CN101059549A - Test apparatus for breakdown strength of material - Google Patents

Test apparatus for breakdown strength of material Download PDF

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Publication number
CN101059549A
CN101059549A CN 200710017877 CN200710017877A CN101059549A CN 101059549 A CN101059549 A CN 101059549A CN 200710017877 CN200710017877 CN 200710017877 CN 200710017877 A CN200710017877 A CN 200710017877A CN 101059549 A CN101059549 A CN 101059549A
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vacuum chamber
xyz
testing apparatus
breakdown strength
anode
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CN 200710017877
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CN100523846C (en
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王发展
原思聪
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Xian University of Architecture and Technology
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Xian University of Architecture and Technology
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Abstract

The invention discloses a tester of material breakage field strength, comprising a XYZ three-coordinate support (1) and a laser ranging device (5), wherein a vacuum room (2) is arranged with the a XYZ three-coordinate support (1) and a fixed anode device (8) fixed with an anode (4), the XYZ three-coordinate support (1) is used to fix the object sample (3) as cathode, the vacuum room (2) is arranged with the laser ranging device (5) outside and vertical to the XYZ three-coordinate support (1), the laser ranging device (5) is communicated with the vacuum room (2). The invention can process accurate adjustment on three-dimension, and accurately measure the breakage distance, with wide application for the accurate tests of breakage field strength and current of metal materials or metal base compound materials, and the generation of cathode spot, and the cathode spot shape real-time watch.

Description

A kind of testing apparatus of breakdown strength of material
Technical field
The present invention relates to a kind of testing apparatus, particularly a kind of testing apparatus of breakdown strength of material.
Background technology
Arc discharge method can be widely used in aspects such as cutting, thermal spray, welding, melting, new material are synthetic, superfine powder preparation, wastewater treatment, space propultion.Negative electrode in the arc plasma generator is the critical component of this system.Negative electrode is being undertaken emitting electrons, and harsh service condition such as high-energy ion bombardment and high temperature ablation is also born in the effect of pilot arc smooth combustion simultaneously, and the weak point in serviceable life that causes because of ablation is its conspicuous contradiction.Therefore, develop and development novel electrode material, satisfy the growth requirement of plasma technique, imperative.The quality of cathode material performance depends on arc starting performance and the arc erosion performance of self.The arc starting performance of cathode material and arc erosion performance then depend primarily on form and the distribution at electrode surface of the electron emissivity of negative electrode and electric arc, and the power of cathode material electron emissivity can be estimated with its vacuum breakdown field intensity.Observe formation, motion and the extinguishing process of cathode protection, can realize by the method for high-speed photography at electrode surface.
In order to develop and develop the novel electrode material, must at first develop the high performance checkout equipment and the method that can be used for estimating the electrode material performance.But, up to the present go back the fairly perfect high precision apparatus of neither one and test above-mentioned performance with exosyndrome material.Therefore, working out the exploitation that precision measurement equipment and corresponding test method can be the novel electrode material provides experiment to support and scientific basis, and can instruct and design the electrode material of new generation with independent intellectual property right.
For the vacuum breakdown performance and the pattern of observing cathode protection of exosyndrome material, present way is that cathode material is to carry out in the TDR-40A vacuum single crystal growing furnace of repacking in the starting the arc field intensity under the little gap of vacuum.Test process is as follows: cathode material is processed to metallographic specimen, puts into vacuum drying oven after the meticulous polishing and makes negative electrode, and anode is made with Φ 2mm pure tungsten, is fixed on the carriage release lever of negative electrode top, and is parallel with cathode plane below.Negative electrode and anode are 5 * 10 -3Be heated to 500 ℃ of insulation 0.5h under the vacuum tightness of Pa to remove surface impurity and adsorbed gas, be cooled to room temperature afterwards in a vacuum.Between negative electrode and anode, add the DC voltage of 8KV, negative electrode is slowly risen with the speed of 0.2mm/min, until the electric arc that ignites, measure at this moment distance between negative electrode with dial gauge near anode between negative electrode and anode, breakdown field strength numerical value is that voltage breakdown is divided by striking distance.Draw back negative electrode and anode, repeat said process.The shortcoming of above-mentioned measuring equipment and method is: the fixed form of negative electrode is simple, and the accurate adjustment that is difficult to it is carried out three-dimensional aligns; Remove sample surfaces impurity and adsorbed gas by the mode that heating under the vacuum is cooled off again, this method needs heating system, and technological process length consuming time, and it is undesirable to remove effect; Adopt traditional turbine and worm gear train, velocity of approach is very fast between the male-female utmost point, and measures distance between negative electrode with dial gauge, and precision is lower; The basic armrest of test process moves and range estimation is carried out, and automation degree of equipment is low; Be not equipped with the CCD camera on the equipment, can not carry out Real Time Observation by the anticathode spot.
The present invention and utilizes computer technology, precise light electrical measurement control techniques on the basis of drawing forefathers' partial test method advantage, invented a kind of full-automatic accurate testing apparatus and corresponding test method by the support of these sophisticated equipments and measuring technology.
Summary of the invention
The technical problem to be solved in the present invention is: a kind of testing apparatus of breakdown strength of material is provided, and the accurate adjustment that this equipment can carry out three-dimensional aligns, and can accurately measure striking distance.
For solving the problems of the technologies described above, the present invention is achieved in that it also comprises XYZ three-dimensional support (1), laser ranging instrument (5), in described vacuum chamber (2), be provided with XYZ three-dimensional support (1) and fixed anode device (8), this fixed anode device (8) is fixed with anode (4), and described XYZ three-dimensional support (1) is used for fixing the tested sample (3) as negative electrode; Perpendicular to XYZ three-dimensional support (1) direction place laser ranging instrument (5) is set outside vacuum chamber (2), laser ranging instrument (5) is communicated with vacuum chamber (2).
For cleaning performance is good, and convenient, outside described vacuum chamber (2), also be provided with Ar +Rifle (15), and be communicated with vacuum chamber (2).
Described laser ranging instrument (5) links to each other with monitor (6), and monitor (6) links to each other with stadimeter control computer (7).
Described vacuum chamber (2) is connected with the vacuum system (9) that is used to vacuumize.
Also be provided with camera (16) outside described vacuum chamber (2), and be communicated with vacuum chamber (2), camera (16) links to each other with stadimeter control computer (7).
Direct supply (14) links to each other with anode (4) with oscillograph (17) respectively.
Described oscillograph (17) is connected with feed system control computer (13).
Described fixed anode device (8) is connected with hydraulic system (10).
In order to make device easy, described fixed anode device (8) can also be connected with stepper motor+ball-screw feed mechanism (18).
The invention has the beneficial effects as follows:
The present invention compared with prior art has the following advantages: this testing apparatus is the instrument of brand-new design; Total system is made up of computing machine and advanced photoelectricity test instrument, and therefore the accuracy of system-wide automaticity height, control accuracy height, data is strong; Measure numerical value and can gather and handle the testing efficiency height in real time; But experimental phenomena Real Time Observation.This invention usable range is extensive, applicable to the breakdown field strength of various metal materials or metal-base composites, the accurate test of breakdown current, and the generating process of cathode protection, the Real Time Observation of cathode protection pattern.
Description of drawings
Fig. 1 is the structural representation of the testing apparatus embodiment 1 of breakdown strength of material of the present invention;
Fig. 2 is the structural representation of the testing apparatus embodiment 2 of breakdown strength of material of the present invention.
Embodiment
Below in conjunction with example the present invention is described in further details:
As shown in Figure 1, a complete set of testing apparatus is by vacuum chamber, XYZ three-dimensional support, laser ranging instrument, CCD camera, monitor, feed system control computer, Ar +Formations such as gun system, oscillograph, CCD camera and stadimeter control computer, hydraulic system, vacuum system, frame, DC power supply.
The present invention is provided with XYZ three-dimensional support 1 and fixed anode device 8 in described vacuum chamber 2, this fixed anode device 8 is fixed with anode 4, and described XYZ three-dimensional support 1 is used for fixing the tested sample 3 as negative electrode; Perpendicular to XYZ three-dimensional support 1 direction place laser ranging instrument 5 is set outside vacuum chamber 2, laser ranging instrument 5 is communicated with vacuum chamber 2.Outside described vacuum chamber 2, also be provided with Ar +Rifle 15, and be communicated with vacuum chamber 2.Described laser ranging instrument 5 links to each other with monitor, and monitor 6 links to each other with stadimeter control computer 7.Also be provided with CCD camera 16 outside described vacuum chamber 2, and be communicated with vacuum chamber 2, CCD camera 16 links to each other with stadimeter control computer 7.Described vacuum chamber 2 should keep higher vacuum tightness, and vacuum tightness is greater than 2 * 10 -3Pa.Direct supply 14 links to each other with fixed anode device 8 with oscillograph 17 respectively.Described fixed anode device 8 is connected with hydraulic system 10.
Its test process is as follows: sample is processed into metallographic specimen, put into vacuum chamber after the meticulous polishing and be fixed on the XYZ three-dimensional support as negative electrode, XYZ three-dimensional support can align negative electrode and anode by adjustment at X, Y, three directional trims of Z, even anode is aimed at the central part of negative electrode.Draw back negative electrode and anode to certain distance, use Ar then +Rifle cleans 5min to remove surface impurity and adsorbed gas.The primer fluid pressing system, under the effect of hydraulic system, anode extremely slowly rises with the speed of 0.01mm/min and near tested sample (negative electrode), punctures when certain distance.Accurately control start and stop time of anode by oscillograph and feed system control computer, promptly when taking place to puncture, when showing a certain amount of electric current when occurring on oscillograph, feed system control computer control feed system stops immediately.Accurately measure distance between anode and negative electrode with the laser ranging instrument, and calculate breakdown field strength immediately by CCD camera and stadimeter control computer.Draw back negative electrode and anode, repeat said process.
The present invention's employing laser range finder of finding range has improved measuring distance greatly; Adopt the argon ion washed samples, cleaning performance is good; Adopt hydraulic system as feed mechanism, can carry out stepless speed regulation, also improved data precision; Adopt XYZ three-dimensional support, make test adjust precision and improve; Be equipped with the CCD camera system, can carry out Real Time Observation by the anticathode spot.
Embodiment 1
The present invention measures W-2%ThO 2Electrode material breakdown field strength process is as follows:
W-2%ThO 2Electrode material is made metallographic specimen to sample again with machining (as line cutting) sampling, put into vacuum chamber after the meticulous polishing and be fixed on the XYZ three-dimensional support, three dimensions fine setting XYZ three-dimensional support make the sample plane level also and anode align.Open vacuum system, make vacuum chamber keep higher vacuum tightness, vacuum tightness is not less than 2 * 10 -3Pa.Start Ar then +The rifle purging system is used Ar +Rifle cleans 5min to remove surface impurity and adsorbed gas.Start the DC adjustable power of direct current, as required voltage is determined at 8000V.Start hydraulic power supply control computer and CCD camera and stadimeter control computer.The primer fluid pressing system, under the effect of hydraulic system and oil cylinder, anode extremely slowly rises with the speed of 0.01mm/min and near tested sample (negative electrode), when certain distance, puncture, accurately control the start and stop time of anode by oscillograph and hydraulic power supply control computer, accurately measure distance between anode and negative electrode with the laser ranging instrument, and calculating breakdown field strength immediately by CCD camera and stadimeter control computer, the breakdown field strength computing formula is the 8000V/ striking distance.Draw back negative electrode and anode, repeat said process.Each sample measurement 100 times, last control computer is drawn breakdown field strength and the relation curve that punctures number of times based on origin software.Utilize the CCD camera system to take the formation of cathode protection, evolution process in real time.
The present invention can test the vacuum breakdown performance of various different materials as required, as W-2%ThO 2The vacuum breakdown performance of electrode material, W-Cu electrode material and other metal-base composites.
Embodiment 2
As shown in Figure 2, other structures are identical with embodiment 1 with test process, fixed anode device 8 is changed into be connected with stepper motor+ball-screw feed mechanism 18.

Claims (9)

1, a kind of testing apparatus of breakdown strength of material, it comprises vacuum chamber (2), it is characterized in that: further comprising XYZ three-dimensional support (1), laser ranging instrument (5), in described vacuum chamber (2), be provided with XYZ three-dimensional support (1) and fixed anode device (8), this fixed anode device (8) is fixed with anode (4), and described XYZ three-dimensional support (1) is used for fixing the tested sample (3) as negative electrode; Perpendicular to XYZ three-dimensional support (1) direction place laser ranging instrument (5) is set outside vacuum chamber (2), laser ranging instrument (5) is communicated with vacuum chamber (2).
2, the testing apparatus of breakdown strength of material according to claim 1 is characterized in that: also be provided with Ar outside described vacuum chamber (2) +Rifle (15)) and be communicated with vacuum chamber (2).
3, the testing apparatus of breakdown strength of material according to claim 1 is characterized in that: described laser ranging instrument (5) links to each other with monitor (6), and monitor (6) links to each other with stadimeter control computer (7).
4, the testing apparatus of breakdown strength of material according to claim 1 is characterized in that: described vacuum chamber (2) is connected with the vacuum system (9) that is used to vacuumize.
5, the testing apparatus of breakdown strength of material according to claim 1 is characterized in that: also be provided with camera (16) outside described vacuum chamber (2), and be communicated with vacuum chamber (2), camera (16) links to each other with stadimeter control computer (7).
6, the testing apparatus of breakdown strength of material according to claim 5 is characterized in that: direct supply (14) links to each other with anode (4) with oscillograph (17) respectively.
7, the testing apparatus of breakdown strength of material according to claim 5 is characterized in that: described oscillograph (17) is connected with feed system control computer (13).
8, according to the testing apparatus of each described breakdown strength of material of claim 1 to 7, it is characterized in that: described fixed anode device (8) is connected with hydraulic system (10).
9, according to the testing apparatus of each described breakdown strength of material of claim 1 to 8, it is characterized in that: described fixed anode device (8) is connected with stepper motor+ball-screw feed mechanism (18).
CNB2007100178771A 2007-05-18 2007-05-18 Test apparatus for breakdown strength of material Expired - Fee Related CN100523846C (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110672992A (en) * 2019-09-27 2020-01-10 清华大学 Electrode material discharge performance testing device and method
CN110850250A (en) * 2019-11-28 2020-02-28 哈尔滨理工大学 Insulating material electric-resistance experiment flat plate electrode device for providing dynamic pressure and experiment method
CN111307861A (en) * 2020-03-18 2020-06-19 浙江大学 Arc ablation test system based on cathode rotation
CN112505455A (en) * 2020-11-26 2021-03-16 国网冀北电力有限公司电力科学研究院 Temperature-based field intensity detection device and method
CN113092968A (en) * 2021-04-14 2021-07-09 哈尔滨理工大学 Automatic testing system for AC/DC breakdown field intensity of film sample

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110672992A (en) * 2019-09-27 2020-01-10 清华大学 Electrode material discharge performance testing device and method
CN110850250A (en) * 2019-11-28 2020-02-28 哈尔滨理工大学 Insulating material electric-resistance experiment flat plate electrode device for providing dynamic pressure and experiment method
CN111307861A (en) * 2020-03-18 2020-06-19 浙江大学 Arc ablation test system based on cathode rotation
CN111307861B (en) * 2020-03-18 2021-04-06 浙江大学 Arc ablation test system based on cathode rotation
CN112505455A (en) * 2020-11-26 2021-03-16 国网冀北电力有限公司电力科学研究院 Temperature-based field intensity detection device and method
CN112505455B (en) * 2020-11-26 2023-08-04 国网冀北电力有限公司电力科学研究院 Temperature-based field intensity detection device and method
CN113092968A (en) * 2021-04-14 2021-07-09 哈尔滨理工大学 Automatic testing system for AC/DC breakdown field intensity of film sample

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