CN101004403A - Electrolytic cell in use for electrochemical tests - Google Patents

Electrolytic cell in use for electrochemical tests Download PDF

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Publication number
CN101004403A
CN101004403A CN 200610022595 CN200610022595A CN101004403A CN 101004403 A CN101004403 A CN 101004403A CN 200610022595 CN200610022595 CN 200610022595 CN 200610022595 A CN200610022595 A CN 200610022595A CN 101004403 A CN101004403 A CN 101004403A
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CN
China
Prior art keywords
hole
electrolytic cell
cylinder
cover plate
lower cover
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 200610022595
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Chinese (zh)
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CN100520387C (en
Inventor
许哲峰
刘姗
方淑芳
何其平
田冰
张爱萍
郭太雄
张勇刚
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pangang Group Panzhihua Iron and Steel Research Institute Co Ltd
Original Assignee
Pangang Group Panzhihua Iron and Steel Research Institute Co Ltd
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Application filed by Pangang Group Panzhihua Iron and Steel Research Institute Co Ltd filed Critical Pangang Group Panzhihua Iron and Steel Research Institute Co Ltd
Priority to CNB2006100225956A priority Critical patent/CN100520387C/en
Publication of CN101004403A publication Critical patent/CN101004403A/en
Application granted granted Critical
Publication of CN100520387C publication Critical patent/CN100520387C/en
Expired - Fee Related legal-status Critical Current
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Abstract

A PVC electrolyzer used in electrochemical test is prepared for opening round hole with thread at bottom surface of top cover and opening round hole with thread at top surface of bottom cover as well as opening holes at top surface of top cover, arranging thread mating with threads on top and bottom covers at two ends of cylinder, connecting top and bottom covers with middle cylinder by threads.

Description

Electrolytic cell in use for electrochemical tests
Technical field
The present invention relates to electro-chemical test and analyze support equipment, particularly relate to a kind of electrolytic cell in use for electrochemical tests.
Background technology
Electrolytic cell is all used in existing electro-chemical test sheet metal corrosion or the corrosion of plate surface rete.As electrolytic cell Tail Cell K0307 and K0302 that U.S. Princeton Applied Research company produces, this all has introduction in the product manual of www.par-online.com and www.perkinelmer.com website; ZL00214803.X also discloses a kind of electrolytic cell.This class cell operation electrode all is to be placed between the lower nozzle of bottom hardboard and sleeve pipe, when changing sample, all disassemble whole devices, and be difficult to control, and the making of sample and placement are also very time-consuming; In addition, this class electrolytic cell is all by placing working electrode part, salt bridge portion, holding the electrolytic solution part and the placement working electrode is partly formed, connection between the each several part generally all adopts iron and steel parts to fix, as screw, screw rod etc., because electrolytic solution has corrosion to iron and steel parts, thereby damage, influence the serviceable life of electrolytic cell; Also have, this class electrolytic cell in use for electrochemical tests is in test process, and tested sheet coupon all is a mono-sheet, and every survey one less important dismounting once, and is very time-consuming; When analyzing the corrosion of sheet material superficial film continuous position, carry out a large amount of monolithic test jobs, and the monolithic sample because scratching and position problems, shear makes test can not reflect the decay resistance of whole rete fully.
Summary of the invention
Technical matters to be solved by this invention provides a kind of electrolytic cell in use for electrochemical tests, this electrolytic cell convenient disassembly.
The technical scheme that technical solution problem of the present invention is adopted is: electrolytic cell in use for electrochemical tests, cylinder by upper cover plate, lower cover, both end thread is formed, lower surface at upper cover plate has threaded circular hole, upper surface at lower cover has threaded circular hole, upper surface at upper cover plate has hole and hole, the screw thread of upper cover plate, lower cover and the screw thread of cylinder are complementary, and upper cover plate, lower cover and middle cylinder are fitted together by thread set.
The invention has the beneficial effects as follows: the present invention dismantles simply, only needs that the cylinder screw thread is loosened several roads and gets final product, and is simple to operate; The present invention all adopts the PVC member to form, and has avoided irony screw and screw rod to get rusty in the salt environment in use, and prolong serviceable life greatly; It is that two directions connect that the present invention places the working electrode position, the working electrode sample can be made into rectangular sample, is placed on the electrolytic cell below, tests successively along the band sample direction, when analyzing the corrosion of sheet material superficial film continuous position, test result can reflect the decay resistance of whole rete.
Description of drawings
Fig. 1 is the cut-open view of upper cover plate of the present invention.
Fig. 2 is the cut-open view of lower cover of the present invention.
Fig. 3 is the cut-open view of duty of the present invention.
Embodiment
The present invention is made up of the cylinder 7 of upper cover plate 8, lower cover 9, both end thread.Lower surface at upper cover plate 8 has threaded circular hole 3, has hole 1 and hole 2 at the upper surface of upper cover plate 8, and hole 1 and hole 2 preferably are set to strip hole 1 and circular hole 2 respectively, place auxiliary electrode and contrast electrode respectively.Sidewall at lower cover 9 laterally has through hole 5, be used for placing the sheet coupon 10 (working electrode) that to test, upper surface at lower cover 9 has threaded circular hole 4, the screw thread of the screw thread of upper cover plate 8, lower cover 9 and cylinder 7 is complementary, and upper cover plate 8, lower cover 9 and middle cylinder 7 are tightened by screw thread and fitted together.
The material of upper cover plate 8, lower cover 9 and cylinder 7 all adopts the PVC material to make, and also is provided with packing washer 6 in cylinder 7 bottoms, is used for preventing that electrolytic solution from flowing out, the influence test.
During test, earlier sheet coupon 10 to be measured is passed the through hole 5 on the lower cover 9, then, PVC cylinder 7 lower ends that will have O-ring seal 6 are screwed into threaded circular hole 4 places on the lower cover 9, and cylinder 7 bottoms are closely contacted with sample 10 on the lower cover 9, then, again threaded circular hole 3 places on the upper cover plate 8 and PVC cylinder 7 upper ends are tightened, in cylinder 7, pour electrolyte solution into again, insert auxiliary electrode at strip hole 1 place, circular hole 2 places insert contrast electrode, turn on the electricity and just can carry out electro-chemical test.
Strip hole 1 can be used for regulating the distance of auxiliary electrode and contrast electrode, reaches best test effect.Auxiliary electrode and contrast electrode and lie in the distance adjustment of the sheet coupon 10 at through hole 5 places, can use wood clamp to block (because test unit precision, the bore of strip hole 1 and circular hole 2 and the bore of electrode coupling also can be regulated height up and down without clip) electrode, reach the purpose of adjusting.

Claims (5)

1, electrolytic cell in use for electrochemical tests, it is characterized in that: the cylinder (7) by upper cover plate (8), lower cover (9), both end thread is formed, lower surface at upper cover plate (8) has threaded circular hole (3), upper surface at lower cover (9) has threaded circular hole (4), upper surface at upper cover plate (8) has hole (1) and hole (2), the screw thread of the screw thread of upper cover plate (8), lower cover (9) and cylinder (7) is complementary, and upper cover plate (8), lower cover (9) and middle cylinder (7) are fitted together by thread set.
2, electrolytic cell in use for electrochemical tests as claimed in claim 1 is characterized in that: described hole (1) and hole (2) is respectively strip hole (1) and circular hole (2).
3, electrolytic cell in use for electrochemical tests as claimed in claim 1 is characterized in that: the sidewall at described lower cover (9) laterally has through hole (5).
4, electrolytic cell in use for electrochemical tests as claimed in claim 1 is characterized in that: be provided with packing washer (6) in described cylinder (7) bottom.
5, electrolytic cell in use for electrochemical tests as claimed in claim 1 is characterized in that: the material of described upper cover plate (8), lower cover (9) and cylinder (7) adopts the PVC material to make.
CNB2006100225956A 2006-12-22 2006-12-22 Electrolytic cell in use for electrochemical tests Expired - Fee Related CN100520387C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2006100225956A CN100520387C (en) 2006-12-22 2006-12-22 Electrolytic cell in use for electrochemical tests

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2006100225956A CN100520387C (en) 2006-12-22 2006-12-22 Electrolytic cell in use for electrochemical tests

Publications (2)

Publication Number Publication Date
CN101004403A true CN101004403A (en) 2007-07-25
CN100520387C CN100520387C (en) 2009-07-29

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CNB2006100225956A Expired - Fee Related CN100520387C (en) 2006-12-22 2006-12-22 Electrolytic cell in use for electrochemical tests

Country Status (1)

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CN (1) CN100520387C (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101788523A (en) * 2010-02-01 2010-07-28 南京星银药业集团有限公司 On-line detecting device of electrochemical process product
CN102426183A (en) * 2011-11-12 2012-04-25 重庆理工大学 Corrosion and degradation experiment device for external medical metal body in dynamic corrosion environment
CN102590299A (en) * 2012-01-10 2012-07-18 中国科学院海洋研究所 Combined electrolytic cell
CN101377539B (en) * 2007-08-29 2013-08-28 深圳市比克电池有限公司 Electrolytic cell for battery electrochemical measuring
CN103604741A (en) * 2013-11-14 2014-02-26 国家电网公司 Electrolytic cell device based on online electrochemical measurement of power transmission line
CN103969472A (en) * 2014-05-28 2014-08-06 国家电网公司 In situ observation device and method of pitting forming process
CN105424773A (en) * 2015-11-05 2016-03-23 中国石油天然气股份有限公司 Electrolytic tank for soil corrosion electrochemical experiment
CN105758906A (en) * 2016-04-18 2016-07-13 青岛科技大学 Electrochemical testing device

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD122284A1 (en) * 1975-11-10 1976-09-20
SU938106A1 (en) * 1980-12-30 1982-06-23 Всесоюзный Научно-Исследовательский Институт По Защите Металлов От Коррозии Cell for corrosive and electrochemical testing of metals under load
DD272512A1 (en) * 1988-06-02 1989-10-11 Medizin Labortechnik Veb K COULOMETRIC MEASURING CELL
US6015479A (en) * 1997-07-25 2000-01-18 The United States Of America As Represented By The Secretary Of The Navy Thin-layer spectroelectrochemical cell
CN1081329C (en) * 1998-12-18 2002-03-20 厦门大学 Portable fast testing system for coating and metal corrosion resistance
CN2421646Y (en) * 2000-05-18 2001-02-28 中国科学院海洋研究所 Coating detecting electrolyzer
CN1334455A (en) * 2000-07-14 2002-02-06 中国科学院力学研究所 Ultrasonic method and equipment for testing resistance of material to corrosion and abrasion

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101377539B (en) * 2007-08-29 2013-08-28 深圳市比克电池有限公司 Electrolytic cell for battery electrochemical measuring
CN101788523A (en) * 2010-02-01 2010-07-28 南京星银药业集团有限公司 On-line detecting device of electrochemical process product
CN102426183A (en) * 2011-11-12 2012-04-25 重庆理工大学 Corrosion and degradation experiment device for external medical metal body in dynamic corrosion environment
CN102426183B (en) * 2011-11-12 2014-01-15 重庆理工大学 Corrosion and degradation experiment device for external medical metal body in dynamic corrosion environment
CN102590299A (en) * 2012-01-10 2012-07-18 中国科学院海洋研究所 Combined electrolytic cell
CN102590299B (en) * 2012-01-10 2014-02-26 中国科学院海洋研究所 Combined electrolytic cell
CN103604741A (en) * 2013-11-14 2014-02-26 国家电网公司 Electrolytic cell device based on online electrochemical measurement of power transmission line
CN103969472A (en) * 2014-05-28 2014-08-06 国家电网公司 In situ observation device and method of pitting forming process
CN105424773A (en) * 2015-11-05 2016-03-23 中国石油天然气股份有限公司 Electrolytic tank for soil corrosion electrochemical experiment
CN105758906A (en) * 2016-04-18 2016-07-13 青岛科技大学 Electrochemical testing device

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Granted publication date: 20090729

Termination date: 20091222