wash tube is arranged, in retort, heating coil (10) is arranged at the bottom, and this heating coil top has guide rail (6), charging basket (1) to be located in can stretch out retort charging or discharging from the gangway on the described guide rail; Filler pipe (7) puts in and adds distillation time institute's water requirement in the retort, one end of feed liquid vapour pipe (3) is communicated with retort (2) from the top of retort (2), the other end is communicated with condensation collector (4) from the lower end of condensation collector (4), condensation collector (4) comprises staving (41), electronic scraper plate (5) in the recirculated water water jacket (43) that staving (41) is peripheral, staving (41).
2. efficient extracting device for natural borneol according to claim 1 is characterized in that described charging basket is connected with a power cylinder (8), drives charging basket (1) turnover retort (2).
3. efficient extracting device for natural borneol according to claim 1 and 2 is characterized in that the top of described retort is provided with the wash tube (9) that is used to clean retort.
4. efficient extracting device for natural borneol according to claim 1 and 2 is characterized in that described condensation collector is provided with the cleaning valve (49) that is used to clean the borneol collector.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100313852A CN101279893B (en) | 2008-05-26 | 2008-05-26 | High-efficient extraction equipment of natural borneol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008100313852A CN101279893B (en) | 2008-05-26 | 2008-05-26 | High-efficient extraction equipment of natural borneol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101279893A CN101279893A (en) | 2008-10-08 |
| CN101279893B true CN101279893B (en) | 2010-12-08 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008100313852A Expired - Fee Related CN101279893B (en) | 2008-05-26 | 2008-05-26 | High-efficient extraction equipment of natural borneol |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101279893B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102512839B (en) * | 2011-12-24 | 2015-06-17 | 吉安市林业科学研究所 | Natural d-borneol extraction equipment |
| CN103265406B (en) * | 2013-05-29 | 2015-06-03 | 华南理工大学 | Complete set extraction equipment of natural d-borneol suitable for field work and application of complete set extraction equipment |
| CN104756678B (en) * | 2015-03-16 | 2016-08-17 | 江苏金叶子生物科技有限公司 | A kind of Borneolum Syntheticum Camphor tree cuts mining method |
| CN104711123B (en) * | 2015-03-16 | 2018-02-23 | 江苏金叶子生物科技有限公司 | A kind of device that natural borneol is slightly carried from borneol camphor tree |
| CN104693008B (en) * | 2015-03-16 | 2017-02-22 | 江苏金叶子生物科技有限公司 | Method for coarsely extracting natural borneol from cinnamomum camphora |
| CN107158732A (en) * | 2017-07-11 | 2017-09-15 | 苏州卓融新能源科技有限公司 | A kind of reduction device for PCB waste liquids |
| CN113149815A (en) * | 2021-05-13 | 2021-07-23 | 安徽右旋龙脑生物科技有限公司 | Extraction system and extraction method of high-purity borneol |
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2008
- 2008-05-26 CN CN2008100313852A patent/CN101279893B/en not_active Expired - Fee Related
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| CN101279893A (en) | 2008-10-08 |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Efficient extracting device for natural borneol Effective date of registration: 20120515 Granted publication date: 20101208 Pledgee: Xinhuang Dong Autonomous County Rural Credit Cooperative Association Pledgor: Hunan Xinhuang Longnao Development Co., Ltd. Registration number: 2012990000209 Denomination of invention: Efficient extracting device for natural borneol Effective date of registration: 20120515 Granted publication date: 20101208 Pledgee: Xinhuang Dong Autonomous County Rural Credit Cooperative Association Pledgor: Hunan Xinhuang Longnao Development Co., Ltd. Registration number: 2012990000209 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20140408 Granted publication date: 20101208 Pledgee: Xinhuang Dong Autonomous County Rural Credit Cooperative Association Pledgor: Hunan Xinhuang Longnao Development Co., Ltd. Registration number: 2012990000209 Date of cancellation: 20140408 Granted publication date: 20101208 Pledgee: Xinhuang Dong Autonomous County Rural Credit Cooperative Association Pledgor: Hunan Xinhuang Longnao Development Co., Ltd. Registration number: 2012990000209 |
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| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20101208 Termination date: 20190526 |