CN101191064A - Novel production device for biological diesel oil - Google Patents

Novel production device for biological diesel oil Download PDF

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Publication number
CN101191064A
CN101191064A CNA2006101343061A CN200610134306A CN101191064A CN 101191064 A CN101191064 A CN 101191064A CN A2006101343061 A CNA2006101343061 A CN A2006101343061A CN 200610134306 A CN200610134306 A CN 200610134306A CN 101191064 A CN101191064 A CN 101191064A
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oil
reactor
diesel
equipment
molecular sieve
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赵文祥
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00Technologies relating to oil refining and petrochemical industry
    • Y02P30/20Technologies relating to oil refining and petrochemical industry using bio-feedstock

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Abstract

The invention discloses novel production equipment for bio-diesel and belongs to the new energy manufacturing equipment. In the prior art, the equipment for producing the bio-diesel has large quantity and large investment, comprises a boiler, two reactors, two clarifying tanks, two conical kettles and a plurality of oil pumps, and has single use. The invention is characterized in that: 1. the equipment has less quantity (see Figure 1), one reactor has multiple uses, the equipment can produce bio-diesel, waste machine oil and diesel abstracted from mineral crude oil. 2. Oil gas can be reclaimed when the mineral crude oil is abstracted. 3. The waste heat can be recycled and the energy can be saved. 4. A water type smoke extraction dust remover is designed, contributes to environmental protection and has no pollution. The invention can be widely used in producing bio-diesel, waste machine oil, crude oil refining and so on.

Description

Novel production device for biological diesel oil
Novel production device for biological diesel oil belongs to the new forms of energy producing apparatus.As shown in Figure 1.
In the technology that oneself has, production biofuel equipment is many, and investment is big, and boiler is arranged, 2 of reactors, and 2 of slurry tanks, the taper still is a plurality of, many in oil pump, the equipment purposes is single can not many use.
Characteristics of the present invention: 1. equipment is few, a stove multiple use.But the production biofuel, refining used oil, refining mineral crude oil.
2. light gold-plating divides gas and 400 ℃ later on heavy gold-platings to divide rich gas all recyclable utilization when refining mineral crude oil.
3. make a heat-eliminating medium with stock oil (soya-bean oil), reclaimed the saving of heat energy.
4. ability of swimming smoking fly-ash separator is overlapped in combustion heat supplying system design one, no black smoke pollution compliance with environmental protection requirements, and this equipment can be widely used in production of biodiesel, the renewable oil refining of biomass, mineral crude oil refinery ... etc. purposes.
One, novel production device for biological diesel oil structure: as shown in Figure 1
(1) thermometer (2) tank contents gauge (3) reactor (4) oil hole (5) manhole (6) molecule screen cloth (7) load hole (8) zeolite molecular sieve (9) finestiller (10) oil vapour outlet pipe (11) ring flange (12) residual oil outlet valve (13) water cooler (14) cooling water tank (15) is observed cup (16) diversion cans (17) oil outlet pipe (18) processed oil storage tank (19) liquid separatnig valve (20) stalk carbon (or hard coal) (21) fire bars (22) vacuum pump (23) waste heat recovery cover (24) agitator.
Two, equipment work principle:
Production biofuel equipment work principle:
Earlier with methyl alcohol CH 3OH, add-on 20%, with catalyzer sodium hydroxide NaOH add-on 1%, pump in (3) reactor from (4) oil hole, treat sodium hydroxide dissolve after with vegetables oil (as soya-bean oil) add-on 80%, pump in (3) reactor from (4) oil hole, observe (2) tank contents gauge, pasta stops charging to (3) reactor 2/3 position.Light (20) the stalk carbon on (21) fire bars, the temperature of (3) reactor is raised to 70 ℃-80 ℃, open (24) agitator, keep constant temperature, reaction pressure is controlled at 0.1-0.5Mpa reaction 2-3 hour, soya-bean oil and methyl alcohol CH in the reactor 3OH generates fatty acid methyl ester (biofuel) and glycerine under catalyzer sodium hydroxide NaOH effect.Soya-bean oil rate of recovery 95%-98%.
Reaction formula:
Figure A20061013430600041
Soya-bean oil methyl alcohol glycerine fatty acid methyl esters
Then pump into 1%, 70 ℃ of hot water of oil quality, stir while adding from (4) oil hole, 10 minutes static 2 hours, open (12) residual oil outlet valve, emit glycerol liquor, tinning in addition.
A part there is not the methanol vapor of reaction in (3) reactor reaction process, through the cooled methyl alcohol CH of (9) finestiller (10) oil gas outlet pipe (13) water cooler 3OH liquid flow into (16) diversion cans and emits recycling from (19) liquid separatnig valve.
Fatty acid methyl ester remaining in (3) reactor is warmed up to 105 ℃-120 ℃, open (22) vacuum pump and carry out drying and dehydrating, water vapour enters (9) finestiller (13) water cooler in the reactor, and cooled water flow into (16) diversion cans, emits from (19) liquid separatnig valve.
Emitting fatty acid methyl ester from (12) residual oil outlet valve of (3) reactor at last promptly is the biofuel that we produce to the finished product jar.
Embodiment:
Lard system biofuel
Earlier with methyl alcohol CH 3OH, add-on 20%, with catalyzer sodium hydroxide NaOH add-on 1%, pump in (3) reactor from (4) oil hole, treat sodium hydroxide dissolve after with animal oil (as lard) add-on 80%, pump in (3) reactor from (4) oil hole, observe (2) tank contents gauge, pasta stops charging to (3) reactor 2/3 position.Light (20) the stalk carbon on (21) fire bars, the temperature of (3) reactor is raised to 70 ℃-80 ℃, open (24) agitator, keep constant temperature, reaction pressure is controlled at 0.1-0.5Mpa reaction 2-3 hour, lard and methyl alcohol CH in the reactor 3OH generates fatty acid methyl ester (biofuel) and glycerine under catalyzer sodium hydroxide NaOH effect.Lard rate of recovery 95%-98%.
Reaction formula:
Figure A20061013430600051
Lard methyl alcohol glycerine fatty acid methyl esters
Then pump into 1%, 70 ℃ of hot water of oil quality, stir while adding from (4) oil hole, 10 minutes static 2 hours, open (12) residual oil outlet valve, emit glycerol liquor, tinning in addition.
A part there is not the methanol vapor of reaction in (3) reactor reaction process, through the cooled methyl alcohol CH of (9) finestiller (10) oil gas outlet pipe (13) water cooler 3OH liquid flow into (16) diversion cans and emits recycling from (19) liquid separatnig valve.
Fatty acid methyl ester remaining in (3) reactor is warmed up to 105 ℃-120 ℃, open (22) vacuum pump and carry out drying and dehydrating, water vapour enters (9) finestiller (13) water cooler in the reactor, and cooled water flow into (16) diversion cans, emits from (19) liquid separatnig valve.
Emitting fatty acid methyl ester from (12) residual oil outlet valve of (3) reactor at last promptly is the biofuel that we produce to the finished product jar.

Claims (7)

1. novel production device for biological diesel oil is constructed:
(1) thermometer (2) tank contents gauge (3) reactor (4) oil hole (5) manhole (6) molecule screen cloth (7) load hole (8) zeolite molecular sieve (9) finestiller (10) oil vapour outlet pipe (11) ring flange (12) residual oil outlet valve (13) water cooler (14) cooling water tank (15) is observed cup (16) diversion cans (17) oil outlet pipe (18) processed oil storage tank (19) liquid separatnig valve (20) stalk carbon (or hard coal) (21) fire bars (22) vacuum pump (23) waste heat recovery cover (24) agitator.
2. said according to claim 1, feature (1) thermometer is used for the temperature of oil in indication (3) reactor altogether.(2) tank contents gauge is used for showing pack into the height of pasta of (3) reactor.(4) oil hole is used to inject stock oil.(5) manhole is used for maintenance.
3. said according to claim 1, be characterised in that altogether (6) molecule screen cloth is used to adorn molecular sieve for the Stainless Steel Wire material.(7) load hole is used for changing the threading zeolite molecular sieve.(9) finestiller is analysed with the thick stainless steel of 5mm and is made, and is used for oily the making with stainless steel tube with (10) oil vapour outlet pipe of distillation and is used for the oil vapour outflow.
4. said according to claim 1, it is characterized in that (8) zeolite molecular sieve has two effects, one is that the long demolase of grease is become short carbon chain.Another is to guarantee the reflux ratio of oil when distillation, improves oil quality.
5. said according to claim 1, it is characterized in that (13) water cooler is made with ф 30mm stainless steel to make oil vapour be cooled to liquid.(14) cooling water tank is made with common 5mm Plate Steel, is used to adorn water coolant.(15) observing cup, is glass material, how much is used to observe out oil quality quality and quantity.
6. said according to claim 1, it is characterized in that (19) liquid separatnig valve, be used to emit (16) and distribute pot liquid.(21) the fire bars material is an ironcasting, is used to the usefulness of charging.
7. said according to claim 1, it is characterized in that (22) vacuum pump is used for reduced pressure distillation, save energy.(23) waste heat recovery is applied mechanically the general steel pipe of ф 30mm diameter and is made, and is used for fuel oil preheating and reclaims the energy, plays a refrigerative effect in addition again.(24) agitator reaches the purpose that mixes with the stock oil that stirs in (3) reactor.
CNA2006101343061A 2006-11-20 2006-11-20 Novel production device for biological diesel oil Pending CN101191064A (en)

Priority Applications (1)

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CNA2006101343061A CN101191064A (en) 2006-11-20 2006-11-20 Novel production device for biological diesel oil

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Application Number Priority Date Filing Date Title
CNA2006101343061A CN101191064A (en) 2006-11-20 2006-11-20 Novel production device for biological diesel oil

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CN101191064A true CN101191064A (en) 2008-06-04

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103275810A (en) * 2013-05-03 2013-09-04 李红艳 Catalytic cracking device for biodiesel preparation
CN105505588A (en) * 2015-08-19 2016-04-20 张敏 Compound biodiesel and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103275810A (en) * 2013-05-03 2013-09-04 李红艳 Catalytic cracking device for biodiesel preparation
CN103275810B (en) * 2013-05-03 2014-08-13 李红艳 Catalytic cracking device for biodiesel preparation
CN105505588A (en) * 2015-08-19 2016-04-20 张敏 Compound biodiesel and preparation method thereof

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