CN101164925B - Sintering method red mud and Bayer method red mud mixed dam building method - Google Patents
Sintering method red mud and Bayer method red mud mixed dam building method Download PDFInfo
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- CN101164925B CN101164925B CN2007101129880A CN200710112988A CN101164925B CN 101164925 B CN101164925 B CN 101164925B CN 2007101129880 A CN2007101129880 A CN 2007101129880A CN 200710112988 A CN200710112988 A CN 200710112988A CN 101164925 B CN101164925 B CN 101164925B
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- sintering process
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- standpipe
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- 238000000034 method Methods 0.000 title claims abstract description 94
- 238000005245 sintering Methods 0.000 title claims abstract description 54
- 238000004131 Bayer process Methods 0.000 claims abstract description 39
- 229910001679 gibbsite Inorganic materials 0.000 claims abstract description 11
- 239000011449 brick Substances 0.000 claims abstract description 10
- 239000004576 sand Substances 0.000 claims description 24
- 230000008595 infiltration Effects 0.000 claims description 19
- 238000001764 infiltration Methods 0.000 claims description 19
- 230000008676 import Effects 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 7
- 239000000463 material Substances 0.000 abstract description 4
- 238000001914 filtration Methods 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 23
- 230000006835 compression Effects 0.000 description 20
- 238000007906 compression Methods 0.000 description 20
- 239000000203 mixture Substances 0.000 description 15
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- 229910000831 Steel Inorganic materials 0.000 description 6
- 239000010959 steel Substances 0.000 description 6
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 5
- 235000011941 Tilia x europaea Nutrition 0.000 description 5
- 239000000292 calcium oxide Substances 0.000 description 5
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000004571 lime Substances 0.000 description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 241000209094 Oryza Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 229910052918 calcium silicate Inorganic materials 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 238000005496 tempering Methods 0.000 description 2
- 229910001570 bauxite Inorganic materials 0.000 description 1
- 239000000404 calcium aluminium silicate Substances 0.000 description 1
- 235000012215 calcium aluminium silicate Nutrition 0.000 description 1
- WNCYAPRTYDMSFP-UHFFFAOYSA-N calcium aluminosilicate Chemical compound [Al+3].[Al+3].[Ca+2].[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O WNCYAPRTYDMSFP-UHFFFAOYSA-N 0.000 description 1
- 229940078583 calcium aluminosilicate Drugs 0.000 description 1
- LHJQIRIGXXHNLA-UHFFFAOYSA-N calcium peroxide Chemical compound [Ca+2].[O-][O-] LHJQIRIGXXHNLA-UHFFFAOYSA-N 0.000 description 1
- 235000019402 calcium peroxide Nutrition 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910001648 diaspore Inorganic materials 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- HUAUNKAZQWMVFY-UHFFFAOYSA-M sodium;oxocalcium;hydroxide Chemical compound [OH-].[Na+].[Ca]=O HUAUNKAZQWMVFY-UHFFFAOYSA-M 0.000 description 1
- 239000002910 solid waste Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Abstract
This invention discloses a method for damming by using mixed mud from sintering process and Bayer process. In this invention, the gibbsite Bayer process and sintering process red mud are mixed in the ratio of (0.43-2.33):1(dried mud) are used for the damming. Bricks are used for building cofferdam columns, in which are placed the vertical tubes which are then connecting filtration tubes and water-drainage ditch. There are permeating holes on the walls of the tubes. Between the column and its tube filled is fine sands. Due to the material of the dam is the same as the material decking-up, it makes simple building process and saving area for decking up Bayer process red mud. Advantages are low cost and saving raw materials.
Description
Technical field
The present invention relates to a kind of red mud from sintering process, Bayer process red mud mixed dam building method, belong to technical field of alumina production.
Background technology
Red mud be bauxite through various physics and chemical treatment, produce aluminum oxide after remaining reddish brown toner mud shape, high-moisture, alkaline solid waste, alumina producing enterprise adopts the mode of storing up of building a dam to handle red mud mostly, and stacked arrangement has wet method, semidrying, dry method etc. multiple.According to the production method difference of aluminum oxide, red mud generally is divided into red mud from sintering process and Bayer process red mud, and its quantum of output is different because of ore grade, production method, state of the art, in aluminum oxide production process, and 1.0~1.8 tons of red muds of 1 ton of aluminum oxide output of every production.Domestic alumina-producing method mainly contains: integrated process (the in parallel or series connection of sintering process and bayer's process), sintering process and bayer's process, wherein, sintering process is called soda-lime sintering process again, needing to add a large amount of lime prepares burden, utilize the high temperature bayer's process of domestic ore (being mainly diaspore type) also need add a certain amount of lime and carry out stripping, and utilize the low temperature bayer's process of external ore (being mainly gibbsite type) when stripping, not need to add lime.Red mud composed as follows:
Bayer's process last red mud weight is formed: SiO
218-25%, Fe
2O
328-35%, Al
2O
318-25%, Na
2O 8-12% and CaO2-4%;
Sintering process last red mud weight is formed: SiO
215-20%, Fe
2O
312-15%, Al
2O
36-9%, Na
2O 2-3% and CaO 35-45%.
Calcium oxide and dioxide-containing silica are higher in the red mud from sintering process, calcium oxide is generally about 40%, in the mineral composition based on beta-dicalcium silicate, the condense composition and the performance of condensing with some cement, and later strength height, be easy to pile up and build a dam, the red mud from sintering process of domestic aluminum oxide enterprise output adopts the wet method mode of storing up of building a dam to handle in the open.This method is simple, prove that through long-term practice its operation, technical qualification are very ripe, the highest dam body can be built more than 70 meters, first red mud dump of the application unit discharging red mud from sintering process is during nearly 50 years storing up, can keep safe and stable operation, and red mud dam, stockyard is in good condition at present always.Bayer process red mud contains higher ferric oxide and aluminum oxide, mineral composition is based on pyrrhosiderite, rhombohedral iron ore, calcium aluminosilicate hydrate (high temperature Bayer process red mud), owing to do not contain beta-dicalcium silicate, its gelling is relatively poor, utilize the high temperature bayer's process of domestic ore owing to when stripping, add lime, calcium oxide content is about 20% in the red mud, higher relatively, can adopt semidrying or the dry method mode of storing up of building a dam to handle mostly in the open, but loose, not fixed, the easy landslide of the red mud of building a dam, dam body is built highly difficult very big; Utilize the low temperature bayer's process of external ore owing to do not add lime during stripping, calcium oxide content is extremely low in the red mud, have only about 3%, the cohesion of red mud and permeability coefficient are all far below the high temperature Bayer process red mud, cause store up the back intensity too low, the red mud dewatering is poor in addition, can't build a dam at all, has the enterprise of sintering process technology to take red mud is pumped into the method processing that the sintering process flow process is prepared burden.Along with the low temperature bayer's process aluminum oxide output of utilizing external ore improves constantly, the sintering process production line is if continue the increasing Bayer process red mud of digestion, become no longer economical, the aluminum oxide enterprise that perhaps has does not have the sintering process flow process at all, the road that Bayer process red mud can only be walked to store up.Because this Bayer process red mud is difficult to build a dam, erecting the dam stacks Bayer process red mud more on every side in the stockyard earlier must to use other material, a kind of damming method is to adopt the red mud from sintering process wet method to build a dam, another kind of damming method is directly to build a cubic meter dam, the cost of building a dam is higher, therefore, the stacking problem of Bayer process red mud is the difficult problem of puzzlement alumina producing industry always.
Summary of the invention
The object of the present invention is to provide a kind of red mud from sintering process, Bayer process red mud mixed dam building method, will build a dam and stockpiling unites two into one, simplifying builds a dam stores up technology, especially improves the Bayer process red mud processing efficiency, reduces the cost of building a dam, and saves a cubic metre of earth and stone resource.
Red mud from sintering process of the present invention, Bayer process red mud mixed dam building method, import hydrargillite Bayer process red mud and red mud from sintering process are mixed counterweight amount ratio 0.43-2.33 in dried red mud: 1 mixes use, and promptly red mud from sintering process and import hydrargillite Bayer process red mud are mixed counterweight amount ratio 1 in dried red mud: 0.43-2.33 mixes use.
With liquid-solid ratio is that the red mud from sintering process washing system last underflow of 1.5-2.5 is pumped into red mud filter and carries out liquid-solid separation, filter filtrate is returned sintering process flow process washing red mud, filter cake enters the red mud tempering tank by chute, the import hydrargillite Bayer process red mud washing system last underflow that with liquid-solid ratio is 1.5-2.0 simultaneously is pumped into the red mud tempering tank, after mixing, two kinds of red muds are pumped into the red mud dump cloth again, stockyard backwater after the water seepage drainage prism dehydration returns bayer's process flow process washing red mud, after the mixing red mud on silt dam forms and does the beach and possess the condition of building a dam, finish again and mix damming with red mud and store up operation.
Ooze performance in order to improve row, fine sand cofferdam type row is set in building a dam oozes cylinder, diameter is at 1.5-3 rice, build the cofferdam cylinder with the brick base, be provided with standpipe in the cylinder of cofferdam, the lower end of standpipe joins with drainage pipe and is communicated with row's sewer, and standpipe and drainage pipe tube wall are provided with the infiltration hole, are filled with fine sand in the cavity that the brickwork joint of cofferdam cylinder and cofferdam cylinder and standpipe constitute.
The cofferdam cylinder is built by brick overlap joint hollow out base, and it is better that row is oozed performance.
It is suitable that the particle diameter of fine sand is controlled to be 0.07-0.9mm.
The steel pipe of the preferred φ 195-219mm of standpipe and drainage pipe, the infiltration hole of standpipe and drainage pipe, aperture are that 5-15mm is suitable, and infiltration is enclosed with gauze on the hole, prevent that fine sand from stopping up the infiltration hole.Extend and there is no need to establish the infiltration hole on the outer section outer drainage pipe of dam body.
Standpipe can be designed to multistage, is connected by flange, increases while constructing, and is flexible.
Cofferdam type of the present invention row is oozed cylinder and draining is become overflow is seepage flow, and ensures the quality of products by the granularity of adjusting fine sand in the cofferdam.In addition, standpipe is suitable for reading can to have reduced the huge investment of reservoir area flood control facility as the flood discharge passage in flood season, plays double-deck effect.In the process of storing up while building a dam, cofferdam type row also can be set in the stockyard ooze cylinder, but spacing distance can be longer slightly, in building a dam, the spacing distance that row is oozed cylinder is at 15-30 rice, and in the stockyard, the spacing distance that row is oozed cylinder can reach more than 40 meter.
The present invention is with red mud from sintering process, Bayer process red mud building dam by mixing, stockyard Bayer process red mud dehydration, accelerate the infiltration except that relying on red mud from sintering process, also rely on the red mud from sintering process aquation to improve intrinsic strength, suitable sintering process Bayer process red mud building dam by mixing intensity of mixing counterweight amount ratio has reached the intensity that pure red mud from sintering process is built a dam, can increase substantially the stockyard red mud and store up height, thereby improve the stockyard utilization ratio.Red mud from sintering process, Bayer process red mud mix, realization is built a dam and is stored up for a kind of material, two kinds of technologies can be united two into one, simplify damming with red mud and stored up technology, damming with red mud mode and the existing sophisticated sintering process wet method mode of storing up of building a dam in the open of mixing is identical, is convenient to production scene management and application.Compare with the low temperature Bayer process red mud stockyard of building cubic meter dam, the identical stackable more Bayer process red mud of area of storing up has especially improved the Bayer process red mud processing efficiency, and can reduce the cost of building a dam, and saves valuable cubic metre of earth and stone resource.
Description of drawings
Cofferdam type row is oozed the column structure synoptic diagram among Fig. 1, the present invention.
Among the figure: 1, joint flange 2, standpipe 3, base are built hollow out 4, drainage pipe 5, are arranged and ooze cylinder 6, fine sand 7, infiltration hole.
Embodiment
The invention will be further described in conjunction with the foregoing description accompanying drawing.
Fine sand cofferdam type row is set in building a dam oozes cylinder, build up the base with the brick base and build the cofferdam cylinder 5 of hollow out 3, be provided with φ 200mm steel pipe riser 2 in the cofferdam cylinder 5, standpipe 2 is designed to multistage, connect by joint flange 1, connect while constructing and to increase, the lower end of standpipe 2 is communicated with drainage pipe 4, the tube wall of standpipe 2 is provided with infiltration hole 7, the aperture is 10mm, infiltration hole 7 is wrapped with gauze, is filled with fine sand 6 in the cavity that the brickwork joint of cofferdam cylinder 5 and cofferdam cylinder 5 and standpipe 2 constitute, and the particle diameter of fine sand is controlled to be 0.5mm.
It is to build a dam after mixing at 0.43: 1 that import hydrargillite Bayer process red mud and red mud from sintering process are mixed counterweight amount ratio in dried red mud, 28 days mix red mud ultimate compression strength is 0.77 MPa, the same period, pure red mud from sintering process ultimate compression strength was 0.99 MPa, 60 days mix red mud ultimate compression strength is 1.47 MPa, and the same period, pure red mud from sintering process ultimate compression strength was 1.16 MPa.
Fine sand cofferdam type row is set in building a dam oozes cylinder, build up the base with the brick base and build the cofferdam cylinder 5 of hollow out 3, be provided with φ 210mm steel pipe riser 2 in the cofferdam cylinder 5, standpipe 2 is designed to multistage, connect by joint flange 1, connect while constructing and to increase, the lower end of standpipe 2 is communicated with drainage pipe 4, the tube wall of standpipe 2 is provided with infiltration hole 7, the aperture is 12mm, infiltration hole 7 is wrapped with gauze, is filled with fine sand 6 in the cavity that the brickwork joint of cofferdam cylinder 5 and cofferdam cylinder 5 and standpipe 2 constitute, and the particle diameter of fine sand is controlled to be 0.08mm.
It is to build a dam after mixing at 1: 1 that import hydrargillite Bayer process red mud and red mud from sintering process are mixed counterweight amount ratio in dried red mud, 28 days mix red mud ultimate compression strength is 0.85MPa, the same period, pure red mud from sintering process ultimate compression strength was 0.99MPa, 60 days mix red mud ultimate compression strength is 1.12MPa, and the same period, pure red mud from sintering process ultimate compression strength was 1.16MPa.
Fine sand cofferdam type row is set in building a dam oozes cylinder, build up the base with the brick base and build the cofferdam cylinder 5 of hollow out 3, be provided with φ 198mm steel pipe riser 2 in the cofferdam cylinder 5, standpipe 2 is designed to multistage, connect by joint flange 1, connect while constructing and to increase, the lower end of standpipe 2 is communicated with drainage pipe 4, the tube wall of standpipe 2 is provided with infiltration hole 7, the aperture is 8mm, infiltration hole 7 is wrapped with gauze, is filled with fine sand 6 in the cavity that the brickwork joint of cofferdam cylinder 5 and cofferdam cylinder 5 and standpipe 2 constitute, and the particle diameter of fine sand is controlled to be 0.2mm.
It is to build a dam after mixing at 2.33: 1 that import hydrargillite Bayer process red mud and red mud from sintering process are mixed counterweight amount ratio in dried red mud, 28 days mix red mud ultimate compression strength is 0.82MPa, the same period, pure red mud from sintering process ultimate compression strength was 0.99MPa, 60 days mix red mud ultimate compression strength is 0.94MPa, and the same period, pure red mud from sintering process ultimate compression strength was 1.16MPa.
Fine sand cofferdam type row is set in building a dam oozes cylinder, build up the base with the brick base and build the cofferdam cylinder 5 of hollow out 3, be provided with φ 205mm steel pipe riser 2 in the cofferdam cylinder 5, standpipe 2 is designed to multistage, connect by joint flange 1, connect while constructing and to increase, the lower end of standpipe 2 is communicated with drainage pipe 4, the tube wall of standpipe 2 is provided with infiltration hole 7, the aperture is 11mm, infiltration hole 7 is wrapped with gauze, is filled with fine sand 6 in the cavity that the brickwork joint of cofferdam cylinder 5 and cofferdam cylinder 5 and standpipe 2 constitute, and the particle diameter of fine sand is controlled to be 0.9mm.
It is to build a dam after mixing at 0.8: 1 that import hydrargillite Bayer process red mud and red mud from sintering process are mixed counterweight amount ratio in dried red mud, 28 days mix red mud ultimate compression strength is 0.75MPa, the same period, pure red mud from sintering process ultimate compression strength was 0.99MPa, 60 days mix red mud ultimate compression strength is 1.47MPa, and the same period, pure red mud from sintering process ultimate compression strength was 1.16MPa.
Fine sand cofferdam type row is set in building a dam oozes cylinder, build up the base with the brick base and build the cofferdam cylinder 5 of hollow out 3, be provided with φ 215mm steel pipe riser 2 in the cofferdam cylinder 5, standpipe 2 is designed to multistage, connect by joint flange 1, connect while constructing and to increase, the lower end of standpipe 2 is communicated with drainage pipe 4, the tube wall of standpipe 2 is provided with infiltration hole 7, the aperture is 15mm, infiltration hole 7 is wrapped with gauze, is filled with fine sand 6 in the cavity that the brickwork joint of cofferdam cylinder 5 and cofferdam cylinder 5 and standpipe 2 constitute, and the particle diameter of fine sand is controlled to be 0.6mm.
It is to build a dam after mixing at 1.8: 1 that import hydrargillite Bayer process red mud and red mud from sintering process are mixed counterweight amount ratio in dried red mud, 28 days mix red mud ultimate compression strength is 0.86MPa, the same period, pure red mud from sintering process ultimate compression strength was 0.99MPa, 60 days mix red mud ultimate compression strength is 1.11MPa, and the same period, pure red mud from sintering process ultimate compression strength was 1.16MPa.
Claims (6)
1. a red mud from sintering process, Bayer process red mud mixed dam building method is characterized in that red mud from sintering process and import hydrargillite Bayer process red mud mix counterweight amount ratio 1: 0.43-2.33 in dried red mud and mix.
2. red mud from sintering process according to claim 1, Bayer process red mud mixed dam building method, it is characterized in that in building a dam, being provided with fine sand cofferdam type row and ooze cylinder, build the cofferdam cylinder with the brick base, be provided with standpipe in the cylinder of cofferdam, the lower end of standpipe joins with drainage pipe and is communicated with row's sewer, standpipe and drainage pipe tube wall are provided with the infiltration hole, are filled with fine sand in the cavity that the brickwork joint of cofferdam cylinder and cofferdam cylinder and standpipe constitute.
3. red mud from sintering process according to claim 2, Bayer process red mud mixed dam building method is characterized in that the cofferdam cylinder overlaps the hollow out base by brick and builds.
4. according to claim 2 or 3 described red mud from sintering process, Bayer process red mud mixed dam building method, the particle diameter that it is characterized in that fine sand is 0.07-0.9mm.
5. red mud from sintering process according to claim 4, Bayer process red mud mixed dam building method is characterized in that being enclosed with gauze on the infiltration hole of standpipe and drainage pipe.
6. red mud from sintering process according to claim 5, Bayer process red mud mixed dam building method is characterized in that standpipe has multistage, are connected by flange.
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CN102409684B (en) * | 2011-08-04 | 2014-08-13 | 中国铝业股份有限公司 | Storage-yard damming method of red mud by mixed self-solidifying dry process |
CN114804693B (en) * | 2022-02-16 | 2023-03-31 | 中铝山西新材料有限公司 | Solid waste compound fly ash excitant and application thereof |
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