CN101167594B - Highly effective active biological preservative and preparation method thereof - Google Patents
Highly effective active biological preservative and preparation method thereof Download PDFInfo
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- CN101167594B CN101167594B CN2007101955753A CN200710195575A CN101167594B CN 101167594 B CN101167594 B CN 101167594B CN 2007101955753 A CN2007101955753 A CN 2007101955753A CN 200710195575 A CN200710195575 A CN 200710195575A CN 101167594 B CN101167594 B CN 101167594B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
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Abstract
The invention relates to a food preservative agent, in particular to an active biological preservative agent for low-sugar, low-salt and neutral foods. The highly effective active biological preservative agent of the invention provides extremely strong bacterial inhibition intensity for putrefactive bacteria and pathogenic bacteria in various foods, the bacterial inhibition has wide spectrum character, the effect is 5-10 times stronger than that of sodium benzoate or potassium sorbate under the same usage, the invention not only has the extremely strong bacterial inhibition effect to acidic foods, but also has the extremely strong bacterial inhibition effect to weakly-acidic, neutral, and faintly alkaline foods, traditional medicine pilula, and cosmetics. The invention is applicable to spreading and utilization.
Description
Technical field
The present invention relates to a kind of anticorrisive agent, particularly relate to a kind of active biological preservative that is used for low sugar, less salt and neutral food.
Background technology
China GB2760-96 all anticorrisive agents allowable all have different selectivity to bacteriostasis intensity, as certain anticorrisive agent to gram-positive bacteria inhibition strength height, but to the antibacterial intensity of Gram-negative bacteria just a little less than.Present domestic each food production producer, the anticorrisive agent that is widely used in foodstuff has: Sodium Benzoate and potassium sorbate, be harmful to health but all query, and only be applicable in the acid food, its anticorrosion some effect, but antibacterial intensity a little less than, antibacterial wide spectrum is narrower, country has begun the restriction use at present, and especially exported product is limited very big, and the novel built anticorrisive agent is recommended to use by native land man.
Summary of the invention
Purpose of the present invention is exactly the deficiency that overcomes existing aseptic technic, a kind of active biological preservative that is used for food and Chinese medicine class and toiletries is provided, and it is favorable anti-corrosion effect not only, and is cheap and meet country and international standard, nontoxic, harmless, environmental protection are fit to extensively promote the use of.
An object of the present invention is to provide a kind of highly effective active biological preservative.
Another object of the present invention provides the preparation method of described highly effective active biological preservative.
The objective of the invention is to be achieved through the following technical solutions:
A kind of highly effective active biological preservative, its feedstock production by following parts by weight forms;
Natamycin 0.01-0.1 anticorrisive agent 0.2-3
Sodium orthophosphate 0.2-2.5 citric acid 0.5-4
Natrium citricum 0.4-3.5 maltodextrin 0.5-3
Described anticorrisive agent is propyl p-hydroxybenzoate sodium or sodium Diacetate.
Natamycin of the present invention: standard GB2760-2001 is a China and international FDA/WHO new bio anticorrisive agent allowable, safe, nontoxic, little residual white powder, its purity 1-50%.Gram-positive bacterias such as the many saccharomycete, mould that food played main putrefaction of this agent have high inhibitory action more potent more than 50 times than potassium sorbate, to Gram-negative bacteria inhibitory action power also clearly, just can suppress breeding and the existence of microorganism at a few millionths through the experiment consumption.It can be to all having antibacterial actual effect in nearly all food, traditional Chinese medicine pill, cosmetics and the food instruments surface such as neutrality, acidity, alkalescent;
Anticorrisive agent: be propyl p-hydroxybenzoate sodium or sodium Diacetate, it all has the broad spectrum activity bacteriostatic agent, mould, saccharomycete, bacillus, Escherichia coli, lactic acid bacteria all there is very strong fungistatic effect, than the strong 5-10 of the antibacterial power of potassium sorbate commonly used doubly, and meet the regulation of GB2760-96 and FDA/WHO international standard, be widely used in the anticorrisive agent of various food, pharmaceuticals, cosmetics, be white powder.After itself and natamycin are composite, because Mi mends mutually, synergistic function.Not only strengthen antibacterial intensity, also increase antimicrobial spectrum, the use amount of anticorrisive agent greatly reduces, and sterilization temperature is also along with reduction, thus energy-conservation reducing cost;
Sodium orthophosphate and natrium citricum: be the neutral white crystalline powder, it is the chelating agent of heavy metal ion, the auxilliary mould middle chelated copper ion passivation of microorganism, and goes its activity.So in anticorrisive agent of the present invention, play complementary synergistic effect.
Citric acid: white acidic crystallization powder, add and work to strengthen acidity in this anticorrisive agent, hydrogen ion wherein reduces activation of microorganism;
Maltodextrin also claims the starch rubber polymer.It is with each kind of starch as raw material, transform through enzyme method technique low degree control hydrolysis, purify, drying forms.Maltodextrin is widely used in candy, the extract of malt and milk, fruit tea, milk powder, ice cream, beverage, can, health products and other food, it is the inserts and the thickener of varieties of food items, plays increase in this preservative substance formula the adhesive force of food surface is closed cohesive force.
Preferably, a kind of highly effective active biological preservative, its feedstock production by following parts by weight forms;
Natamycin 0.02-0.8 anticorrisive agent 0.5-2
Sodium orthophosphate 0.5-2 citric acid 1-3
Natrium citricum 0.5-3 maltodextrin 1-3
Described anticorrisive agent is propyl p-hydroxybenzoate sodium or sodium Diacetate.
The preparation method of a kind of highly effective active biological preservative of the present invention, it may further comprise the steps;
Take by weighing each raw material by formula ratio, mix, packing gets final product.
The using method of a kind of highly effective active biological preservative of the present invention, it may further comprise the steps;
1, the use in the thermally processed foods: before food processing, 0.05-0.1% by the raw-food material gross weight takes by weighing biological preservative, the hot water of getting anticorrisive agent 5-10 times weight again dissolves biological preservative, at last the biological antiseptic agent solution is joined in the raw-food material, and food prepared therefrom gets final product;
2, the use in the normal temperature converted products: the 0.05-0.1% by the products material gross weight takes by weighing biological preservative, the hot water of getting anticorrisive agent 5-10 times weight again dissolves biological preservative, at last the biological antiseptic agent solution is joined in the product, mix, and finish;
3, the use on food and food utensil surface: the biological antiseptic liquid of getting 0.3-0.5% concentration, to the food of need surface anticorrosion or food utensil surface spraying or food and food utensil are dipped into a moment in the biological antiseptic liquid of same concentrations, pull out and dry, and finish.
Described thermally processed foods comprises: cake, meat products, sweet potato goods (little potato son), can, jam, jelly, tartar sauce, fruit wine, beverage etc., described normal temperature converted products comprises: pickles, pickles, cold drink, health products, medicine pill, cosmetics etc.
Highly effective active biological preservative of the present invention has extremely strong antibacterial intensity to spoilage organisms and pathogenic bacteria in the various food, antibacterial have a broad spectrum activity, under equal consumption than Sodium Benzoate or the strong 5-10 of potassium sorbate effect doubly, it not only has extremely strong fungistatic effect to acid food, and faintly acid, neutrality, alkalescent food and medicine pill and cosmetics are had extremely strong fungistatic effect equally.Be well suited for promoting the use of.
The specific embodiment
Below adopt embodiment to specify a kind of highly effective active biological preservative of the present invention and preparation method thereof.
Embodiment 1
Natamycin 0.02kg propyl p-hydroxybenzoate sodium 0.5kg
Sodium orthophosphate 1kg citric acid 1kg
Natrium citricum 0.5kg maltodextrin 3kg
Take by weighing each raw material by formula ratio, mix, packing gets final product.
Embodiment 2
Natamycin 0.08kg sodium Diacetate 2.5kg
Sodium orthophosphate 0.3kg citric acid 3kg
Natrium citricum 2kg maltodextrin 2kg
Its preparation method is with embodiment 1
Embodiment 3
Natamycin 0.05kg propyl p-hydroxybenzoate sodium 0.9kg
Sodium orthophosphate 2.3kg citric acid 2kg
Natrium citricum 3.5kg maltodextrin 0.8kg
Its preparation method is with embodiment 1
Below by the contrast experiment effect of the embodiment of the invention 1 highly effective active biological preservative is described;
The experimental situation temperature: 20-25 above freezing ℃, relative humidity: 50-60%;
With and low sugar red bean jelly food young with the little potato of sweet potato processing is experimental subjects, is divided into 3 groups;
First group is the young and low sugar red bean jelly of little potato that adds Sodium Benzoate anticorrisive agent (0.05%);
Second group is the young and low sugar red bean jelly of little potato that adds potassium sorbate anticorrisive agent (0.1%);
The 3rd group is the young and low sugar red bean jelly of little potato that adds embodiment 1 highly effective active biological preservative (0.07%);
Experimental period: above-mentioned 3 groups of food are after placing 15 days, and second group slight denaturalization phenomenon occurred, first group and the 3rd group of no change;
Above-mentioned 3 groups of food are after placing 30 days, and second group serious denaturalization phenomenon occurred, and mouldy, and slight mildew phenomenon has appearred in first group of surface, the 3rd group of no change, and second group is withdrawed from experiment;
Remaining two groups of food are after placing three months, and first group a mould rotten phenomenon occurred, the 3rd group of no change, and first group is promptly withdrawed from experiment;
Remaining the 3rd group of food still remains intact after placing 12 months, and no change is unpacked, and taste does not still become when edible.
The anticorrisive agent cost of its 3 groups of food is as follows: first group of per kilogram food institute adding preservative agent cost is about 0.01 yuan, second group of per kilogram food institute adding preservative agent cost is about 0.035 yuan, and the 3rd group of per kilogram food institute adding preservative agent cost is about 0.015-0.02 unit.
Experiment showed, that more than the embodiment of the invention 1 highly effective active biological preservative effect is obvious, and cost is low, uses proof, broken through the difficulty of food antiseptic technology such as domestic neutrality really, have the leading position, be well suited for manufacturer and promote the use of through a large amount of production.
Claims (5)
1. highly effective active biological preservative, its feedstock production by following parts by weight forms;
Natamycin 0.01-0.1 anticorrisive agent 0.2-3
Sodium orthophosphate 0.2-2.5 citric acid 0.5-4
Natrium citricum 0.4-3.5 maltodextrin 0.5-3
Described anticorrisive agent is propyl p-hydroxybenzoate sodium or sodium Diacetate.
2. the preparation method of a kind of highly effective active biological preservative according to claim 1, it may further comprise the steps;
Take by weighing each raw material by formula ratio, mix, packing gets final product.
3. the using method of a kind of highly effective active biological preservative according to claim 1 is characterized in that;
1) use in the thermally processed foods: before food processing, 0.05-0.1% by the raw-food material gross weight takes by weighing biological preservative, the hot water of getting anticorrisive agent 5-10 times weight again dissolves biological preservative, at last the biological antiseptic agent solution is joined in the raw-food material, and food prepared therefrom gets final product;
2) use in the normal temperature converted products: the 0.05-0.1% by the products material gross weight takes by weighing biological preservative, the hot water of getting anticorrisive agent 5-10 times weight again dissolves biological preservative, at last the biological antiseptic agent solution is joined in the product, mix, promptly finish;
3) use on food and food utensil surface: the biological antiseptic liquid of getting 0.3-0.5% concentration, to the food of need surface anticorrosion or food utensil surface spraying or food and food utensil are dipped into a moment in the biological antiseptic liquid of same concentrations, pull out and dry, promptly finish.
4. the using method of a kind of highly effective active biological preservative according to claim 3, wherein said thermally processed foods comprises: a kind of in cake or meat products or sweet potato goods or jelly or tartar sauce or the beverage, described normal temperature converted products comprises: a kind of in pickles or pickles or cold drink or medicine pill or the cosmetics.
5. the using method of a kind of highly effective active biological preservative according to claim 3, wherein said thermally processed foods comprises can, described normal temperature converted products comprises health products.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2007101955753A CN101167594B (en) | 2007-12-07 | 2007-12-07 | Highly effective active biological preservative and preparation method thereof |
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| CN2007101955753A CN101167594B (en) | 2007-12-07 | 2007-12-07 | Highly effective active biological preservative and preparation method thereof |
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| CN101167594A CN101167594A (en) | 2008-04-30 |
| CN101167594B true CN101167594B (en) | 2010-06-02 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101797071B (en) * | 2010-01-28 | 2012-08-22 | 川渝中烟工业有限责任公司 | Cigar mildewproof additive and using method thereof |
| CN102993811A (en) * | 2012-11-29 | 2013-03-27 | 陈小康 | Preparation method of mildew-proof agent for coating |
| CN103416480B (en) * | 2013-08-07 | 2015-04-08 | 杨文侠 | Compound navel orange preservative prepared from plant extract |
| CN104413371A (en) * | 2013-08-22 | 2015-03-18 | 杜建安 | Method for preparing pickled vegetable by silage fresh fruit sugar biology fermentation preparation as well as technology thereof |
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| US6156362A (en) * | 1998-11-02 | 2000-12-05 | Lipton, Division Of Conopco, Inc. | Natamycin and chemical preservatives in foods and method of making |
| CN1336145A (en) * | 2000-08-01 | 2002-02-20 | 北京市营养源研究所 | Compound biological preservative |
| CN1806573A (en) * | 2006-01-26 | 2006-07-26 | 浙江工商大学 | Waxberry antistaling technique |
-
2007
- 2007-12-07 CN CN2007101955753A patent/CN101167594B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6156362A (en) * | 1998-11-02 | 2000-12-05 | Lipton, Division Of Conopco, Inc. | Natamycin and chemical preservatives in foods and method of making |
| CN1336145A (en) * | 2000-08-01 | 2002-02-20 | 北京市营养源研究所 | Compound biological preservative |
| CN1806573A (en) * | 2006-01-26 | 2006-07-26 | 浙江工商大学 | Waxberry antistaling technique |
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| JOHN L. et. al.Formation of Natamycin:Cyclodextrin Inclusion ComplexesandTheir Characterization.Agricultural and Food Chemistry51 24.2003,51(24),7106-7110. |
| JOHN L. et. al.Formation of Natamycin:Cyclodextrin Inclusion ComplexesandTheir Characterization.Agricultural and Food Chemistry51 24.2003,51(24),7106-7110. * |
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