CN101220257A - Process for producing vehicle glass antifogging agent - Google Patents
Process for producing vehicle glass antifogging agent Download PDFInfo
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- CN101220257A CN101220257A CNA2007100131440A CN200710013144A CN101220257A CN 101220257 A CN101220257 A CN 101220257A CN A2007100131440 A CNA2007100131440 A CN A2007100131440A CN 200710013144 A CN200710013144 A CN 200710013144A CN 101220257 A CN101220257 A CN 101220257A
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Abstract
The invention relates to a method for preparing an automobile glass antifoggant, wherein deionized water is added into a reaction kettle, and 0.1-0.6 percent of high molecular filmogen is added, heated to 40 DEG C, and agitated until dissolved, then 0.6-4.0 percent of fatty alcohol polyethenoxy ether or nonyl phenol polyethenoxy ether nonionics, 0.1-0.6 percent of coconut fatty alkyl trimethyl chloride or lauryl amphoteric propyl juanacidate cationic surfactant, and 0.2-1.0 percent mono ethanol amine or trolamine acidity modifier are added orderly; finally, 5.0-30 percent of isopropyl alcohol, ethanol, propanediol, and propanetriol are added, evenly agitated until the temperature lowers to the room temperature, and then the glass antifoggant is obtained. The method has the advantages that the use is simple; the glass atomizing effect is good; dust can not be absorbed on the surface of the glass after the drying process, and no trace is left on the surface; the product is colorless and flavorless, safe and reliable.
Description
Technical field:
The present invention relates to a kind of compound method, belong to filed of daily-use chemical industry with macromolecule film former and bioactive agent composition anti-fog agent for wind-screen of automobile thereof.
Technical background:
Automobile has the electric heating anti-fog device on the front windshield of high-grade car at present, the windshield glass of its side window, rear window and general automobile such as passenger vehicle, agricultural vehicle, truck does not all have anti-smog device, inside and outside the vehicle temperature difference is arranged so in the winter time, or when rainy day, humidity was bigger, airborne water vapour is met cold meeting and is condensed at glass surface, make the glass surface atomizing, when windshield atomizes, can have a strong impact on pilot's line of vision.At present, existing a small amount of glass antidimmer product on the market, majority is the bottling liquid product, need during use to be sprayed onto antifogging agent on glass earlier or to be sprayed onto on the paper handkerchief, smear evenly with clean paper or napkin then, till polishing, exist and carry and use inconvenience, easily stain positions such as automotive seat, car panel during sprinkling, and the antifog time is short and effect is bad, leaves a trace easily after dried and adsorb dust.
Summary of the invention:
The objective of the invention is to overcome the deficiency that existing automobile antifogging agent exists, a kind of new automobile glass antidimmer preparation method is provided, more effectively reach anti-fog effect.
To achieve these goals, the deionized water that the present invention gets metering adds in the reactor, add 0.1~0.6% (mass percent) macromolecule film former, be heated to 40 ℃ and stirring and dissolving, add 0.6~4.0% fatty alcohol-polyoxyethylene ether or polyoxyethylene nonylphenol ether nonionogenic tenside then successively, 0.1~0.6% coco alkyl trimethyl ammonium chloride or lauryl both sexes propyl group sulfonate cats product, 0.2~1.0% monoethanolamine or trolamine acidity regulator, add 5.0~30% Virahols at last, ethanol, propylene glycol, glycerol stirs and reduces to room temperature and promptly get glass antidimmer.
The present invention has easy to carry, uses simply, and during glass atomization, wiping can be antifog conveniently, and the not only antifog time is long, and the glass transparent degree is good; Add the cation surface activating composition, antistatic effect is strong, and dry back glass surface does not adsorb dust, leaves no trace; The product colorless and odorless, safe and reliable.
Specific embodiments:
The present invention can be specifically described its preparation method by following examples:
Embodiment 1: quality %
Fatty alcohol-polyoxyethylene ether (AEO-9) 1.0~4.0%
Lauryl both sexes propyl group sulfonate 0.2~0.6%
Ethanol 6~15%
Glycerol 6~20%
Trolamine 0.2~2.0%
Virahol 1.0~5%
Polyoxyethylene glycol (800) 0.1~0.6%
Deionized water~100%
The deionized water of getting metering adds in the reactor, add 0.2% macromolecule film former polyoxyethylene glycol (800) and be heated to 40 ℃ and stirring and dissolving, the nonionogenic tenside that adds 2.0% fatty alcohol-polyoxyethylene ether (AEO-9) then successively, the cats product of 0.3% lauryl both sexes propyl group sulfonate, add 8% ethanol, 10% glycerol and 2.0% Virahol, add 0.5% acidity regulator trolamine at last, transferring pH value of solution is neutrality or slightly acidic, stirs to reduce to room temperature and promptly get the glass antifogging anti agent solution.
Embodiment 2: quality %
Polyoxyethylene nonylphenol ether (OP-10) 1~4%
Coco alkyl trimethyl ammonium chloride 0.2~0.6%
Ethanol 6~15%
Glycerol 6~20%
Trolamine 0.5~1.5%
Virahol 1~5%
Polyvinylpyrrolidone 0.1~0.6%
Deionized water~100%
The deionized water of getting metering adds in the reactor, add 0.2% macromolecule film former polyvinylpyrrolidone, be heated to 40 ℃ and stirring and dissolving, the nonionogenic tenside that adds 2% polyoxyethylene nonylphenol ether then successively, the cats product of 0.2% coco alkyl trimethyl ammonium chloride, add 8% ethanol, 10% glycerol and 2% Virahol, add 1% acidity regulator trolamine at last, transferring pH value of solution is neutrality or slightly acidic, stirs to reduce to room temperature and promptly get the glass antifogging anti agent solution.
Claims (2)
1. the preparation method of an anti-fog agent for wind-screen of automobile is to carry out in the reactor of routine, and it is molten to it is characterized in that adding deionized water, macromolecule film former polyoxyethylene glycol (800) or polyvinylpyrrolidone heated and stirred; Adding fatty alcohol-polyoxyethylene ether nonionogenic tenside, lauryl both sexes propyl group sulfonate cats product, ethanol, glycerol and Virahol then successively stirs, add the acidity regulator trolamine at last, making pH is neutrality or slightly acidic, stirs to reduce to room temperature and promptly get the glass antifogging anti agent solution.
2. the preparation method of a kind of anti-fog agent for wind-screen of automobile according to claim 1 is characterized in that cats product lauryl both sexes propyl group sulfonate or coco alkyl trimethyl ammonium chloride are 0.2~0.6%; Macromolecule film former polyoxyethylene glycol (800) or polyvinylpyrrolidone 0.1~0.6%.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007100131440A CN101220257B (en) | 2007-01-09 | 2007-01-09 | Process for producing vehicle glass antifogging agent |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007100131440A CN101220257B (en) | 2007-01-09 | 2007-01-09 | Process for producing vehicle glass antifogging agent |
Publications (2)
Publication Number | Publication Date |
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CN101220257A true CN101220257A (en) | 2008-07-16 |
CN101220257B CN101220257B (en) | 2010-09-01 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN2007100131440A Expired - Fee Related CN101220257B (en) | 2007-01-09 | 2007-01-09 | Process for producing vehicle glass antifogging agent |
Country Status (1)
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CN (1) | CN101220257B (en) |
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2011066718A1 (en) * | 2009-12-01 | 2011-06-09 | The Hong Kong University Of Science And Technology | Compositions containing thermally-induced self-assembly of nonionic surfactants and their application in smart glass technologies |
CN102241960A (en) * | 2011-05-13 | 2011-11-16 | 上海大学 | Antifog bactericide for automobile window |
CN102850998A (en) * | 2012-08-30 | 2013-01-02 | 苏州市德莱尔建材科技有限公司 | Corrosion-resistant glass antifogging agent |
CN102936487A (en) * | 2012-11-29 | 2013-02-20 | 大连创达技术交易市场有限公司 | Preparation method of automotive glass antifogging agent |
CN103409110A (en) * | 2013-08-20 | 2013-11-27 | 南通市通州区益君劳务有限公司 | Cleaning and antifogging agent for glass |
CN103602314A (en) * | 2013-12-04 | 2014-02-26 | 宁波赛茵特科技服务有限公司 | Normal temperature type automobile glass fog remover |
CN103709994A (en) * | 2013-12-04 | 2014-04-09 | 宁波赛茵特科技服务有限公司 | Low-temperature-type automobile glass fog remover |
CN103740333A (en) * | 2013-11-27 | 2014-04-23 | 南通晶鑫光学玻璃有限公司 | Long-acting decontamination anti-fog agent for glass, and preparation method thereof |
CN105713575A (en) * | 2016-04-05 | 2016-06-29 | 四川理工学院 | Long-acting anti-fog agent for automotive glass and preparation method of anti-fog agent |
CN106350290A (en) * | 2016-08-23 | 2017-01-25 | 余姚市德派日用品有限公司 | Concentrated glass cleaning product and preparation method thereof |
CN107022342A (en) * | 2017-05-31 | 2017-08-08 | 江苏精盾节能科技有限公司 | A kind of glass antidimmer and preparation method thereof |
CN107083234A (en) * | 2017-05-23 | 2017-08-22 | 句容耀皮节能玻璃科技发展有限公司 | A kind of automobile glass anti-fog antifreezing agent and preparation method thereof |
CN109762521A (en) * | 2019-01-08 | 2019-05-17 | 杨记周 | A kind of new-energy automobile antifoggant and preparation method thereof |
CN110066639A (en) * | 2019-04-17 | 2019-07-30 | 上海和黄白猫有限公司 | A kind of anti-scratch type glass antidimmer and preparation method thereof |
CN110359284A (en) * | 2019-08-08 | 2019-10-22 | 广州市泰克斯乐科技有限公司 | A kind of collar of yarn and its application with anti-fog effect |
CN117089179A (en) * | 2023-09-11 | 2023-11-21 | 佛山赛和薄膜科技有限公司 | High-transmittance low-fog optical base film and preparation method thereof |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1030201C (en) * | 1991-09-04 | 1995-11-01 | 黄标春 | Anti-fog agent |
CN1208754A (en) * | 1997-08-14 | 1999-02-24 | 张志贤 | Agent for application glass surface to minimize adherence of ice or mist, and prepn. method therefor |
CN100360632C (en) * | 2003-08-18 | 2008-01-09 | 侯宏森 | Multifunctional long-effect environmental protective glass antifogging defrosting agent |
CN1557904A (en) * | 2004-01-18 | 2004-12-29 | 上海师范大学 | Composition for prevention of vapor fogging on the surface of glass |
-
2007
- 2007-01-09 CN CN2007100131440A patent/CN101220257B/en not_active Expired - Fee Related
Cited By (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102892834B (en) * | 2009-12-01 | 2014-07-30 | 香港科技大学 | Compositions containing thermally-induced self-assembly of nonionic surfactants and their application in smart glass technologies |
CN102892834A (en) * | 2009-12-01 | 2013-01-23 | 香港科技大学 | Compositions containing thermally-induced self-assembly of nonionic surfactants and their application in smart glass technologies |
WO2011066718A1 (en) * | 2009-12-01 | 2011-06-09 | The Hong Kong University Of Science And Technology | Compositions containing thermally-induced self-assembly of nonionic surfactants and their application in smart glass technologies |
CN102241960B (en) * | 2011-05-13 | 2013-05-08 | 上海大学 | Antifog bactericide for automobile window |
CN102241960A (en) * | 2011-05-13 | 2011-11-16 | 上海大学 | Antifog bactericide for automobile window |
CN102850998B (en) * | 2012-08-30 | 2014-05-14 | 苏州市德莱尔建材科技有限公司 | Corrosion-resistant glass antifogging agent |
CN102850998A (en) * | 2012-08-30 | 2013-01-02 | 苏州市德莱尔建材科技有限公司 | Corrosion-resistant glass antifogging agent |
CN102936487A (en) * | 2012-11-29 | 2013-02-20 | 大连创达技术交易市场有限公司 | Preparation method of automotive glass antifogging agent |
CN103409110A (en) * | 2013-08-20 | 2013-11-27 | 南通市通州区益君劳务有限公司 | Cleaning and antifogging agent for glass |
CN103740333A (en) * | 2013-11-27 | 2014-04-23 | 南通晶鑫光学玻璃有限公司 | Long-acting decontamination anti-fog agent for glass, and preparation method thereof |
CN103602314A (en) * | 2013-12-04 | 2014-02-26 | 宁波赛茵特科技服务有限公司 | Normal temperature type automobile glass fog remover |
CN103709994A (en) * | 2013-12-04 | 2014-04-09 | 宁波赛茵特科技服务有限公司 | Low-temperature-type automobile glass fog remover |
CN103709994B (en) * | 2013-12-04 | 2015-09-16 | 宁波保税区安德利斯机械有限公司 | The agent of a kind of low temperature modification removing fog on automobile glass |
CN103602314B (en) * | 2013-12-04 | 2015-09-16 | 宁波保税区安德利斯机械有限公司 | The agent of a kind of normal temperature type removing fog on automobile glass |
CN105713575A (en) * | 2016-04-05 | 2016-06-29 | 四川理工学院 | Long-acting anti-fog agent for automotive glass and preparation method of anti-fog agent |
CN106350290A (en) * | 2016-08-23 | 2017-01-25 | 余姚市德派日用品有限公司 | Concentrated glass cleaning product and preparation method thereof |
CN107083234A (en) * | 2017-05-23 | 2017-08-22 | 句容耀皮节能玻璃科技发展有限公司 | A kind of automobile glass anti-fog antifreezing agent and preparation method thereof |
CN107022342A (en) * | 2017-05-31 | 2017-08-08 | 江苏精盾节能科技有限公司 | A kind of glass antidimmer and preparation method thereof |
CN109762521A (en) * | 2019-01-08 | 2019-05-17 | 杨记周 | A kind of new-energy automobile antifoggant and preparation method thereof |
CN110066639A (en) * | 2019-04-17 | 2019-07-30 | 上海和黄白猫有限公司 | A kind of anti-scratch type glass antidimmer and preparation method thereof |
CN110359284A (en) * | 2019-08-08 | 2019-10-22 | 广州市泰克斯乐科技有限公司 | A kind of collar of yarn and its application with anti-fog effect |
CN117089179A (en) * | 2023-09-11 | 2023-11-21 | 佛山赛和薄膜科技有限公司 | High-transmittance low-fog optical base film and preparation method thereof |
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Granted publication date: 20100901 Termination date: 20110109 |