CN101126051A - Subacidity skin-moistening synthetic toilet soap - Google Patents
Subacidity skin-moistening synthetic toilet soap Download PDFInfo
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- CN101126051A CN101126051A CNA2007100444286A CN200710044428A CN101126051A CN 101126051 A CN101126051 A CN 101126051A CN A2007100444286 A CNA2007100444286 A CN A2007100444286A CN 200710044428 A CN200710044428 A CN 200710044428A CN 101126051 A CN101126051 A CN 101126051A
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Abstract
The invention discloses a skin-moistening synthesis toilet soap with weak acidic, comprising the components according to weight proportion: 40-60 shares of coconut acyloxyethanesulfonate, 5-10 shares of coconut acid, 5-20 shares of sodium dodecyl sulfate, 0.2-3 shares of glycerol, 0.5-4 shares of softening agent SG, 0.1-0.4 shares of chelating agent, 10-35 shares of filling agent and 1-5shares of deionized water. The pH value of the toilet soap is between 4.5 and 6.5, and is close to the weak acidic environment of human body. Therefore, the invention has little degreasing ability, mild property and can avoid the stimulation to skin when in washing.
Description
Technical field
The present invention relates to a kind of perfumed soap, relate to a kind of synthetic soap particularly.
Background technology
In the prior art, the many insights of perfumed soap are to be the Cake-shape soap of soap base with animals and plants or animal-plant oil synthetic sodium soap, though have cleaning force, whipability and easy washability preferably, but the pH value of its monoblock soap product between 9.5～10.5, soap body meta-alkalescence, not anti-hard water, can produce incrustation scale during washing, form the calcium magnesium soap, degreasing power is strong, and the skin sense is poor.And the pH value 4.5～6.5 of general human body skin, tart on the weak side if the soap of human body life-time service meta-alkalescence can make skin feel dry and astringent, has excitement.
In order to solve the pungency problem of perfumed soap to skin, products such as rich fat perfumed soap and skin care scented soap have appearred on the market, these products are further to reduce free alkali content in general perfumed soap prescription, added fat agent or skin-protecting agent, these are crossed fat agent or skin-protecting agent and form one deck hydrophobic film and wetting effect is provided or stays hydrophobic film and make the skin softness on skin in cleaning course, but because its pH value is 8～10, still be alkalescence, still bigger to the stimulation of skin.
In Chinese invention patent 200510095229.9, disclose a kind of prescription of neutral fancy soap for moistening skin, comprised 50.00～70.00 parts of anion surfactants, 8.00～10.00 parts of amphotericses, 5.00～8.00 parts in lipid acid, 0.10～0.50 part of titanium dioxide, 0.10～0.30 part of sequestrant, 1.00～5.00 parts of deionized waters.Obviously, the pH value of product is a very important technical indicator in this patent, yet only mentions this product for neutral in this patent, and pH value does not provide the concrete pH value data of its product about 7, the concrete grammar of producing this finished product is not provided yet.And, because human body skin pH value 4.5～6.5,, do not provide and the adapt wash conditions of pH value of human body skin acidic conditions even this product P H value is 7 yet, cause using this product to alleviate and can't fundamentally avoid its stimulation skin.
Summary of the invention
Technical problem to be solved by this invention provides a kind of Subacidity skin-moistening synthetic toilet soap, and its pH value near the weak acid environment of human body skin, can be avoided in the washing process stimulation to skin between 4.5～6.5.
Technical scheme of the present invention is: a kind of Subacidity skin-moistening synthetic toilet soap, it comprises each component of following weight proportion, 40～60 parts in cocounut oil acyloxy ethylsulfonic acid sodium, 5～10 parts of cocinic acids, 5～20 parts of sodium lauryl sulphate, 0.2～3 part of glycerine, 0.5～4 part of softener sg, 0.1～0.4 part of sequestrant, 10～35 parts of weighting agents, 1～5 part of deionized water.
Wherein, described softener sg, for lipid acid and ethylene oxide condensation make, pH value 5.0～7.0, be white in color or flaxen soft paste, external trade name Soromine SG, this type of raw material can be bought acquisition on Chemical market, common model has softener sg-6, softener sg-7, softener sg-9, softener sg-10 etc., and selection optimum among the present invention is a softener sg-6.By in product of the present invention, adding softener sg, main component cocounut oil acyloxy ethylsulfonic acid sodium of the present invention, sodium lauryl sulphate are the solid state raw material on the one hand, binding property is relatively poor in the one-tenth soap process, and soap body ftractures easily, can impel the soap body moulding well by adding softener sg; This raw material belongs to non-ionic type on the other hand, is diffusion type in water, has good flexibility and oilness, in washing process skin is had the better protecting effect.
Described sequestrant is a kind of or its mixture among EDTA-4Na, the H501.
Described weighting agent is selected from a kind of or its mixture in sodium sulfate, sodium-chlor, talcum powder, starch, the dextrin.Best is to select to adopt dextrin as weighting agent.
Among the present invention, can also comprise that weight proportion is 1～4 part a skin moisten nutritive ingredient, described skin moisten nutritive ingredient is a kind of or its mixture in vitamin E, extract solution from aloe, wallantoin, isostearoyl Sodium.alpha.-hydroxypropionate, the lactic acid.Be better protection skin, preferred, in Subacidity skin-moistening synthetic toilet soap of the present invention, comprise: 0.2～0.4 part of 10 times of extract solution from aloe, 0.1～0.4 part of wallantoin, 0.5～2 part of isostearoyl Sodium.alpha.-hydroxypropionate, 0.2～1.2 part of lactic acid.
Among the present invention, can also comprise that weight proportion is 0.2～0.8 part a antiseptic-germicide, described antiseptic-germicide is a kind of or its mixture in Trichlorocarbanilide, the trichlorine hydroxy diphenyl ether.
In addition, in the present invention, can also add other functional ingredient commonly used in the common perfumed soap, for example: pigment, essence, oxidation inhibitor, titanium dioxide etc., to realize corresponding function respectively.
Preferably, Subacidity skin-moistening synthetic toilet soap of the present invention, it comprises each component of following weight proportion, 50～55 parts in cocounut oil acyloxy ethylsulfonic acid sodium, 5～10 parts of cocinic acids, 7～10 parts of sodium lauryl sulphate, 1～2 part of glycerine, 1.5～2.5 parts of softener sgs, 0.2～0.3 part of H501 sequestrant, 10～35 parts in dextrin, 1～5 part of deionized water, 0.2～0.4 part of 10 times of extract solution from aloe, 0.1～0.4 part of wallantoin, 0.5～2 part of isostearoyl Sodium.alpha.-hydroxypropionate, 0.2～1.2 part of lactic acid, titanium dioxide 0.08～0.1 2 part, 0.2～0.6 part of antiseptic-germicide, 1.0～1.5 parts in essence.The Subacidity skin-moistening synthetic toilet soap that adopts this preferred version proportioning component to make, foam are fine and smooth more, performance is gentle more, and degrease power is very low.
Subacidity skin-moistening synthetic toilet soap of the present invention compared with prior art has following advantage:
It is the perfumed soap main component that the present invention has adopted cocounut oil acyloxy ethylsulfonic acid sodium, sodium lauryl sulphate, cocinic acid, softener sg, the perfumed soap pH value that makes is between 4.5～6.5, weak acid environment near human body skin, degrease power is low, the performance gentleness can be avoided in the washing process stimulation to skin.
Subacidity skin-moistening synthetic toilet soap of the present invention can adopt the general soapmaking step of common perfumed soap to be prepared:
(a) spice of kneading: the various raw materials of said components are taken by weighing in proportion join in the kneading machine that conventional soapmaking uses, kneading mixes.
(b) mill: the material after mixing will kneaded, enter in the runner milling, carry out soap body and mill.
(c) vacuum press strip: the soap body after will grinding, enter vacuum plodder, carry out the vacuum press strip.
(d) print: the rectangular soap body that plodder extrudes directly enters printer prints, obtains the soap body of moulding.
This Subacidity skin-moistening synthetic toilet soap soap body that adopts the perfumed soap manufacturing step of above-mentioned routine to produce meets the requirements on physical and chemical index fully, in use can be slightly acidic, skin irritation not in washed skin.But soap body occurs sticking with paste mashed, coarse, the surperficial phenomenons such as bubble and Bai Xin that occur of soap body of soap body easily, and outward appearance is not attractive in appearance.
For further improving the over-all properties of Subacidity skin-moistening synthetic toilet soap of the present invention, solve the soap body that exists in the soap body process of manufacture and occur sticking with paste mashed, coarse, the surperficial problems such as bubble and Bai Xin that occur of soap body of soap body easily.Forming in conjunction with soap body material combination of the present invention is based on the on-soap tensio-active agent, and the practical situation that soap body plasticity is less, be not easy to moulding are adjusted targetedly to the processing parameter in the soapmaking step.
The present invention can adopt following steps to be prepared:
(a) the various raw materials of said components are taken by weighing in proportion join in the kneading machine that conventional soapmaking uses, kneading mixes, and the churning time of wherein kneading is that 10～15 minutes, whipping temp are 30～35 ℃.
(b) will knead material after mixing enters in the runner milling, carries out soap body and mills, and the thickness of the back soap flakes of milling is 0.2～0.4 millimeter.
(c) soap body after will grinding enters vacuum plodder, carries out the vacuum press strip, and wherein press strip big gun head temperature out is controlled at 35～40 ℃, and the logical temperature of cooling water of plodder is controlled at 2～10 ℃.
(d) the rectangular soap body of plodder extrusion directly enters printer prints, obtains the soap body of moulding, and the temperature of mould is at-15～-25 ℃ when wherein printing.
Embodiment
Further specify the present invention below by embodiment.
Embodiment 1
The various raw materials of embodiment 1 component corresponding in the table 1 are taken by weighing join in the kneading machine, kneading mixes, and the churning time of kneading is 4 minutes; To knead again material after mixing enters in the runner milling, carries out soap body and mills; Soap body with after grinding enters vacuum plodder, carries out the vacuum press strip, and press strip big gun head temperature out is controlled at 55 ℃, and the logical temperature of cooling water of plodder is controlled at 20 ℃; The rectangular soap body that plodder extrudes directly enters printer prints, and logical refrigerant device is housed in the soap body mould of printer, and mould is cooled off, and promptly obtains this Subacidity skin-moistening synthetic toilet soap.
What this Subacidity skin-moistening synthetic toilet soap adopted is that conventional perfumed soap manufacturing process is produced, and the soap body basic forming that makes meets the requirements on the physical and chemical index fully.But the soap body surface ratio is more coarse, printing effect is relatively poor, outward appearance is not attractive in appearance, and soap body occurs sticking with paste mashed easily after the entry.
The method of pressing defined in the mensuration potentiometry of GB/T6368-93 water phase surfactant mixture pH value is measured the pH value of soap body, has listed test result in table 4.
Embodiment 2
The various raw materials of embodiment 2 components corresponding in the table 1 are taken by weighing join in the kneading machine, kneading mixes, and the churning time of kneading is that 10 minutes, whipping temp are 35 ℃; To knead again material after mixing enters in the runner milling, carries out soap body and mills, and the thickness of the back soap flakes of milling is 0.4 millimeter; Soap body with after grinding enters vacuum plodder, carries out the vacuum press strip, and press strip big gun head temperature out is controlled at 35 ℃, and the logical temperature of cooling water of plodder is controlled at 10 ℃; The rectangular soap body that plodder extrudes directly enters printer prints, and the temperature of mould promptly obtains this Subacidity skin-moistening synthetic toilet soap at-25 ℃ during printing.
What this Subacidity skin-moistening synthetic toilet soap adopted is to produce after existing perfumed soap manufacturing process adjusting process controlled variable, and the complete moulding of the soap body that makes meets the requirements on the physical and chemical index fully.Soap body smooth surface, printing effect are better, aesthetic in appearance, and soap body does not occur sticking with paste mashed after the entry.
In table 4, listed test pH value result.
Embodiment 3
The various raw materials of embodiment 3 components corresponding in the table 1 are taken by weighing join in the kneading machine that conventional soapmaking uses, kneading mixes, and the churning time of kneading is that 15 minutes, whipping temp are 30 ℃; To knead again material after mixing enters in the runner milling, carries out soap body and mills, and the thickness of the back soap flakes of milling is 0.2 millimeter; Soap body with after grinding enters vacuum plodder, carries out the vacuum press strip, and press strip big gun head temperature out is controlled at 40 ℃, and the logical temperature of cooling water of plodder is controlled at 2 ℃; The rectangular soap body that plodder extrudes directly enters printer prints, and the temperature of mould promptly obtains this Subacidity skin-moistening synthetic toilet soap at-15 ℃ during printing.
What this Subacidity skin-moistening synthetic toilet soap adopted is to produce after existing perfumed soap manufacturing process adjusting process controlled variable, and the complete moulding of the soap body that makes meets the requirements on the physical and chemical index fully.Soap body smooth surface, printing effect are better, aesthetic in appearance, and soap body does not occur sticking with paste mashed after the entry.
In table 4, listed test pH value result.
Embodiment 4
The various raw materials of embodiment 4 components corresponding in the table 1 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 2.In table 4, listed test pH value result.
Embodiment 5
The various raw materials of embodiment 5 components corresponding in the table 1 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 3.In table 4, listed test pH value result.
Embodiment 6
The various raw materials of embodiment 6 components corresponding in the table 2 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 2.In table 4, listed test pH value result.
Embodiment 7
The various raw materials of embodiment 7 components corresponding in the table 2 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 3.In table 4, listed test pH value result.
Embodiment 8
The various raw materials of embodiment 8 components corresponding in the table 2 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 2.In table 4, listed test pH value result.
Embodiment 9
The various raw materials of embodiment 9 components corresponding in the table 2 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 3.In table 4, listed test pH value result.
Embodiment 10
The various raw materials of embodiment 10 components corresponding in the table 2 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 2.In table 4, listed test pH value result.
Embodiment 11
The various raw materials of embodiment 11 components corresponding in the table 3 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 3.In table 4, listed test pH value result.
Embodiment 12
The various raw materials of embodiment 12 components corresponding in the table 3 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 2.In table 4, listed test pH value result.
Embodiment 13
The various raw materials of embodiment 13 components corresponding in the table 3 are taken by weighing, produce, obtain this Subacidity skin-moistening synthetic toilet soap according to the method steps of embodiment 3.In table 4, listed test pH value result.
Table 1
| Component/consumption (kilogram) | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| The cocounut oil sodium isethionate | 40 | 50 | 55 | 60 | 53 |
| Sodium lauryl sulphate | 20 | 10 | 8 | 5 | 9 |
| Cocinic acid | 10 | 8 | 5 | 6 | 7 |
| Glycerine | 1 | 0.2 | 2 | 3 | 1.5 |
| Softener sg-6 | 0.5 | 1.5 | 4 | 2.5 | 2 |
| The H501 sequestrant | 0.4 | 0.2 | 0.1 | 0.3 | 0.25 |
| Dextrin | 35 | 10 | 20 | 25 | 23 |
| Water | 3 | 2 | 1 | 5 | 4 |
Table 2
| Component/consumption (kilogram) | Embodiment 6 | Embodiment 7 | Embodiment 8 | Embodiment 9 | Embodiment 10 |
| The cocounut oil sodium isethionate | 60 | 53 | 60 | 53 | 55 |
| Sodium lauryl sulphate | 5 | 9 | 5 | 9 | 8 |
| Cocinic acid | 6 | 7 | 6 | 7 | 5 |
| Glycerine | 3 | 1.5 | 3 | 1.5 | 2 |
| Softener sg-6 | 0 | 2 | 2.5 | 2 | 4 |
| The H501 sequestrant | 0.3 | 0.25 | 0 | 0.25 | 0.1 |
| Dextrin | 25 | 0 | 25 | 13 | 5 |
| Water | 2 | 1 | 3 | 4 | 5 |
| Softener sg-10 | 2.5 | 0 | 0 | 0 | 0 |
| Starch | 0 | 23 | 0 | 10 | 15 |
| EDTA-4Na | 0 | 0 | 0.3 | 0 | 0 |
| Trichlorocarbanilide | 0.2 | 0.8 | 0.5 | 0 | 0 |
Table 3
| Component/consumption (kilogram) | Embodiment 11 | Embodiment 12 | Embodiment 13 |
| The cocounut oil sodium isethionate | 50 | 55 | 53 |
| Sodium lauryl sulfate | 7 | 10 | 9 |
| Cocinic acid | 10 | 5 | 8 |
| Glycerine | 1.5 | 1 | 2 |
| Softener sg-6 | 2.5 | 1.5 | 2 |
| The H501 sequestrant | 0.2 | 0.2 | 0.3 |
| Dextrin | 35 | 10 | 20 |
| Water | 5 | 1 | 4 |
| 10 times of extract solution from aloe | 0.4 | 0.2 | 0.3 |
| Wallantoin | 0.1 | 0.4 | 0.3 |
| The isostearoyl Sodium.alpha.-hydroxypropionate | 0.5 | 2 | 1.5 |
| Lactic acid | 0.2 | 1.2 | 0.8 |
| Titanium dioxide | 0.08 | 0.12 | 0.10 |
| Trichlorine hydroxy diphenyl ether | 0.2 | 0.6 | 0.4 |
| Essence | 1.5 | 1.3 | 1.0 |
Table 4
| PH value | PH value | ||
| Embodiment 1 | 4.7 | Embodiment 8 | 6.2 |
| Embodiment 2 | 5.1 | Embodiment 9 | 5.7 |
| Embodiment 3 | 6.4 | Embodiment 10 | 6.5 |
| Embodiment 4 | 6.1 | Embodiment 11 | 4.5 |
| Embodiment 5 | 5.5 | Embodiment 12 | 6.3 |
| Embodiment 6 | 6.0 | Embodiment 13 | 4.9 |
| Embodiment 7 | 5.6 |
Claims (7)
1. Subacidity skin-moistening synthetic toilet soap, it is characterized in that: it comprises each component of following weight proportion, 40～60 parts in cocounut oil acyloxy ethylsulfonic acid sodium, 5～10 parts of cocinic acids, 5～20 parts of sodium lauryl sulphate, 0.2～3 part of glycerine, 0.5～4 part of softener sg, 0.1～0.4 part of sequestrant, 10～35 parts of weighting agents, 1～5 part of deionized water, described sequestrant are a kind of or its mixture among EDTA-4Na, the H501, and described weighting agent is selected from a kind of or its mixture in sodium sulfate, sodium-chlor, talcum powder, starch, the dextrin.
2. Subacidity skin-moistening synthetic toilet soap according to claim 1 is characterized in that: described softener sg is a softener sg-6.
3. Subacidity skin-moistening synthetic toilet soap according to claim 1 is characterized in that: described weighting agent is a dextrin.
4. Subacidity skin-moistening synthetic toilet soap according to claim 1, it is characterized in that: it comprises that also weight proportion is 1～4 part a skin moisten nutritive ingredient, and described skin moisten nutritive ingredient is a kind of or its mixture in vitamin E, extract solution from aloe, wallantoin, isostearoyl Sodium.alpha.-hydroxypropionate, the lactic acid.
5. Subacidity skin-moistening synthetic toilet soap according to claim 3 is characterized in that: described skin moisten nutritive ingredient component by weight ratio is 0.2～0.4 part of 10 times of extract solution from aloe, 0.1～0.4 part of wallantoin, 0.5～2 part of isostearoyl Sodium.alpha.-hydroxypropionate, 0.2～1.2 part of lactic acid.
6. Subacidity skin-moistening synthetic toilet soap according to claim 1 is characterized in that: it comprises that also weight proportion is 0.2～0.8 part a antiseptic-germicide, and described antiseptic-germicide is a kind of or its mixture in Trichlorocarbanilide, the trichlorine hydroxy diphenyl ether.
7. Subacidity skin-moistening synthetic toilet soap according to claim 1, it is characterized in that: each component that comprises following weight proportion, 50～55 parts in cocounut oil acyloxy ethylsulfonic acid sodium, 5～10 parts of cocinic acids, 7～10 parts of sodium lauryl sulphate, 1～2 part of glycerine, 1.5～2.5 parts of softener sgs, 0.2～0.3 part of H501 sequestrant, 10～35 parts in dextrin, 1～5 part of deionized water, 0.2～0.4 part of 10 times of extract solution from aloe, 0.1～0.4 part of wallantoin, 0.5～2 part of isostearoyl Sodium.alpha.-hydroxypropionate, 0.2～1.2 part of lactic acid, 0.08～0.12 part of titanium dioxide, 0.2～0.6 part of trichlorine hydroxy diphenyl ether antiseptic-germicide, 1.0～1.5 parts in essence.
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| CN101475879B (en) * | 2009-01-19 | 2011-04-06 | 广东拉芳日化有限公司 | Sterilizing skin-protective hand cleanser |
| CN102776087A (en) * | 2012-07-10 | 2012-11-14 | 广东名臣有限公司 | Multifunctional perfumed soap |
| CN102978048A (en) * | 2012-11-16 | 2013-03-20 | 广州伊凡生物科技有限公司 | Weakly acidic transparent soap and preparation method thereof |
| CN104059785A (en) * | 2014-06-20 | 2014-09-24 | 苏州锐耐洁电子科技新材料有限公司 | Nourishing and moistening cleanser |
| CN104232384A (en) * | 2014-09-24 | 2014-12-24 | 上海制皂有限公司 | Hair washing perfumed soap |
| CN104688628A (en) * | 2015-03-24 | 2015-06-10 | 济南玛卡化妆品有限公司 | Faintly acid essential oil hairdressing soap and manufacturing method thereof |
| CN104403855B (en) * | 2014-11-21 | 2017-09-29 | 上海制皂有限公司 | Neutral moistening and cleaning skin perfumed soap |
| CN107881031A (en) * | 2017-11-09 | 2018-04-06 | 杨解定 | The concentration liquid detergent of the aliphatic acid of the oil production containing usefully ditch |
| CN108774609A (en) * | 2018-08-23 | 2018-11-09 | 安庆枝梅化工有限责任公司 | A kind of preparation method of skin care scented soap |
| CN108865543A (en) * | 2018-08-23 | 2018-11-23 | 安庆枝梅化工有限责任公司 | A kind of neutrality skin care scented soap |
| CN109135972A (en) * | 2018-09-21 | 2019-01-04 | 杭州萧山钱江洗涤用品有限公司 | Perfumed soap and its production technology |
| CN109825386A (en) * | 2019-01-29 | 2019-05-31 | 丰益油脂科技（东莞）有限公司 | A kind of neat soap and environment-friendly soap containing Organic grape sodium saccharate |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US5510050A (en) * | 1993-11-08 | 1996-04-23 | The Procter & Gamble Company | Improved acyl isethionate skin cleansing bar containing liquid polyols and magnesium soap |
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| CN101475879B (en) * | 2009-01-19 | 2011-04-06 | 广东拉芳日化有限公司 | Sterilizing skin-protective hand cleanser |
| CN102776087A (en) * | 2012-07-10 | 2012-11-14 | 广东名臣有限公司 | Multifunctional perfumed soap |
| CN102776087B (en) * | 2012-07-10 | 2015-08-12 | 广东名臣有限公司 | Multifunctional fancy soap |
| CN102978048A (en) * | 2012-11-16 | 2013-03-20 | 广州伊凡生物科技有限公司 | Weakly acidic transparent soap and preparation method thereof |
| CN102978048B (en) * | 2012-11-16 | 2014-11-05 | 广州伊凡生物科技有限公司 | Weakly acidic transparent soap and preparation method thereof |
| CN104059785A (en) * | 2014-06-20 | 2014-09-24 | 苏州锐耐洁电子科技新材料有限公司 | Nourishing and moistening cleanser |
| CN104232384B (en) * | 2014-09-24 | 2017-09-29 | 上海制皂有限公司 | Hair washing perfumed soap |
| CN104232384A (en) * | 2014-09-24 | 2014-12-24 | 上海制皂有限公司 | Hair washing perfumed soap |
| CN104403855B (en) * | 2014-11-21 | 2017-09-29 | 上海制皂有限公司 | Neutral moistening and cleaning skin perfumed soap |
| CN104688628A (en) * | 2015-03-24 | 2015-06-10 | 济南玛卡化妆品有限公司 | Faintly acid essential oil hairdressing soap and manufacturing method thereof |
| CN107881031A (en) * | 2017-11-09 | 2018-04-06 | 杨解定 | The concentration liquid detergent of the aliphatic acid of the oil production containing usefully ditch |
| CN108774609A (en) * | 2018-08-23 | 2018-11-09 | 安庆枝梅化工有限责任公司 | A kind of preparation method of skin care scented soap |
| CN108865543A (en) * | 2018-08-23 | 2018-11-23 | 安庆枝梅化工有限责任公司 | A kind of neutrality skin care scented soap |
| CN109135972A (en) * | 2018-09-21 | 2019-01-04 | 杭州萧山钱江洗涤用品有限公司 | Perfumed soap and its production technology |
| CN109825386A (en) * | 2019-01-29 | 2019-05-31 | 丰益油脂科技（东莞）有限公司 | A kind of neat soap and environment-friendly soap containing Organic grape sodium saccharate |
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