CN101006854B - Preparation method of lycopene powder - Google Patents
Preparation method of lycopene powder Download PDFInfo
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- CN101006854B CN101006854B CN2006100921098A CN200610092109A CN101006854B CN 101006854 B CN101006854 B CN 101006854B CN 2006100921098 A CN2006100921098 A CN 2006100921098A CN 200610092109 A CN200610092109 A CN 200610092109A CN 101006854 B CN101006854 B CN 101006854B
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- oleoresin
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Abstract
The inventive method for producing lycopene powder belongs to the field of food industry and solves the problem of easy oxidation and uneasy use. The method comprises taking lycopene containing lycopene oleoresin 10-50% as raw material, mixing with carrier such as tomato powder, carrot powder or beta-cyclodextrin at a weight ratio of 1:4-1:9, dissolving, harmonizing, vacuum-drying, pulverizing and grading to obtain lycopene powder with lycopene oleoresin 1-10%. It has good fluidity and re-workability; and can be used as colorant and antioxidant of food. It can also be processed into capsule.
Description
One, technical field the invention belongs to field of food industry, and particularly relating to a kind of is the preparation method of the lycopene powder of raw material with the natural lycopene.
Two, background technology lycopene (Lycopene) molecular formula C
40H
56Molecular weight 536.85, different name: lycopene, general structure is by 11 conjugation and 2 linearity hydrocarbons that non-conjugated carbon-carbon double bond is formed, and pure product are needle-like peony crystal, water insoluble, be insoluble in methyl alcohol, ethanol, dissolve in ether, benzinum, hexane, acetone, be soluble in organic solvents such as chloroform, benzene, carbon disulfide, being a kind of fat-soluble natural pigment, is a kind of of carotenoid.Natural lycopene has maximum absorption band at 470nm, can be used as food color, and outstanding anti-oxidation function makes it can play antioxidation as colouring agent the time, is a kind of food additives of promising complex function.Current research is the result show: the lycopene non-oxidizability is very strong, is 100 times of vitamin E, more than 2 times of β-carrotene.Lycopene has multiple biologically active, as cancellation singlet oxygen, removing free radical, inducing cell gap junction communication, regulation and control cancer propagation.Therefore, it is a kind of rising new type functional natural colouring matter, as the food additives with nutrition and painted double action, is widely used in health food, medicine and cosmetic field.But the lycopene oleoresin that content is low is not easy to disperse in the process of food, and the crystalline lycopene of high-load is owing to easily oxidizedly be difficult to preserve and be not used in food.Result of study shows that lycopene in tomato meal processing and storage oxidative degradation and isomerization will take place.In spray-drying process, there is 1.1% lycopene that degraded has taken place approximately, 2.1% lycopene has become cis-isomer.When tomato meal with 37 ℃ of room temperatures under the storage 6 weeks after, the retention rate of lycopene is respectively 70% and 86%.
Three, summary of the invention the purpose of this invention is to provide the preparation method that a kind of content of lycopene is 1～10% lycopene powder, easy oxidation of lycopene and awkward problem have been solved, it is to be that 10～50% lycopene oleoresin is a raw material with content of lycopene, and lycopene oleoresin and carrier carry out successively by weight 1:4～1:9 and following steps:
1. the lycopene raw material is joined alcohol concentration and be in 90% the edible alcohol, make stabilized uniform lycopene alcohol suspension through shearing homogeneous;
2. be that tomato meal or carrot meal or beta-schardinger dextrin-join in the lycopene alcohol suspension according to the above ratio with carrier, to make vector contg be 40～60% mixture through stirring;
3. the mixture that 2. step is made is transferred in the vacuum drying chamber, 40 ℃ ,-remove the alcohol block that must loosen under the condition of 100kpa;
4. it is 1～10% lycopene powder that the loose block crushing and classification of 3. step being made can obtain content.
The lycopene powder of the present invention's preparation has reasonable flowability and cycling processability, can be used as food color and antioxidant and uses, and also can make hard shell capsules.
Four, the preparation of specific embodiment embodiment one 1% lycopene powder, carry out successively according to the following steps:
1. the lycopene oleoresin of 1000g15% is joined alcohol concentration and be in 90% the edible alcohol, make stabilized uniform lycopene alcohol suspension through shearing homogeneous;
2. the 13700g tomato meal is joined in the lycopene alcohol suspension, to make vector contg be 40% mixture through stirring;
3. the mixture that 2. step is made is transferred in the vacuum drying chamber, 40 ℃ ,-remove the alcohol block that must loosen under the condition of 100kpa;
4. the loose block crushing and classification of 3. step being made is made 1% lycopene powder that contains 2% volatile matter.
The preparation of embodiment 2 5% lycopene powders, carry out successively according to the following steps:
1. the lycopene oleoresin of 1000g25% is joined alcohol concentration and be in 90% the edible alcohol, make stabilized uniform lycopene alcohol suspension through shearing homogeneous;
2. the 3900g carrot meal is joined in the lycopene alcohol suspension, to make vector contg be 50% mixture through stirring;
3. the mixture that 2. step is made is transferred in the vacuum drying chamber, 40 ℃ ,-remove the alcohol block that must loosen under the condition of 100kpa;
4. the loose block crushing and classification of 3. step being made is made 5% lycopene powder that contains 2% volatile matter.
The preparation of embodiment 3 10% lycopene powders, carry out successively according to the following steps:
1. 1000950% lycopene oleoresin is joined alcohol concentration and be in 90% the edible alcohol, make stabilized uniform lycopene alcohol suspension through shearing homogeneous;
2. the 3980g beta-schardinger dextrin-is joined in the lycopene alcohol suspension, to make vector contg be 60% mixture through stirring;
3. the mixture that 2. step is made is transferred in the vacuum drying chamber, 40 ℃ ,-remove the alcohol block that must loosen under the condition of 100kpa;
4. the loose block crushing and classification of 3. step being made is made 10% lycopene powder that contains 3% volatile matter.
Claims (2)
1. the preparation method of lycopene powder is characterized in that with content of lycopene being that 10～50% lycopene oleoresin is a raw material, and the weight ratio of lycopene oleoresin and carrier is 1: 4～1: 9, and steps in sequence is as follows:
1. be that 10～50% lycopene oleoresin joins in the edible alcohol with content of lycopene, make stabilized uniform lycopene alcohol suspension through shearing homogeneous;
2. will join in the lycopene alcohol suspension as the tomato meal of carrier or carrot meal or beta-schardinger dextrin-according to the above ratio, to make vector contg be 40～60% mixture through stirring;
3. the mixture that 2. step is made is transferred in the vacuum drying chamber, 40 ℃ ,-remove the alcohol block that must loosen under the condition of 100kpa;
4. it is 1～10% lycopene powder that the loose block crushing and classification of 3. step being made can obtain content.
2. preparation method according to claim 1 is characterized in that edible alcohol concentration is 90%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2006100921098A CN101006854B (en) | 2006-05-27 | 2006-05-27 | Preparation method of lycopene powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2006100921098A CN101006854B (en) | 2006-05-27 | 2006-05-27 | Preparation method of lycopene powder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101006854A CN101006854A (en) | 2007-08-01 |
| CN101006854B true CN101006854B (en) | 2011-08-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2006100921098A Active CN101006854B (en) | 2006-05-27 | 2006-05-27 | Preparation method of lycopene powder |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2310480B1 (en) * | 2007-06-18 | 2010-02-10 | Consejo Superior De Investigaciones Cientificas | MEAT AND FISHING PRODUCTS ENRIQUECIDOS IN LICOPENO THROUGH THE ADDITION OF TOMATO SKIN. |
| CN102885245A (en) * | 2012-10-23 | 2013-01-23 | 新疆中富益健生物科技有限公司 | Lycopene-contained composite microcapsule powder and preparation method thereof |
| CN105942327B (en) * | 2016-05-20 | 2022-12-13 | 江南大学 | Tomato powder product characterized by three highs of lycopene and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1252238A (en) * | 1998-09-14 | 2000-05-10 | Basf公司 | Stable powder tomato red agent preparation containing crystallinity large than 20% tomato red agent |
| CN1472183A (en) * | 2003-06-19 | 2004-02-04 | 上海交通大学 | Preparing method for high-purity lycopene |
-
2006
- 2006-05-27 CN CN2006100921098A patent/CN101006854B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1252238A (en) * | 1998-09-14 | 2000-05-10 | Basf公司 | Stable powder tomato red agent preparation containing crystallinity large than 20% tomato red agent |
| CN1472183A (en) * | 2003-06-19 | 2004-02-04 | 上海交通大学 | Preparing method for high-purity lycopene |
Non-Patent Citations (1)
| Title |
|---|
| 李伟,丁宵霖.番茄红素β-环糊精包合物的制备.<食品科技>.2002,(第10期),39-40,43. * |
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Address after: 831100 No. 333 Wuyidong Road, Changji City, Xinjiang Uygur Autonomous Region Patentee after: COFCO TUNHE SUGAR INDUSTRY CO.,LTD. Address before: 831100 No. 333 Wuyidong Road, Changji City, Xinjiang Uygur Autonomous Region Patentee before: COFCO TUNHE Co.,Ltd. Address after: 831100 No. 333 Wuyidong Road, Changji City, Xinjiang Uygur Autonomous Region Patentee after: COFCO TUNHE Co.,Ltd. Address before: 831100 No. 333 Wuyidong Road, Changji City, Xinjiang Uygur Autonomous Region Patentee before: COFCO XINJIANG TUNHE Co.,Ltd. Address after: 831100 No. 333 Wuyidong Road, Changji City, Xinjiang Uygur Autonomous Region Patentee after: COFCO XINJIANG TUNHE Co.,Ltd. Address before: 831100 No. 333 Wuyidong Road, Changji City, Xinjiang Uygur Autonomous Region Patentee before: Xinjiang Tunhe Investment Co.,Ltd. |
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Effective date of registration: 20190110 Address after: 831100 1st floor w101, 82 blocks, Yutang Village Qiu, Daxiqu Town, Changji City, Xinjiang Uygur Autonomous Region Patentee after: COFCO TUNHE TOMATO Co.,Ltd. Address before: 831100 No. 333 Wuyidong Road, Changji City, Xinjiang Uygur Autonomous Region Patentee before: COFCO TUNHE SUGAR INDUSTRY CO.,LTD. |
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