CN101249048B - Elevated plain loessial processing method and applications in producing beauty treatment article - Google Patents
Elevated plain loessial processing method and applications in producing beauty treatment article Download PDFInfo
- Publication number
- CN101249048B CN101249048B CN2007103055059A CN200710305505A CN101249048B CN 101249048 B CN101249048 B CN 101249048B CN 2007103055059 A CN2007103055059 A CN 2007103055059A CN 200710305505 A CN200710305505 A CN 200710305505A CN 101249048 B CN101249048 B CN 101249048B
- Authority
- CN
- China
- Prior art keywords
- loess
- plateau
- precipitation
- add
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention provides a method for treating plateau loess. The method comprises the steps of selection, refining, micropore formation and sterilization. The method can improve the composition of the plateau loess and simultaneously remove useless substances and harmful microorganisms and bacteria. The treated plateau loess is rich in minerals, trace elements and collagens which are beneficial for health protection and beautification. Therefore, the treated plateau loess can be used as raw materials of cosmetics and skin care products such as facial masks, scrubbing cream and bath shampoo.
Description
Technical field
The invention belongs to field of fine chemical, relate to a kind of raw material of producing cosmetics and skincare product, especially be particularly related to a kind of plateau loess that is used to produce cosmetics and skincare product; Also relate to the processing method and the application in producing the beauty and skin care product of plateau loess simultaneously.
Background technology
The Qinghai-Tibet Platean is the 3rd utmost point in the world, is the highest area of height above sea level in the world.The Qinghai-Tibet Platean spreads all over many special soil properties, and loess is exactly a part wherein.These loess contain a large amount of mineral, trace element, microtriche pore and colloidal substance.Through identifying that the plateau loess mineral and the content of elements of natural ecological are as follows: ferrum 0.02～5%, sodium 0.02～5%, potassium 0.02～5%, magnesium 0.02～5%, boron 0.02～5%, lithium 0.02～5%, selenium 0.02～5%, calcium 0.02～5%, zinc 0.02～5%.Because plateau loess is rich in several mineral materials, trace element, microtriche pore and collagen protein, human body there are health care, beautification function preferably.
Summary of the invention
The processing method that the purpose of this invention is to provide a kind of plateau loess;
Another object of the present invention just provides the application of plateau loess in producing the beauty and skin care product.
The processing method of plateau of the present invention loess comprises following processing step:
1. select: utilize Chemical Physics Processing to remove the unhelpful composition that plateau loess contains, concrete technology is as follows:
A, washing: with the water washing of plateau loess 1～10 times of volume, make the nutrient dissolving in the loess of plateau, precipitation is collected supernatant then, concentrates to remove 80～99% water and get nutritional solution, and is stand-by;
The washing water can be snow water, lake water, sea water, well water, tap water etc., also can be the combination at several water sources wherein.
B, alkali cleaning: in above-mentioned precipitation, add alkali liquid washing, remove the unhelpful composition that can be dissolved in alkali in the loess of plateau, especially deleterious heavy metal ion; The pH of control dispersion is at 7.2～14 (best 8～13.8) in the washing, and precipitation is removed supernatant then.
Alkali liquor can be one or more in sodium hydroxide, potassium hydroxide, ammonia, sodium sulfide, carbonate, subcarbonate, NaHS, phosphate, subphosphate, the organic base etc.
C, pickling: in precipitation, continue to add the acid solution washing, remove the unhelpful composition that is dissolved in acid in the loess of plateau, especially deleterious heavy metal ion; The pH of control dispersion is at 0.1～6.8 (best 0.4～5.8) during washing, and precipitation is removed supernatant then.
Acid solution can be one or more in hydrochloric acid, sulphuric acid, sulfur hydracid, phosphoric acid, organic acid, the nitric acid etc.
D, neutralization: add in the weak base and excessive acid, the pH of control dispersion is between 4～10, and precipitation is removed supernatant;
E, in precipitation, add a gained nutritional solution.In order to improve the nutritional labeling of plateau loess, in precipitation, also can add the nutrient of loess weight 0.001～30%.The nutrient here can be other micromolecule nutrients and macromole nutrients such as any group vitamins, needed by human body trace element, human hormone, protein, polypeptide, saccharide, cellulose, oils and fats.
Supernatant after above-mentioned alkali cleaning, pickling and the neutralization is collected, mix the back and removes the heavy metal ion that is dissolved in the water, and concentratedly remove recyclable utilization behind the moisture with traditional " two alkaline process " technology.
2. refinement: adopt the mode of physics to be refined into the granule that particle diameter is 1mm～1nm through the above-mentioned loess of selecting; Can adopt ball mill, grinder etc. to realize the purpose of plateau loess micropowder.
3. microporeization: add the water of plateau loess quality 5%～50%, stir, at 120～180 ℃ of following evaporative removal moisture, make the loess particle surface form a large amount of micropores then.
For structure and the composition that makes plateau loess better improved, the pH value of adjusting water is 2～12, and the micro-pore diameter that forms with control loess particle surface is controlled between 0.1mm～0.1nm.Here employed pH value regulator is water miscible alkali and salt sour and that have Acidity of Aikalinity.
4. sterilization: adopt high temperature and/or ultraviolet to carry out disinfection, remove the harmful microorganism in the loess, promptly get the plateau loess of improveing.
The inventive method is handled in the plateau loess of improvement, and the percentage composition of the percentage composition trace element of its mineral and trace element is controlled at:
Ferrum 0.02～5%, sodium 0.02～5%, potassium 0.02～5%, magnesium 0.02～5%, boron 0.02～5%,
Lithium 0.02～5%, selenium 0.02～5%, calcium 0.02～5%, zinc 0.02～5%.
Because the plateau loess after the improvement is rich in a large amount of mineral, trace element, microtriche pore and collagen protein, have and enhance metabolism, make skin white and moist, soft and smooth, deep layer cleaning skin improves oils and fats distribution in the body, remove acne, acne, reduce wrinkle, eliminate interior free yl, defying age, eliminate effects such as ultraviolet, therefore can be used as the raw material of producing the beauty and skin care product.
The specific embodiment
Below by some specific embodiments improved process and improved effect to plateau loess are described, and to its in producing cosmetics should be as specifying.
Embodiment 1
Get the loess of 100 gram Qinghai-Tibet Plateans, and measure various trace element and essential element in the loess, data following (unit: restrain):
Ferrum 3.51, sodium 0.12, potassium 0.12, magnesium 0.36, boron 0.05, lithium 0.02, selenium 0.12, calcium 3.5, zinc 0.041;
Select: will gather the plateau loess and the mixed of water according to 1: 1 that come, and break into mud, centrifugalize then separates the solution on upper strata, takes out the plateau loess of separating, and concentrated supernatant liquid is removed 95% water; With sodium hydroxide, sodium carbonate, the ammonia aqueous solution alkali cleaning of pH=13, centrifugalize, detect plateau loess, mercury content is ppm0.2; Continue hydrochloric acid and hydrogen sulfide solution pickling plateau loess with pH=4, the arsenic content that detects in the loess of plateau is ppm0.1; Mixed acid washing liquid and alkali wash water add sodium hydroxide and sodium carbonate, are settled out hydrargyrum and arsenic; Concentrate with pH=10 onium hydroxide solution neutralizing acid washing liquid,, pickle, alkali wash water and neutralising fluid are mixed, transfer pH=7, concentrate and remove 95% water, join in the upper strata concentrated solution that centrifugalize goes out to pH=7; With this part the concentrated plateau loess of also putting into, add 0.1% vitamin E, highland barley soy Protein, Semen avenae nudae polysaccharide, highland barley embryo bud oil oven dry, remove moisture, the plateau loess powder that obtains selecting.
Refinement: adopt with three roller ball mill grindings, loess is ground to form the granule that granularity is 1mm～1nm.
Microporeization: the pure water that adds plateau loess quality 20% stirs, and makes the loess aquation, at 150 ℃ of following evaporative removal moisture, makes the loess particle surface have a large amount of micropores then.The micro-pore diameter that obtains the formation of loess particle surface is controlled at 0.1mm.
Sterilization: adopt what mode to sterilize and remove detrimental microorganisms, promptly get the plateau loess of improveing.After testing, the total content of microorganisms in this loess is less than 5, and pathogenic bacterium do not have.
Measure the essential element and the content of elements of the finished product loess of improvement, data following (unit, gram): ferrum 2.51, sodium 0.12, potassium 0.12, magnesium 0.36, boron 0.05, lithium 0.02, selenium 0.02, calcium 3.5, zinc 0.040.
The content of each element in the loess of plateau before and after relatively improveing, we find that the content of these elements does not almost change.But very big variation has taken place in the structure of plateau loess.
Embodiment 2
Select: with embodiment 1
Refinement: adopt three roller ball mill grindings, loess is ground to form the granule that particle mean size is 100nm;
Microporeization: the aqueous hydrochloric acid solution that adds the pH=4 of plateau loess quality 30% stirs, and makes the loess aquation, then at 120 ℃ of following evaporative removal moisture, makes the loess particle surface have a large amount of micropore (the micropore average diameter is 10nm).
Sterilization: adopt disinfection by ultraviolet light to remove detrimental microorganisms, promptly get the plateau loess of improveing.
The content (unit, gram) of each element in per 100 grams of this loess: ferrum 4.51, sodium 0.72, potassium 0.52, magnesium 0.36, boron 0.15, lithium 0.22, selenium 1.12, calcium 4.5, zinc 0.14;
Get plateau loess 80 grams of above-mentioned preparation, pure water 200 grams, arabic gum 1 gram, cellulose 1 gram behind the mix homogeneously, is prepared into facial film with common process.
(every square centimeter 2 acne occur to give the more serious patient of 10 plane portion acne respectively with the facial film of this formulation, and with symptoms such as hoary hairs) use, adhere to using every day, the acne of 10 user faces disappear substantially after 20 days, and allergic phenomena do not occur.
Embodiment 3
Select: with embodiment 1
Refinement: adopt three roller ball mill grindings, loess is ground to form the granule that particle mean size is 100nm;
Microporeization: the caustic soda aqueous solution that adds the pH=9 of plateau loess quality 5% stirs, and makes the loess aquation, then at 180 ℃ of following evaporative removal moisture, makes the loess particle surface have a large amount of micropore (the micropore average diameter is 100nm).
The content (unit, gram) of each element in per 100 grams of this loess: ferrum 2.51, sodium 0.12, potassium 0.12, magnesium 0.36, boron 0.05, lithium 0.02, selenium 0.52, calcium 3.5, zinc 0.04;
Get plateau loess 80 grams of above-mentioned prepared, pure water 200 grams, arabic gum 1 gram, cellulose 1 gram behind the mix homogeneously, is prepared into facial film with common process.
Use for respectively the more serious volunteer (age is about 60 years old) of 10 plane portion wrinkles the facial film of this formulation, adhere to using every day, use after 20 days, the facial wrinkles of 10 user obviously tails off, and skin is white and moist flexible.
Embodiment 4
Select: with embodiment 1
Refinement: adopt three roller ball mill grindings, loess is ground to form the granule that particle mean size is 30nm;
Microporeization: the pure water that adds plateau loess quality 1% stirs, and makes the loess aquation, then at 165 ℃ of following evaporative removal moisture, makes the loess particle surface have a large amount of micropore (the micropore average diameter is 300nm).
The content (unit, gram) of each element in per 100 grams of this loess: ferrum 3.51, sodium 0.12, potassium 0.12, magnesium 0.36, boron 0.05, lithium 0.12, selenium 1.22, calcium 3.5, zinc 0.04;
With the plateau loess of above-mentioned prepared, the mass percent with 3% adds in the scrubbing cream.Scrubbing cream is satiny, does not hinder skin; Use back skin exquisiteness, glossy.
Embodiment 5,
Select: with embodiment 1
Refinement: adopt three roller ball mill grindings, loess is ground to form the granule that particle mean size is 30nm;
Microporeization: the pure water that adds plateau loess quality 50% stirs, and makes the loess aquation, then at 135 ℃ of following evaporative removal moisture, makes the loess particle surface have a large amount of micropore (the micropore average diameter is 300nm).
In per 100 grams of this loess, the content of each element (unit, gram):
Constituent content ferrum 3.51, sodium 0.12, potassium 0.12, magnesium 0.36, boron 0.05, lithium 0.02, selenium 0.12, calcium 3.5, zinc 2.14.
With the plateau loess of above-mentioned prepared, the mass percent with 3% adds in the bath gel, and bath gel is satiny, does not hinder skin.Use the fine and smooth China Resources of back skin, glossy.
Claims (6)
1. the processing method of plateau loess comprises following processing step:
1. select: utilize Chemical Physics Processing to remove the unhelpful composition that a kind of Qinghai-Tibet loess contains, concrete technology is as follows:
A, washing: with the water washing of 1～10 times of volume of Qinghai-Tibet loess, precipitation is collected supernatant, concentrates to remove 80～99% water and get nutritional solution, and is stand-by;
B, alkali cleaning: add alkali liquid washing in above-mentioned precipitation, the pH of control dispersion is 7.2～14, and precipitation is removed supernatant;
C, pickling: continue to add the acid solution washing in precipitation, the pH of control dispersion is 0.1～6.8, and precipitation is removed supernatant;
D, neutralization: add in the weak base and excessive acid, the pH of control dispersion is between 4～10, and precipitation is removed supernatant;
E, in precipitation, add a gained nutritional solution, moisture is removed in oven dry;
2. refinement: adopt physical method to be refined into the granule that granule is 1mm～1nm through the above-mentioned loess of selecting;
3. microporeization: add the water of plateau loess quality 5%～50%, stir, then 120 ℃～180 ℃ down evaporation remove moisture, make the loess particle surface form a large amount of micropores;
4. sterilization: adopt high temperature and/or ultraviolet to carry out disinfection, remove the harmful microorganism in the loess; Described Qinghai-Tibet loess mineral and content of elements are as follows: ferrum 0.02～5%, sodium 0.02～5%, potassium 0.02～5%, magnesium 0.02～5%, boron 0.02～5%, lithium 0.02～5%, selenium 0.02～5%, calcium 0.02～5%, zinc 0.02～5%.
2. the processing method of plateau loess according to claim 1 is characterized in that: the nutrient that adds loess weight 0.001%～30% in above-mentioned steps e; Described nutrient is any group vitamins, needed by human body trace element, protein, polypeptide, saccharide and oils and fats.
3. the plateau loess handled of method according to claim 1 is as the raw material of producing the beauty and skin care product.
4. the application of plateau as claimed in claim 3 loess in producing the beauty and skin care product: be with plateau loess: pure water: arabic gum: cellulose was with 100: 100: 1: 1～100: behind 150: 2: 2 the part by weight mix homogeneously, be prepared into facial film with common process.
5. the application of plateau as claimed in claim 3 loess in producing the beauty and skin care product: be that plateau loess is added in the scrubbing cream with 3% mass percent.
6. the application of plateau as claimed in claim 3 loess in producing the beauty and skin care product: be that plateau loess is added in the bath gel with 3% mass percent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007103055059A CN101249048B (en) | 2007-12-22 | 2007-12-22 | Elevated plain loessial processing method and applications in producing beauty treatment article |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007103055059A CN101249048B (en) | 2007-12-22 | 2007-12-22 | Elevated plain loessial processing method and applications in producing beauty treatment article |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101249048A CN101249048A (en) | 2008-08-27 |
| CN101249048B true CN101249048B (en) | 2010-12-29 |
Family
ID=39952762
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2007103055059A Active CN101249048B (en) | 2007-12-22 | 2007-12-22 | Elevated plain loessial processing method and applications in producing beauty treatment article |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101249048B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110123679A (en) * | 2019-06-18 | 2019-08-16 | 宁夏微友汇网络科技有限公司 | Bathing mud with health-care efficacy and preparation method thereof |
| CN111888310A (en) * | 2020-08-19 | 2020-11-06 | 袁海峰 | Traditional Chinese medicine solution for removing freckles and wrinkles |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1633979A (en) * | 2004-10-25 | 2005-07-06 | 段锡黎 | Salt mud extraction from liquid and solid coexisting sodium salt lake and powder making process, and its product |
-
2007
- 2007-12-22 CN CN2007103055059A patent/CN101249048B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1633979A (en) * | 2004-10-25 | 2005-07-06 | 段锡黎 | Salt mud extraction from liquid and solid coexisting sodium salt lake and powder making process, and its product |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101249048A (en) | 2008-08-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102939958B (en) | Silver-carrying shell powder antibacterial agent and preparation method thereof | |
| CN101249048B (en) | Elevated plain loessial processing method and applications in producing beauty treatment article | |
| CN101147721B (en) | Plateau red soil processing method and application in producing beautifying product | |
| CN100377700C (en) | Embossed-rod health-cave bathing-mud powder | |
| KR101250545B1 (en) | Method for manufacturing the functional toilet soap | |
| CN102242026A (en) | Skin care fancy soap | |
| CN106377455A (en) | Ice silkworm silk nanocarbon mask | |
| CN100366236C (en) | Attapulgite sea salt health-care bathing powder | |
| CN101147722B (en) | Plateau white soil processing method and application in producing beautifying product | |
| CN105456124A (en) | Grape seed whitening mask | |
| CN101239027B (en) | Plateau green clay processing method and application in producing beauty treatment article | |
| KR101260423B1 (en) | The soap of rock salt and preparation method thereof | |
| CN101011330A (en) | Mineral salt shower cream | |
| CN102085167A (en) | Preparation method of hibiscus syriacus leaf and sodium hyaluronate shampoo | |
| CN101129307B (en) | Method of processing slosh and application in producing beauty treatment skin care products of the same | |
| CN115581656A (en) | Marine organism combination-based emotion awakening iceberg gel with soothing and repairing effects and preparation method thereof | |
| CN104922043A (en) | Natural spirulina mask | |
| CN1259350A (en) | Vulcanic rock mineral face mould | |
| CN1875910A (en) | A carbon particle cream cleanser and cream mask | |
| CN105106037A (en) | Olive bubble bath salt | |
| CN102670420A (en) | Negative ion mask | |
| CN103330674A (en) | Selenium-enriched cucumber and egg white eye mask | |
| CN106430271A (en) | Bionics synthetic micron calcium carbonate particle method | |
| CN105362165A (en) | Aloe nutrient skin cream | |
| CN107374989A (en) | Application of the electrolytic reduction water in skin care item |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee |
Owner name: LANZHOU QIZHENG ECOLOGICAL HEALTH PRODUCT CO., LTD Free format text: FORMER NAME: LANZHOU QIZHENG HEALTH DAILY NECESSITIES CO., LTD. |
|
| CP03 | Change of name, title or address |
Address after: 730070, Gansu, Anning District, Lanzhou 25 Avenue No. Patentee after: Lanzhou Cheezheng ecological health products Co. Ltd. Address before: 730100 Gansu city of Lanzhou province Yuzhong Cheezheng Avenue Patentee before: Lanzhou Qizheng Health Daily Necessities Co., Ltd. |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160918 Address after: 850000, Tibet autonomous region of Lhasa City, north of Tong song Road, west of teachers' Village Patentee after: Yutuo Tibetan Medicine Research Co., Ltd., Tibet Address before: 730070, Gansu, Anning District, Lanzhou 25 Avenue No. Patentee before: Lanzhou Cheezheng ecological health products Co. Ltd. |