CN101108951A - Aquosity bi-component polyurethane coloured paint and method of manufacturing the same - Google Patents
Aquosity bi-component polyurethane coloured paint and method of manufacturing the same Download PDFInfo
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Abstract
The invention discloses a two-component waterborne polyurethane colored paint and the preparation method. The components of the paint are 5 to 15 water, 0.2 to 0.5 dispersant, 0.1 to 0.3 antifoamer, 0.1 to 0.3 wetting agent, 3 to 25 paints, 0 to 50 fillers, 10 to 80 film forming resins, 0 to 5 film forming additives, 0.1 to 0.3 disinfectant, 0.1 to 0.3 antiflash rust agent, 0.5 to 2 thickeners, 1 to 20 hydrophilically-modified polyisocyanate. The preparation method is that water, dispersant, antifoamer, wetting agent, paints and fillers are dispersed evenly by a sand mill, a ball mill or a high-speed stirrer after stirring, and are added with film forming resins, film forming additives, disinfectant, antiflash rust agent and thickeners to gain the product-component A. The hydrophilically-modified polyisocyanate is component B. The component A and component B are mixed uniformly when using. The invention is characterized in that the invention does not adopt organic solvents, does not contain toxic paints and has no harm on the human body and environment, and the properties can reach the solvent two-component polyurethane paint, which can be produced to the primer, intermediate coat and finishing coat, and can be applied in the surface of the wooden ware, cement and metals.
Description
Technical field
The present invention relates to a kind of water-based bi-component polyurethane color paint and preparation method thereof.
Technical background
Polyurethane coating has the performance of many excellences, as strong adhesion, wear resistance is good, elasticity is adjustable, have performances such as excellent acid, alkaline-resisting, high-low temperature resistant simultaneously, therefore obtained using widely at aspects such as national defence, building, chemical industry, vehicle, woodenware, aircrafts.The type and the kind of polyurethane coating are a lot, can be divided into one-can urethane coating and bicomponent polyurethane coating according to packaging type.One-can urethane coating is easy to use, but poor-performing; Bicomponent polyurethane coating, effective chemical is crosslinked owing to having carried out, and paint film property is good.Hydroxyl cure type polyurethane coating is the polyurethane coating of consumption maximum in the market.Component of this coating is to contain polyisocyanate prepolymers, and another component is the hydroxy-containing resin component.Polyurethane coating contains human body and the deleterious volatile organic compounds of environment.Along with the enhancing of people's Environmental awareness and the foundation of various countries' environmental regulation, its application more and more is restricted.And aqueous polyurethane coating, water has replaced poisonous and hazardous organic solvent, have nontoxic, do not fire, free from environmental pollution, save advantage such as the energy, be subjected to people to pay close attention to widely, progressively replace traditional solvent borne polyurethane coating, representing the developing direction of coating industry.The spendable hydroxy-containing component of aqueous polyurethane coating with bi component has the emulsion acrylate polyvalent alcohol and disperses the build polyvalent alcohol, disperses the build polyvalent alcohol can be divided into polyester dispersions, polyethers dispersion, polyurethane dispersions, acrylate dispersoid and acroleic acid polyurethane dispersion etc. again.Aqueous two-component polyurethane varnish document and patent report are more, as CN03811951.X (aqueous two-component polyurethane systems), CN200410027543.9 (aqueous double-component polyurethane wood lacquer and preparation method thereof), CN200510101108.0 (Bicompenent high solid content aqueous polyurethane and preparation method thereof and application), CN200410000762.8 (a kind of aqueous polyurethane coating with bi component and preparation method thereof), CN200410042723.4 (a kind of organic silicon modified aqueous bicomponent polyurethane coating and preparation method thereof).And the prescription and the aspect of performance of research preparation Color paint rarely have report.Aqueous polyurethane varnish purposes is limited, only is used in the woodenware aspect, and safeguards market at building coating and industrial plants, needs a large amount of Color paints.Solvent-type acrylic urethane Color paint occupies a large amount of market shares in this field at present, because the enforcement of national environmental protection rules, require to reduce volatile organic compounds, reduce pollution, so use colored paint replacement solvent-type paint is imperative atmosphere and environment.
Summary of the invention
The purpose of this invention is to provide a kind of water-based bi-component polyurethane color paint and preparation method thereof.
Ultimate principle of the present invention is: with water, dispersion agent, defoamer, wetting agent, after pigment and filler grinding, obtain the water-based hydroxy-containing component with film-forming resin, film coalescence aid, sterilant, the agent of anti-sudden strain of a muscle rust, thickening material after mixing, again with after hydrophilically modified polyisocyanates mixes, because the reaction of hydroxyl and isocyanate groups is main reaction, and the reaction of water and isocyanate groups is less important reaction, obtains water-based bi-component polyurethane color paint.
Particular content of the present invention is:
Water-based bi-component polyurethane color paint its consist of: 5～15 parts in water, 0.2～0.5 part of dispersion agent, 0.1～0.3 part of defoamer, 0.1～0.3 part of wetting agent, 3～25 parts of pigment, 0～50 part of filler, 10～80 parts of film-forming resins, 0～5 part of film coalescence aid, 0.1～0.3 part in sterilant, anti-0.1～0.3 part of agent of rust, 0.5～2 part of thickening material, 1～20 part of the hydrophilically modified polyisocyanates of dodging.
2. the preparation method of water-based bi-component polyurethane color paint is: add film-forming resin, film coalescence aid, sterilant, the agent of anti-sudden strain of a muscle rust, thickening material after water, dispersion agent, defoamer, wetting agent, pigment, filler stirring back are uniformly dispersed with sand mill, ball mill or high speed dispersor, products therefrom is component A; Hydrophilically modified polyisocyanates is a B component, during use component A and B component is mixed to get final product.
Above-mentioned film-forming resin is one or more mixtures in hydroxy acrylate emulsion, water soluble acrylic acid ester dispersion, aqueous polyurethane dispersion, the water soluble acrylic acid polyurethane dispersions.
Above-mentioned pigment is one or more in titanium dioxide, zinc sulfide white, zinc oxide, carbon black, iron oxide red, toluidine red, red, iron oxide yellow, iron oxide black, middle Huang, Hua Lan, phthalocyanine blue, phthalein viridescent, aluminium powder, copper powder, the pigment slurry.
Above-mentioned filler is one or more in lime carbonate, talcum powder, barite, calcium sulfate, mica powder, kaolin, wollastonite powder, zinc powder, zinc phosphate, ferrotitanium powder, the barium metaborate.
Compared with prior art, the present invention has following advantage:
1, the present invention has not with an organic solvent reduced the pollution to human body and environment;
2, the present invention can make color bottom paint, coloured intermediate coat and coloured finish paint, can be used in surfaces such as woodenware, metal, cement;
3, Color paint performance of the present invention can reach solvent-type double-component polyurethane coating performance;
4, the present invention uses conventional paint production plant, need not add new production unit.
5, the present invention uses conventional coating material production raw material, does not need raw material is carried out special processing.
Embodiment
Embodiment 1
13 parts in water, 0.5 part of dispersion agent, 0.2 part of defoamer, 0.3 part of wetting agent, 8 parts of iron oxide red pigments, 7 parts in ferrotitanium powder, 8 parts of talcum powder, 12 parts of backs that stir of barium sulfate are ground to fineness when 60 μ m are following in sand mill, add 45.3 parts of aqueous polyurethane dispersion, 5 parts of film coalescence aid 2-Butoxyethyl acetates, 0.1 part in sterilant, the anti-sudden strain of a muscle obtains 100 parts of component A after 0.5 part of 0.1 part of agent of rust, thickening material stirs, and adds 5 parts of hydrophilically modified polyisocyanates B component during use.This iron oxide red primer coating stirs, and to test its performance as follows for the back brush board: surface drying time 1 hour, do solid work 18 hours time h, hardness 2H, shock strength 50Kg.cm, sticking power 100%, snappiness 1mm, gloss 42,14 days no changes of water tolerance.
Embodiment 2
13 parts in water, 0.5 part of dispersion agent, 0.2 part of defoamer, 0.3 part of wetting agent, 8 parts of iron oxide red pigments, 7 parts in ferrotitanium powder, 8 parts of talcum powder, 12 parts of backs that stir of barium sulfate are ground to fineness when 60 μ m are following in sand mill, add 25.3 parts of aqueous polyurethane dispersion, 20 parts of hydroxyl acrylic emulsions, 5 parts of film coalescence aid 2-Butoxyethyl acetates, 0.1 part in sterilant, the anti-sudden strain of a muscle obtains 100 parts of component A after 0.5 part of 0.1 part of agent of rust, thickening material stirs, and adds 5 parts of hydrophilically modified polyisocyanates B component during use.This iron oxide red primer coating stirs, and to test its performance as follows for the back brush board: surface drying time 1 hour, do solid work 18 hours time, hardness 2H, shock strength 50Kg.cm, sticking power 100%, snappiness 1mm, gloss 35,14 days no changes of water tolerance.
Embodiment 3
11 parts in water, 0.4 part of dispersion agent, 0.2 part of defoamer, 0.1 part of wetting agent, 20.6 parts of backs that stir of titanium dioxide are ground to fineness when 20 μ m are following in sand mill, add 61 parts of hydroxyl acrylic emulsions, 6 parts of film coalescence aid 2-Butoxyethyl acetates, 0.1 part in sterilant, the anti-sudden strain of a muscle obtains 100 parts of component A after 0.5 part of 0.1 part of agent of rust, thickening material stirs, and adds 15 parts of hydrophilically modified polyisocyanates B component during use.This white finish paint coating stirs, and to test its performance as follows for the back brush board: surface drying time 1 hour, do solid work 24 hours time, hardness 2H, shock strength 50Kg.cm, sticking power 100%, snappiness 1mm, gloss 84,72 hours no changes (brush and test) of water tolerance on iron oxide red primer.
Embodiment 4
11 parts in water, 0.4 part of dispersion agent, 0.2 part of defoamer, 0.1 part of wetting agent, 18.6 parts of backs that stir of titanium dioxide are ground to fineness when 20 μ m are following in sand mill, add 61 parts of hydroxyl acrylic emulsions, 6 parts of film coalescence aid 2-Butoxyethyl acetates, 0.1 part in sterilant, the anti-sudden strain of a muscle obtains 100 parts of component A after 2 parts of 0.1 part of agent of rust, 0.5 part of thickening material, black color paste stir, and adds 15 parts of hydrophilically modified polyisocyanates B component during use.This grey finish paint coating stirs, and to test its performance as follows for the back brush board: surface drying time 1 hour, do solid work 24 hours time, hardness 2H, shock strength 50Kg.cm, sticking power 100%, snappiness 1mm, gloss 85, water tolerance 72h no change (brush and test) on iron oxide red primer.
Claims (5)
1. a water-based bi-component polyurethane color paint is characterized in that it consists of: 5～15 parts in water, 0.2～0.5 part of dispersion agent, 0.1～0.3 part of defoamer, 0.1～0.3 part of wetting agent, 3～25 parts of pigment, 0～50 part of filler, 10～80 parts of film-forming resins, 0～5 part of film coalescence aid, 0.1～0.3 part in sterilant, anti-0.1～0.3 part of agent of rust, 0.5～2 part of thickening material, 1～20 part of the hydrophilically modified polyisocyanates of dodging.
2. the preparation method of the described water-based bi-component polyurethane color paint of claim 1, it is characterized in that step is: add film-forming resin, film coalescence aid, sterilant, the agent of anti-sudden strain of a muscle rust, thickening material after water, dispersion agent, defoamer, wetting agent, pigment, filler stirring back are uniformly dispersed with sand mill, ball mill or high speed dispersor, products therefrom is component A; Hydrophilically modified polyisocyanates is a B component, during use component A and B component is mixed to get final product.
3. water-based bi-component polyurethane color paint according to claim 1 and 2 and preparation method thereof is characterized in that described film-forming resin is one or more mixtures in hydroxy acrylate emulsion, water soluble acrylic acid ester dispersion, aqueous polyurethane dispersion, the water soluble acrylic acid polyurethane dispersions.
4. water-based bi-component polyurethane color paint according to claim 1 and 2 and preparation method thereof is characterized in that used pigment is one or more in titanium dioxide, zinc sulfide white, zinc oxide, carbon black, iron oxide red, toluidine red, red, iron oxide yellow, iron oxide black, middle Huang, Hua Lan, phthalocyanine blue, phthalein viridescent, aluminium powder, copper powder, the pigment slurry.
5. water-based bi-component polyurethane color paint according to claim 1 and 2 and preparation method thereof is characterized in that described filler is one or more in lime carbonate, talcum powder, barite, calcium sulfate, mica powder, kaolin, wollastonite powder, zinc powder, zinc phosphate, ferrotitanium powder, the barium metaborate.
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| Application Number | Priority Date | Filing Date | Title |
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| CNA2007101484755A CN101108951A (en) | 2007-08-30 | 2007-08-30 | Aquosity bi-component polyurethane coloured paint and method of manufacturing the same |
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| CNA2007101484755A CN101108951A (en) | 2007-08-30 | 2007-08-30 | Aquosity bi-component polyurethane coloured paint and method of manufacturing the same |
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