CN101122755B - Blue ink powder and its preparation method - Google Patents
Blue ink powder and its preparation method Download PDFInfo
- Publication number
- CN101122755B CN101122755B CN2007101321461A CN200710132146A CN101122755B CN 101122755 B CN101122755 B CN 101122755B CN 2007101321461 A CN2007101321461 A CN 2007101321461A CN 200710132146 A CN200710132146 A CN 200710132146A CN 101122755 B CN101122755 B CN 101122755B
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- Prior art keywords
- blue
- wax
- ink powder
- emulsion polymerization
- granular material
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- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a blue ink power and manufacturing method of ink power. Specifically, the invention is the ink power used for a color copying machine, a color printer, a color facsimile apparatus and a color press and the manufacturing method of the ink power. The invention is made of raw materials such as emulsion polymerization high molecular resin, blue pigment, blue magnetic particle, charge controlling agent, wax, hydrotropism dispersant, silica, hexamethy azane and dimethyl dichlorosilane. The emulsion polymerization high molecular resin, the charge controlling agent, the blue pigment, the blue magnetic particle, the hydrotropism dispersant and the wax are put together to be made into solution by being evenly mixed. The solution is evaporated into granules by a spray dryer under 160 DEG C to 300 DEG C. And then, the granules are selected with the silica, hexamethy azane and the dimethyl dichlorosilane added and evenly mixed, which makes the ink power. The blue ink power has low production cost. In addition, the blue ink power does not cause environmental pollution.
Description
Technical field
The present invention relates to a kind of ink powder and preparation method thereof.Be color copy machine, color printer, colour facsimile apparatus and chromatic printing machine blue ink powder and preparation method thereof specifically.
Background technology
At present, the blue ink powder that uses on color copy machine, color printer, colour facsimile apparatus and the chromatic printing machine all is the emulsion polymerization ink powder.This emulsion polymerization ink powder is mainly made by other auxiliary material such as emulsion, pigment and crosslinking chemical.Its preparation method is that elder generation puts other auxiliary materials such as emulsion, pigment and crosslinking chemical together, through evenly stirring, makes granular material.Then, add acid and washing agent and granular material is cleaned the buoyant on the flush away granular material.Afterwards, the granular material through cleaning is carried out dried.At last, in the granular material that drying was handled, add auxiliary materials such as silicon dioxide, and evenly mix and make.Because this blue ink powder needs to clean with a large amount of clear water in process of production, and one ton of product of every production just needs 50～100 tons of clear water, not only water resource waste is serious, production cost is higher, and the water wasting after cleaning emits, and can pollute environment.
Summary of the invention
The problem to be solved in the present invention provides a kind of blue ink powder.This blue ink powder, not only production cost is low, and can not pollute environment.
Another problem that the present invention will solve provides a kind of preparation method of blue ink powder.
For addressing the above problem, take following technical scheme:
Blue ink powder characteristics of the present invention are the raw materials that contain following weight portion:
70～96 parts of emulsion polymerization macromolecule resins;
0.5～10 part of blue pigment;
0～11 part of blue magnetic;
3～10 parts of charge adjusting agents;
0～5 part in wax;
0～2 part of aqueous dispersion;
0.05～0.6 part of silicon dioxide;
0～3 part of hexamethyldisilazane;
0～3 part of dimethyldichlorosilane;
Wherein: said charge adjusting agent is metal salicylate complex compound or metal azo complex compound; Said wax is any one in polypropylene wax, Tissuemat E or the paraffin; Said aqueous dispersion is methylene two bitter edible plant sodium sulfonates or methyl bitter edible plant sulfonic acid and formaldehyde.
The preparation method of blue ink powder of the present invention contains following steps:
Earlier emulsion polymerization macromolecule resin, charge adjusting agent, blue pigment, blue magnetic, aqueous dispersion and wax are put together, stir, make mixed solution;
Under 160～300 ℃ temperature, above-mentioned mixed solution spraying is dried to granular material with spray dryer again;
Afterwards, above-mentioned granular material is screened, remove particle diameter greater than 13 microns, less than 1 micron particle;
At last, will drop in the mixer, and add silicon dioxide, hexamethyldisilazane and dimethyldichlorosilane,, make blue ink powder through evenly mixing through garbled granular material.
Take above scheme, have the following advantages:
Because blue ink powder of the present invention contains raw materials such as emulsion polymerization macromolecule resin, blue pigment, blue magnetic, charge adjusting agent, wax, aqueous dispersion, silicon dioxide, hexamethyldisilazane and dimethyldichlorosilane, and adopt spray drying process to make, need not clean in the production run, not only can avoid water resource waste, reduced production cost, and the pollution that does not have water wasting to discharge, avoided water wasting that environment is brought.
Embodiment
First embodiment
Choose 96 parts emulsion polymerization macromolecule resin, 7 parts blue pigment, 4 parts charge adjusting agent, 0.05 part silicon dioxide; Wherein: said emulsion polymerization macromolecule resin is west, a Wuxi refreshing cosmetics of everyday use factory product; Said charge adjusting agent is the metal salicylate complex compound;
Earlier emulsion polymerization macromolecule resin, charge adjusting agent and blue pigment are put together, stir, make mixed solution;
Under 250 ℃ temperature, above-mentioned mixed solution spraying is dried to granular material with spray dryer again;
Afterwards, above-mentioned granular material is screened, remove particle diameter greater than 13 microns, less than 1 micron particle;
At last, will drop in the mixer, and add silicon dioxide,, make blue ink powder through evenly mixing through garbled granular material.
Second embodiment
Choose 70 parts emulsion polymerization macromolecule resin, 0.5 blue pigment, 11 parts blue magnetic, 3 parts charge adjusting agent, 1 part wax, 1 part aqueous dispersion, 1.5 parts silicon dioxide, 1 part hexamethyldisilazane and 1.2 parts dimethyldichlorosilane.Wherein: said emulsion polymerization macromolecule resin is the product of west, Wuxi refreshing cosmetics of everyday use factory; Said charge adjusting agent is a metal azo complex compound; Said wax is polypropylene wax; Said aqueous dispersion is methylene two bitter edible plant sodium sulfonates;
Earlier emulsion polymerization macromolecule resin, charge adjusting agent, blue pigment, blue magnetic, aqueous dispersion and wax are put together, stir, make mixed solution;
Under 160 ℃ temperature, above-mentioned mixed solution spraying is dried to granular material with spray dryer again;
Afterwards, above-mentioned granular material is screened, remove particle diameter greater than 13 microns, less than 1 micron particle;
At last, will drop in the mixer, and add silicon dioxide, hexamethyldisilazane and dimethyldichlorosilane,, make blue ink powder through evenly mixing through garbled granular material.
The 3rd embodiment
Choose 85 parts emulsion polymerization macromolecule resin, 10 parts blue pigment, 10 parts charge adjusting agent, 5 parts wax, 2 parts aqueous dispersion, 0.6 part silicon dioxide, 3 parts hexamethyldisilazane and 3 parts dimethyldichlorosilane.Wherein: said emulsion polymerization macromolecule resin is the product of west, Wuxi refreshing cosmetics of everyday use factory; Said charge adjusting agent is the metal salicylate complex compound; Said wax is Tissuemat E; Said aqueous dispersion is a methyl bitter edible plant sulfonic acid and formaldehyde;
Earlier emulsion polymerization macromolecule resin, charge adjusting agent, blue pigment, aqueous dispersion and wax are put together, stir, make mixed solution;
Under 300 ℃ temperature, above-mentioned mixed solution spraying is dried to granular material with spray dryer again;
Afterwards, above-mentioned granular material is screened, remove particle diameter greater than 13 microns, less than 1 micron particle;
At last, will drop in the mixer, and add silicon dioxide, hexamethyldisilazane and dimethyldichlorosilane,, make blue ink powder through evenly mixing through garbled granular material.
Claims (1)
1. the preparation method of a blue ink powder, described blue ink powder contains the raw material of following weight portion:
70～96 parts of emulsion polymerization macromolecule resins;
0.5～10 part of blue pigment;
0～11 part of blue magnetic;
3～10 parts of charge adjusting agents;
0～5 part in wax;
0～2 part of aqueous dispersion;
0.05～0.6 part of silicon dioxide;
0～3 part of hexamethyldisilazane;
0～3 part of dimethyldichlorosilane;
Wherein: said charge adjusting agent is metal salicylate complex compound or metal azo complex compound; Said wax is any one in polypropylene wax, Tissuemat E or the paraffin; Said aqueous dispersion is methylene two bitter edible plant sodium sulfonates or methyl bitter edible plant sulfonic acid and formaldehyde;
Described preparation method may further comprise the steps:
Earlier emulsion polymerization macromolecule resin, charge adjusting agent, blue pigment, blue magnetic, aqueous dispersion and wax are put together, stir, make mixed solution;
Under 160～300 ℃ temperature, above-mentioned mixed solution spraying is dried to granular material with spray dryer again;
Afterwards, above-mentioned granular material is screened, remove particle diameter greater than 13 microns, less than 1 micron particle;
At last, will drop in the mixer, and add silicon dioxide, hexamethyldisilazane and dimethyldichlorosilane,, make blue ink powder through evenly mixing through garbled granular material.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101321461A CN101122755B (en) | 2007-09-24 | 2007-09-24 | Blue ink powder and its preparation method |
| PCT/CN2008/000644 WO2009039717A1 (en) | 2007-09-24 | 2008-03-31 | Colorful toner and a method of preparing the toner |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007101321461A CN101122755B (en) | 2007-09-24 | 2007-09-24 | Blue ink powder and its preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101122755A CN101122755A (en) | 2008-02-13 |
| CN101122755B true CN101122755B (en) | 2010-06-09 |
Family
ID=39085123
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2007101321461A Expired - Fee Related CN101122755B (en) | 2007-09-24 | 2007-09-24 | Blue ink powder and its preparation method |
Country Status (1)
| Country | Link |
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| CN (1) | CN101122755B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009039717A1 (en) * | 2007-09-24 | 2009-04-02 | Jianxin Wang | Colorful toner and a method of preparing the toner |
| JP4660580B2 (en) * | 2008-09-11 | 2011-03-30 | シャープ株式会社 | Toner manufacturing method, toner, developer, developing device, and image forming apparatus |
| CN107305325A (en) * | 2016-04-20 | 2017-10-31 | 天津市有为印刷包装有限公司 | It is a kind of suitable for color toner of high-speed printer and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1996159A (en) * | 2006-12-12 | 2007-07-11 | 王建新 | Blue carbon powder and method for preparing same |
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2007
- 2007-09-24 CN CN2007101321461A patent/CN101122755B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1996159A (en) * | 2006-12-12 | 2007-07-11 | 王建新 | Blue carbon powder and method for preparing same |
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| CN101122755A (en) | 2008-02-13 |
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| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Wuxi Meiling Digital Technology Co., Ltd. Assignor: Wang Jianxin Contract record no.: 2010320000478 Denomination of invention: Blue ink powder and preparation method thereof License type: Exclusive License Open date: 20080213 Record date: 20100427 |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100609 Termination date: 20150924 |
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| EXPY | Termination of patent right or utility model |