CN101224183A - Bioremediation hand cleaning powder and prearing method thereof - Google Patents

Bioremediation hand cleaning powder and prearing method thereof Download PDF

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Publication number
CN101224183A
CN101224183A CNA2008100468529A CN200810046852A CN101224183A CN 101224183 A CN101224183 A CN 101224183A CN A2008100468529 A CNA2008100468529 A CN A2008100468529A CN 200810046852 A CN200810046852 A CN 200810046852A CN 101224183 A CN101224183 A CN 101224183A
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China
Prior art keywords
washing
powder
percent
builder
hands
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CNA2008100468529A
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Chinese (zh)
Inventor
户业丽
程波
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Wuhan Institute of Technology
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Wuhan Institute of Technology
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Priority to CNA2008100468529A priority Critical patent/CN101224183A/en
Publication of CN101224183A publication Critical patent/CN101224183A/en
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Abstract

The invention relates to a biological restorative powder hand cleaner and a preparation method thereof. The powder hand cleaner consists of 65 percent-80 percent of detergency builder, 1.0 percent-5.0 percent of aloe juice, 5 percent-20 percent of surfactant, 1 percent-10 percent of humectant, 5 percent-20 percent of water and 0.1 percent-1 percent of natural perfume, which are mixed. The water, the humectant, the aloe juice, the surfactant and the natural perfume are mixed and dissolved, and the detergency builder is added into the mixture and evenly stirred, thus acquiring the biological restorative wet powder hand cleaner. The invention has the advantages of 1) wet powder property, water solubility, neutrality, no irritation, capability of eliminating heavy-duty greasy dirt with or without water with remarkable efficiency; 2) that the aloe juice is added, so that injury skin can be restored and the cleaned hands are smooth.3) and that modified starch of renewable resource is adopted as the detergency builder, which is environment friendly.

Description

A kind of biological restoration type powder and preparation method thereof of washing one's hands
Technical field
The present invention relates to a kind of heavy-dirty liquid-detergent, concrete a kind of biological restoration type powder and preparation method thereof of washing one's hands that relates to can have under water or the anhydrous condition removing fast reach the greasy dirt on implements surface on hand.
Background technology
The anhydrous hand cleaner powder mainly adopts dual mode at present: first kind of mode is to adopt sawdust or water-insoluble natural fiber to mix with detergent, for example Chinese patent communique CN1385510 discloses a kind of hand-washing powder, it comprises detergent, bagasse powder and wood powder, the second way is the surfactant dodecylbenzene sodium sulfonate to be cooperated with sodium carbonate, sodium silicate etc. form, for example Chinese patent communique CN1241625 discloses a kind of hand-washing powder, and its composition includes Radix Glycyrrhizae, Semen arachidis hypogaeae, dodecylbenzene sodium sulfonate etc.Above-mentioned two kinds of hand-washing powders are the alkalescence prescription, and skin is had certain stimulation.
Summary of the invention
Problem to be solved by this invention is to propose a kind of biological restoration type powder of washing one's hands at above-mentioned prior art, and is little to skin injury, and can repair the skin of damage.
Another object of the present invention is to propose the wash one's hands preparation method of powder of biological restoration type.
The present invention is adopted solution to be by the problem of the above-mentioned proposition of solution: a kind of biological restoration type powder of washing one's hands, it is characterized in that including builder, aloe juice, surfactant, wetting agent, water, natural essence, form through mixed preparing, its constituent content is by mass percentage:
Builder 65%-80% aloe juice 1.0%-5.0% surfactant 5%-20%
Wetting agent 1%-10% water 5%-20% natural essence 0.1%-1%.
Press such scheme, the preparation method of described modified starch is: take by weighing starch 50.0g, add entry 50-200mL, the furnishing pulpous state, be heated to 20 ℃-40 ℃, transfer pH to 5-10 with diluted sodium hydroxide solution, by the 5%-20% adding oxidant of amount of starch, insulated and stirred reaction 1-5h, add the sodium sulfite solution that accounts for oxidant 8%-10%, remove unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white.
Press such scheme, described oxidant is selected from any one in hydrogen peroxide, potassium permanganate or the sodium hypochlorite.
Press such scheme, described surfactant is the mixture of any one or they in anionic polyoxyethylenated alcohol sodium sulfate (AES), nonionic fatty alcohol-polyoxyethylene ether (AEO), the NPE (TX-10).
Press such scheme, described wetting agent is any one among glycerol, ethylene glycol or the PEG400.
Press such scheme, described builder is modified starch and the Natrii Sulfas mixture by mass ratio 1: 3-8.
The wash one's hands technical scheme of powder, preparation method thereof of described biological restoration type is characterized in that including following steps:
1) preparation of modified starch: take by weighing starch 50.0g, add entry 50-200mL, the furnishing pulpous state is heated to 20 ℃-40 ℃, transfers pH5-10 with diluted sodium hydroxide solution, 5%-20% by amount of starch adds oxidant, insulated and stirred reaction 1-5h adds the sodium sulfite solution that accounts for oxidant content 8%-10%, removes unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white;
2) preparation of aloe juice: get fresh aloe leaf 1000g, clean up, chopping obtains aloe juice with milling process ,-4 ℃ of preservations;
3) preparation of builder: Natrii Sulfas was ground the 40-80 mesh sieve, and with above-mentioned steps 1) modified starch of gained is by mass ratio 3-8: 1 mixes, and obtains builder;
4) be mixed with: get material by following mass percent, aloe juice 1.0%-5.0%, builder 65%-80%, surfactant 5%-20%, wetting agent 1%-10%, water 5%-20%, natural essence 0.1%-1%, with water, wetting agent, aloe juice, surfactant, natural essence mixed dissolution, again builder is added stirring and evenly mixing, promptly get the powdered biological restoration type that the wets powder of washing one's hands.
Advantage of the present invention:
1) the biological restoration type of the present invention powder of washing one's hands is a wet-milling shape, water-soluble, neutral, has no stimulation, and can remove heavy dirty greasy dirt under water or the anhydrous condition having, and degreasing result is remarkable.
2) owing to added aloe juice, can repair, and make the back feel of washing one's hands satiny the skin of damage.
3) the present invention has adopted the Renewable resource modified starch as builder, and is environmentally friendly.
The specific embodiment
The invention will be further described below in conjunction with embodiment.
Embodiment 1:
The biological restoration type powder, preparation method thereof of washing one's hands includes following steps:
1) preparation of modified starch: take by weighing starch 50.0g, add entry 50mL, the furnishing pulpous state is heated to 20, transfers pH5 with diluted sodium hydroxide solution, add oxidant (hydrogen peroxide) by 5% of amount of starch, insulated and stirred reaction 1h adds 8% the sodium sulfite solution that accounts for oxidant content, removes unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white;
2) preparation of aloe juice: get fresh aloe leaf 1000g, clean up, chopping obtains aloe juice with milling process ,-4 ℃ of preservations;
3) preparation of builder: Natrii Sulfas was ground 40 mesh sieves, and with above-mentioned steps 1) modified starch of gained mixes by mass ratio at 3: 1, obtains builder;
4) get material by following mass percent: aloe juice 4%, builder 75%, polyoxyethylenated alcohol sodium sulfate (AES) 7%, ethylene glycol 3%, water 10%, natural essence 1% is with water, wetting agent, aloe juice, surfactant, natural essence mixed dissolution, again builder is added stirring and evenly mixing, promptly get the powdered biological restoration type that the wets powder of washing one's hands.
Embodiment 2
The biological restoration type powder, preparation method thereof of washing one's hands includes following steps:
1) preparation of modified starch: take by weighing starch 50.0g, add entry 150mL, the furnishing pulpous state is heated to 30 ℃, transfers pH7 with diluted sodium hydroxide solution, add oxidant (potassium permanganate) by 15% of amount of starch, insulated and stirred reaction 3h adds 9% the sodium sulfite solution that accounts for oxidant content, removes unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white;
2) preparation of aloe juice: get fresh aloe leaf 1000g, clean up, chopping obtains aloe juice with milling process ,-4 ℃ of preservations;
3) preparation of builder: Natrii Sulfas was ground 60 mesh sieves, and with above-mentioned steps 1) modified starch of gained mixes by mass ratio at 6: 1, obtains builder;
4) get material by following mass percent: aloe juice 5%, builder 65%, NPE (TX-10) 20%, PEG400 4.5%, water 5%, natural essence 0.5% is with water, wetting agent, aloe juice, surfactant, natural essence mixed dissolution, again builder is added stirring and evenly mixing, promptly get the powdered biological restoration type that the wets powder of washing one's hands.
Embodiment 3
The biological restoration type powder, preparation method thereof of washing one's hands includes following steps:
1) preparation of modified starch: take by weighing starch 50.0g, add entry 200mL, the furnishing pulpous state is heated to 40 ℃, transfers pH10 with diluted sodium hydroxide solution, add oxidant (sodium hypochlorite) by 20% of amount of starch, insulated and stirred reaction 5h adds 10% the sodium sulfite solution that accounts for oxidant content, removes unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white;
2) preparation of aloe juice: get fresh aloe leaf 1000g, clean up, chopping obtains aloe juice with milling process ,-4 ℃ of preservations;
3) preparation of builder: Natrii Sulfas was ground 80 mesh sieves, and with above-mentioned steps 1) modified starch of gained mixes by mass ratio at 8: 1, obtains builder;
4) get material by following mass percent: aloe juice 5%, builder 70%, fatty alcohol-polyoxyethylene ether (AEO) 10%, glycerol 5.2%, water 9%, natural essence 0.8% is with water, wetting agent, aloe juice, surfactant, natural essence mixed dissolution, again builder is added stirring and evenly mixing, promptly get the powdered biological restoration type that the wets powder of washing one's hands.
Embodiment 4
The biological restoration type powder, preparation method thereof of washing one's hands includes following steps:
1) preparation of modified starch: take by weighing starch 50.0g, add entry 180mL, the furnishing pulpous state is heated to 35 ℃, transfers pH9 with diluted sodium hydroxide solution, add oxidant (sodium hypochlorite) by 16% of amount of starch, insulated and stirred reaction 1h adds 8% the sodium sulfite solution that accounts for oxidant content, removes unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white;
2) preparation of aloe juice: get fresh aloe leaf 1000g, clean up, chopping obtains aloe juice with milling process ,-4 ℃ of preservations;
3) preparation of builder: Natrii Sulfas was ground 50 mesh sieves, and with above-mentioned steps 1) modified starch of gained mixes by mass ratio at 6: 1, obtains builder;
4) get material by following mass percent: aloe juice 4%, builder 80%, polyoxyethylenated alcohol sodium sulfate (AES) 4%, fatty alcohol-polyoxyethylene ether (AEO) 4%, glycerol 3.2%, water 4%, natural essence 0.8% is with water, wetting agent, aloe juice, surfactant, natural essence mixed dissolution, again builder is added stirring and evenly mixing, promptly get the powdered biological restoration type that the wets powder of washing one's hands.

Claims (7)

1. biological restoration type powder of washing one's hands is characterized in that including builder, aloe juice, surfactant, wetting agent, water, natural essence, forms through mixed preparing, and its constituent content is by mass percentage:
Builder 65%-80% aloe juice 1.0%-5.0% surfactant 5%-20%
Wetting agent 1%-10% water 5%-20% natural essence 0.1%-1%.
2. by the described biological restoration type of claim 1 powder of washing one's hands, the preparation method that it is characterized in that described modified starch is: take by weighing starch 50.0g, add entry 50-200mL, the furnishing pulpous state, be heated to 20 ℃-40 ℃, transfer pH to 5-10 with diluted sodium hydroxide solution, 5%-20% by amount of starch adds oxidant, insulated and stirred reaction 1-5h, add the sodium sulfite solution that accounts for oxidant 8%-10%, remove unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white.
3. by the described biological restoration type of claim 2 powder of washing one's hands, it is characterized in that described oxidant is selected from any one in hydrogen peroxide, potassium permanganate or the sodium hypochlorite.
4. by the described biological restoration type of claim 1 powder of washing one's hands, it is characterized in that described surfactant is the mixture of any one or they in anionic polyoxyethylenated alcohol sodium sulfate, nonionic fatty alcohol-polyoxyethylene ether, the NPE.
5. by claim 1 or the 3 or 4 described biological restoration types powder of washing one's hands, it is characterized in that described wetting agent is any one among glycerol, ethylene glycol or the PEG400.
6. by claim 1 or the 3 or 4 described biological restoration types powder of washing one's hands, it is characterized in that described builder is modified starch and the Natrii Sulfas mixture by mass ratio 1: 3-8.
7. the described biological restoration type of claim 1 powder, preparation method thereof of washing one's hands is characterized in that including following steps:
1) preparation of modified starch: take by weighing starch 50.0g, add entry 50-200mL, the furnishing pulpous state is heated to 20 ℃-40 ℃, transfers pH5-10 with diluted sodium hydroxide solution, 5%-20% by amount of starch adds oxidant, insulated and stirred reaction 1-5h adds the sodium sulfite solution that accounts for oxidant content 8%-10%, removes unreacted oxidant, pass through filtration, washing, drying again, obtain pale yellow modified starch to white;
2) preparation of aloe juice: get fresh aloe leaf 1000g, clean up, chopping obtains aloe juice with milling process ,-4 ℃ of preservations;
3) preparation of builder: Natrii Sulfas was ground the 40-80 mesh sieve, and with above-mentioned steps 1) modified starch of gained is by mass ratio 3-8: 1 mixes, and obtains builder;
4) be mixed with: get material by following mass percent, aloe juice 1.0%-5.0%, builder 65%-80%, surfactant 5%-20%, wetting agent 1%-10%, water 5%-20%, natural essence 0.1%-1%, with water, wetting agent, aloe juice, surfactant, natural essence mixed dissolution, again builder is added stirring and evenly mixing, promptly get the powdered biological restoration type that the wets powder of washing one's hands.
CNA2008100468529A 2008-02-01 2008-02-01 Bioremediation hand cleaning powder and prearing method thereof Pending CN101224183A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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CN101224183A true CN101224183A (en) 2008-07-23

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103893044A (en) * 2012-12-28 2014-07-02 青岛锦涟鑫商贸有限公司 Method for preparing nontoxic liquid soap
CN104288001A (en) * 2014-09-11 2015-01-21 东莞市和生环保科技开发有限公司 Hand wash capable of powerfully removing oil and protecting skin

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103893044A (en) * 2012-12-28 2014-07-02 青岛锦涟鑫商贸有限公司 Method for preparing nontoxic liquid soap
CN104288001A (en) * 2014-09-11 2015-01-21 东莞市和生环保科技开发有限公司 Hand wash capable of powerfully removing oil and protecting skin
CN104288001B (en) * 2014-09-11 2017-07-18 东莞市和生环保科技开发有限公司 A kind of potent oil removing skin care hand cleaning liquid

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Open date: 20080723