CN101157511A - Oil-bearing sludge decomposition method - Google Patents

Oil-bearing sludge decomposition method Download PDF

Info

Publication number
CN101157511A
CN101157511A CNA2007100129332A CN200710012933A CN101157511A CN 101157511 A CN101157511 A CN 101157511A CN A2007100129332 A CNA2007100129332 A CN A2007100129332A CN 200710012933 A CN200710012933 A CN 200710012933A CN 101157511 A CN101157511 A CN 101157511A
Authority
CN
China
Prior art keywords
oil
mud
oil sludge
effluent oil
sump oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CNA2007100129332A
Other languages
Chinese (zh)
Other versions
CN100572309C (en
Inventor
隋学平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daqing Luyuan forest biological environmental protection Co. Ltd.
Original Assignee
隋学平
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 隋学平 filed Critical 隋学平
Priority to CNB2007100129332A priority Critical patent/CN100572309C/en
Publication of CN101157511A publication Critical patent/CN101157511A/en
Application granted granted Critical
Publication of CN100572309C publication Critical patent/CN100572309C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Abstract

A decomposition method of effluent oil sludge is characterized in that the effluent oil sludge is added into a treatment tank which can be heated up, according to the weight percentage in the effluent oil sludge, sodium metasilicate, polyether polylol and ethylene diamine tetraacetic acid are added to mixed evenly with the effluent oil sludge, and is reacted to the effluent oil sludge under the condition of being heated up, thereby ensuring that oil, mud and water are separated completely, oil at the upper layer is extracted, and the treatment without social effects of pollution is performed for the rest mud and water. The sodium metasilicate, the polyether polylol and the ethylene diamine tetraacetic acid which are added according to the weight percentage in the effluent oil sludge are respectively 2.5 to 3.0 percent, 0.3 to 0.5 percent, and 0.05 percent. The sodium metasilicate, the polyether polylol and the ethylene diamine tetraacetic acid react to the effluent oil sludge under the condition of being heated up to 70 to 85 Deg C. The three articles are innoxious and are all neutral materials, no secondary pollution is caused, a little dosage is needed, and the decomposition of effluent oil sludge is complete. The invention has the advantages of wide raw material sources, lower price, simple technique and easy operation.

Description

A kind of oil-bearing sludge decomposition method
Technical field
The present invention relates to the oil-bearing sludge decomposition method that produces in the oil recovery process of oil field.
Background technology
Sump oil mud is in oil field oil recovery or the oil refining process, the thick viscid oil contaminants that contains that spins off from oil.Present treatment process: partition method, decomposition method, re-injection method are arranged, bury method, biological degradation method or burning method to sump oil mud.These treatment processs except that burning method, maximum shortcoming are to exist processing not thorough, need take the farmland of a large amount of preciousnesses, and chemical separation, decomposition agent in separation, the decomposition method can cause secondary pollution.Though burning method is comparatively thorough, burn for the sump oil mud of oil-containing more than 35%, do not meet energy-conservation principle.The common oil-containing 35% of the sump oil mud that produces after the oil production, this part sump oil mud is valuable secondary resource, if these sump oil mud are carried out the collection of science, and develop this partly crude oil, not only reclaimed a large amount of resources, bring huge economic benefit, and the meeting pollution abatement, huge environmental benefit produced.
Summary of the invention
The technical problem to be solved in the present invention provides and extracts crude oil a kind of sump oil mud can the decomposition, and cost is low, and disaggregating treatment is oil-bearing sludge decomposition method completely.
The technical scheme that adopts is:
A kind of oil-bearing sludge decomposition method, sump oil mud is added in the treatment trough that can heat, stir by per-cent adding Starso, polyether glycol and the disodium salt and the sump oil mud that account for sump oil mud weight, under heating condition, react with sump oil mud, oil, mud, water are thoroughly separated, extract upper strata oil composition, all the other mud, water are done nuisanceless processing.
The above-mentioned Starso that adds by sump oil mud weight percent is that 2.5-3.0%, polyether glycol are that 0.3-0.5%, disodium salt are 0.05%.
Above-mentioned Starso, polyether glycol and disodium salt and sump oil mud react being warmed under the 70-85 ℃ of condition.
The present invention handles that sump oil mud method is simple, science, rationally.Adopt Starso (Na 2SiO 3) modulus is 1 neutral crystal type water glass, nontoxic polyether glycol, disodium salt (C 10H 16N 2O 8) complexing agent adds sump oil mud and be dissolved in the sump oil mud, Starso reduces sump oil mud surface tension, improves the decomposition effect of sump oil mud.Described polyether glycol can be used as crude oil demulsifier in the present invention, can interrupt the effect of crude oil molecular chain, prevents that hard scale from forming, and promotes the abundant breakdown of emulsion of sump oil mud, reduces its surface tension, improves sump oil mud and decomposes effect, favourable secondary oil recovery.Described disodium salt is in the present invention as complexing agent, generate water-fast intermediate product, the nuclear that coagulates as new life, promote suspended particulate matter or colloid thing that the sedimentation downwards of cohesion back takes place, reduce the organic content in the pending water, thereby improved decomposing, purifying effect effectively sump oil mud.The above-mentioned nontoxic neutral material that is of three kinds of chemical substances can not produce secondary pollution, and it is thorough that consumption decomposes sump oil mud less.Have raw material sources extensively, price is lower, technology is simple, the advantage of easy handling.
Embodiment
Embodiment one
A kind of oil-bearing sludge decomposition method, sump oil mud is added in the groove of handling of can heating, Starso by the per-cent adding 2.8% that accounts for sump oil mud weight, the polyether glycol of adding 0.4%, the disodium salt of adding 0.05%, and stir with sump oil mud, be warmed to 80 ℃ with the greasy dirt reaction, make oil, mud, water sepn.
Embodiment two
A kind of oil-bearing sludge decomposition method, sump oil mud is added in the groove of handling of can heating, sump oil mud is warmed to 75 ℃, Starso by the per-cent adding 2.6% that accounts for sump oil mud weight, the polyether glycol of adding 0.3%, add 0.05% disodium salt, and stir with sump oil mud and to make oil, mud, water sepn.
Embodiment three
A kind of oil-bearing sludge decomposition method, by weight per-cent in the sump oil mud added 3.0% Starso, the polyether glycol of adding 0.5%, the disodium salt of adding 0.05%, mix, mixed sump oil mud is put into and can be warmed to 78 ℃ and greasy dirt reaction at the treatment trough of heating, make oil, mud, water sepn.

Claims (3)

1. oil-bearing sludge decomposition method, it is characterized in that sump oil mud is added in the treatment trough that can heat, stir by per-cent adding Starso, polyether glycol and the disodium salt and the sump oil mud that account for sump oil mud weight, under heating condition, react with greasy dirt, oil, mud, water are thoroughly separated, extract upper strata oil composition, all the other mud, water are done nuisanceless processing.
2. a kind of oil-bearing sludge decomposition method according to claim 1 is characterized in that the described Starso that adds by sump oil mud weight percent is that 2.5-3.0%, polyether glycol are that 0.3-0.5%, disodium salt are 0.05%.
3. a kind of oil-bearing sludge decomposition method according to claim 1 is characterized in that described Starso, polyether glycol and disodium salt and sump oil mud react being warmed under the 70-85 ℃ of condition.
CNB2007100129332A 2007-09-24 2007-09-24 A kind of oil-bearing sludge decomposition method Expired - Fee Related CN100572309C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2007100129332A CN100572309C (en) 2007-09-24 2007-09-24 A kind of oil-bearing sludge decomposition method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2007100129332A CN100572309C (en) 2007-09-24 2007-09-24 A kind of oil-bearing sludge decomposition method

Publications (2)

Publication Number Publication Date
CN101157511A true CN101157511A (en) 2008-04-09
CN100572309C CN100572309C (en) 2009-12-23

Family

ID=39305763

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2007100129332A Expired - Fee Related CN100572309C (en) 2007-09-24 2007-09-24 A kind of oil-bearing sludge decomposition method

Country Status (1)

Country Link
CN (1) CN100572309C (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103803765A (en) * 2012-11-07 2014-05-21 中国石油化工股份有限公司 Oil sludge demulsifier and preparation method thereof
CN104310725A (en) * 2014-09-23 2015-01-28 胡延节 Splitting separation technology and equipment for oil sand
CN105084687A (en) * 2015-08-13 2015-11-25 中国海洋石油总公司 Chemical comprehensive treatment method of fatlute containing polymers

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103803765A (en) * 2012-11-07 2014-05-21 中国石油化工股份有限公司 Oil sludge demulsifier and preparation method thereof
CN103803765B (en) * 2012-11-07 2015-08-12 中国石油化工股份有限公司 A kind of greasy filth emulsion splitter and preparation method thereof
CN104310725A (en) * 2014-09-23 2015-01-28 胡延节 Splitting separation technology and equipment for oil sand
CN105084687A (en) * 2015-08-13 2015-11-25 中国海洋石油总公司 Chemical comprehensive treatment method of fatlute containing polymers
CN105084687B (en) * 2015-08-13 2017-08-04 中国海洋石油总公司 A kind of chemical synthesis processing method of polymer-containing oil sludge

Also Published As

Publication number Publication date
CN100572309C (en) 2009-12-23

Similar Documents

Publication Publication Date Title
CN102786713B (en) A kind of oil field mud recycling processing method
CN103739137B (en) The harmless treatment recovery method of oilfield sump oil and device
CN100355677C (en) Process for separating treating mud containing oil
CN102872614B (en) Petrochemical engineering waste separating processing method
CN103896466A (en) Dirty oil sludge decomposition method
CN108409077A (en) Oily sludge materialization coupled processing method
CN101781575B (en) Method for preparing high-cleanness fuel oil from intermediate-temperature and low-temperature coal tar
CN108558154A (en) The immediate processing method of oily sludge
CN103215064A (en) Method for removing metal in high-acid heavy crude oil
CN100572309C (en) A kind of oil-bearing sludge decomposition method
CN105176565B (en) A kind of method that heterogeneous reaction separates tar sand oil
CN212246242U (en) Sodium sulfate and mixed useless salt sediment processing system of sodium chloride
CN103113912A (en) Method for separating and extracting crude oil from oil sand
CN103194275B (en) Absorbent of naphthaline in coke oven gas and preparation method thereof
CN109020107A (en) Greasy filth demulsification three phase separation agent and its preparation process
CN108176518A (en) A kind of preparation method of neutral flotation agent for quartz mineral purification
CN111498871A (en) System and method for treating waste salt residues mixed by sodium sulfate and sodium chloride
CN106984264A (en) The method that harmless treatment prepares atlapulgite is carried out to spent FCC catalyst
CN103801546A (en) Resource treatment method for oil, mud and sand
CN1235843C (en) Method for eliminating and reclaiming acid component from oil products
CN105062557B (en) The anacidity process for purification of waste mineral oil
CN86101738A (en) The waste acid recycling method of sulfuric acid alkylation
CN111099796A (en) Method for decomposing oil sludge
CN107162365B (en) Preparation method and use method of sludge oil removal agent
CN1243072C (en) Method for recovering clean oil from heavy dirty oil

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: DAQING ZHONGLIN LVYUAN BIOLOGICAL ENVIRONMENTAL PR

Free format text: FORMER OWNER: SUI XUEPING

Effective date: 20100122

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20100122

Address after: Room 403, block C, Pioneer Park, hi tech Zone, Heilongjiang, Daqing

Patentee after: Daqing Luyuan forest biological environmental protection Co. Ltd.

Address before: Anda City, Heilongjiang Wanbao Town Center School

Patentee before: Sui Xueping

DD01 Delivery of document by public notice

Addressee: Xia Guanghui

Document name: Notification to Pay the Fees

DD01 Delivery of document by public notice

Addressee: Daqing Luyuan forest biological environmental protection Co. Ltd.

Document name: Notification of Termination of Patent Right

C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20091223

Termination date: 20130924