CN100999747A - Preparation process of syrup special for yellow wine - Google Patents
Preparation process of syrup special for yellow wine Download PDFInfo
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- CN100999747A CN100999747A CN 200610166245 CN200610166245A CN100999747A CN 100999747 A CN100999747 A CN 100999747A CN 200610166245 CN200610166245 CN 200610166245 CN 200610166245 A CN200610166245 A CN 200610166245A CN 100999747 A CN100999747 A CN 100999747A
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Abstract
The process of preparing syrup specially for yellow wine with corn starch as material includes adding heat resistant alpha-amylase into corn starch milk, continuous spray liquification, saccharifying, decolorizing, concentrating and refining. The process is one multiple enzyme hydrolysis one with controlled sugar component, and the syrup specially for yellow wine has proper amount of amino nitrogen for meeting the requirement as yellow wine producing yeast. The syrup specially for yellow wine can replace partial rice for producing yellow wine, and results in low power consumption, less sewage drainage, raised yellow wine yield and lowered yellow wine producing cost.
Description
Technical field
The present invention relates to a kind of preparation method of syrup special for yellow wine, belong to the production technical field of syrup special for yellow wine.
Background technology
Yellow rice wine is national special product and traditional drink of China, also is one of the most ancient in the world alcoholic drink, and as the peculiar wine kind of the Chinese nation, its alcoholic strength is submissive, and the wine body is plentiful, and vinosity is mellow, has embodied the inherent honest and sincere of Chinese nation, and residence has just given gentle cultural spirit.
According to the Tenth Five-Year Plan (2001-2005) and 2015 planning, yellow rice wine output will be increased to ten thousand tons of 250-280 in 2015 from 1,450,000 tons in 2000.In the 3rd board of management of Wine Industry Association that held in 2005, meeting proposes yellow rice wine export amount to 2015 and year increased by 100% target than 2000.
The consumption burden of taxation of yellow rice wine in various alcohol products is the lightest at present, has embodied the support of country to the yellow rice wine industry.According to the authoritative department prediction, by 2015, yellow rice wine consumption will reach 2.65 liters per capita, be equivalent to present liquor per capita consuming level, and the yellow rice wine market of China will reach 3,600,000 kilolitres.
The yellow rice wine of China began to reverse in 2003 after the experience low ebb, and market and output are all progressively increasing.Yellow rice wine output was 1,800,000 tons in 2004,37.7 hundred million yuan of whole industry sales revenue, and 2.98 hundred million yuan of total profits increase by 10.23% and 14.18% on a year-on-year basis.Yellow rice wine also progressively squeezes into the international market, and export volume also increases year by year, and the export volume of yellow rice wine in 2004 has increased about 20% on year-on-year basis.China's yellow rice wine output reached 2,000,000 tons in 2005, and China's yellow rice wine output in 2006 is estimated to reach 2,100,000 tons, and the yellow rice wine industry is just being stepped into a new growth stage.
The main raw material of China's rice wine production south glutinous rice, polished rice and long-grained nonglutinous rice are northern with milled glutinous broomcorn millet, maize and corn at present.In recent years, along with the support on policy of country to agricultural, the price increase of agricultural-food particularly in today that the yellow rice wine market competition is growing more intense, brings white elephant for rice wine production enterprise.Calculate according to present yellow rice wine liquor ratio of raw material 275% (14.5v/v), the yellow rice wine annual production was by 2,000,000 tons of calculating in 2005, and China's year is consumed about 730,000 tons of rice, accounts for 2.5% of China's rice output.
Summary of the invention
The present invention is based on the common development of Dian Fentang industry and yellow rice wine industry, make full use of the advantage of producing starch syrup, enterprise reaches mutual supplement with each other's advantages with rice wine production.According to rice wine production characteristics and processing requirement, a kind of syrup special for yellow wine of suitable rice wine production is provided, can significantly improve the consumption of liquor ratio of raw material, optimization production technology, minimizing water power vapour when being used for rice wine production, reduce sewage discharge, reduce production costs.
Technical assignment of the present invention provides a kind of preparation method of syrup special for yellow wine, and with the syrup special for yellow wine of this method preparation.
Technical scheme of the present invention is as follows:
A kind of preparation method of syrup special for yellow wine, comprise size mixing, liquefaction, saccharification, decolouring and enrichment step, it is characterized in that, with the W-Gum is that raw material is sized mixing, add high temperature resistant α-Dian Fenmei 400～800ml/T (butt starch) in the W-Gum Ruzhong of 16～19 ° of Be ' of concentration (degree Beaume) and carry out continuous injection liquefaction, 70～110 ℃ of temperature, time 20～120min.
Preferably, control saccharification temperature in the above-mentioned saccharification step: 60 ℃ ± 2 ℃, add fungal enzyme and Pullulanase 300-500ml/T (butt sugar), the volume ratio of fungal enzyme and Pullulanase is (2: 0.5-1); Saccharification time: 60-72h, and then add neutral protease, dosage is 30-40ml/T (a butt sugar), transfers pH=5.6-7.0, hydrolysis 20-50min.
Preferably, the condition that above-mentioned saccharification liquid is decoloured is: activated carbon dosage is a 1.5-5.0kg/ ton butt syrup, bleaching temperature 60-70 ℃, decolours 20-40 minute.Filter.
Preferably, it is 75-80% that the filtered liquid after the above-mentioned decolouring is adopted falling film type triple effect vacuum-evaporator evaporation concentration to concentration, gets syrup special for yellow wine.
Adopt the advantage of falling film type triple effect vacuum-evaporator to be, each vacuum tightness of imitating of vacuum-evaporator is higher in concentration process, liquid glucose just can reach boiling state in lower temperature, has avoided liquid glucose when high temperature and proteinic metachromasia, guarantees the syrupy quality of finished product.
The syrup special for yellow wine that the inventive method is prepared, its characteristics are that contents of monosaccharides is few, infiltration is forced down when being used for rice wine production, does not influence zymic growth and fermentation; And contain an amount of amino nitrogen, fatty hardly; The pH value that suitable yellow wine fermentation requirement is arranged; Fermentable sugar content height.Concrete index sees attached list 1 and 2.
The Oranoleptic indicator of table 1 syrup special for yellow wine
| Project | Requirement |
| Outward appearance | Thick transparent liquid, the visible impurity of no naked eyes |
| Smell | Has the due fragrance of this product |
| Flavour | Sweet taste gentleness, pure, free from extraneous odour |
| Color and luster | Colourless or little yellow |
The physical and chemical index of table 2 syrup special for yellow wine
| Project | Unit | Index |
| Solid substance | ％ | ≥75 |
| The DE value | ％ | ≥42 |
| PH value | 4.0-6.0 | |
| Sulphated ash | ％ | ≤0.6 |
| Amino nitrogen content | mg/l | ≥50 |
| Plumbous (in pb) | Mg/kg | ≤0.5 |
| Arsenic (in As) | Mg/kg | ≤0.5 |
| Coliform | Individual/100g | ≤30 |
| Total plate count | Individual/g | ≤2000 |
| Pathogenic bacterium (Salmonellas) | Must not detect |
The present invention a kind ofly prepares the processing method of syrup special for yellow wine with W-Gum, and W-Gum is used high-temperature, Pullulanase, fungal enzyme, neutral proteinase hydrolysis successively; And control proper hydrolyzing condition and zymin addition, guarantee the suitable sugar component and the content of amino nitrogen; With the refining syrup special for yellow wine that is condensed into of hydrolyzed solution.The processing method of this syrup special for yellow wine adopts multi-enzymatic hydrolysis, control suitable sugar component, and give this syrup special for yellow wine an amount of amino nitrogen, can satisfy the saccharomycetic demand of rice wine production, can partly substitute brewing yellow rice wine raw material rice, cut down the consumption of energy, reduce sewage discharge, improve liquor ratio of raw material, optimize yellow wine production technology, reduce labor intensity, help more the mechanize production of yellow rice wine, and reduce the production cost of yellow rice wine, have higher social utility and be worth.
Advantage of the present invention and positively effect are that the product that adopts this method to produce has following advantage when being used for rice wine production:
1. can carry out brewing yellow rice wine by equivalent replacement part rice raw material, and improve liquor ratio of raw material, not influence yellow rice wine and ferment normally, and easy to use;
2. energy-saving effect is obvious, mainly shows to save to soak rice, wash rice and to drench a rice water, saves to steam rice and use steam, has reduced sewage discharge;
3. optimization production technology reduces labor intensity, and helps the mechanize production of yellow rice wine more;
4. reduced the production cost of yellow rice wine, economic benefit and obvious social benefit;
5. the crisis in food of China is alleviated in the appearance of syrup special for yellow wine, has promoted the common development of Dian Fentang industry and yellow rice wine industry.
Embodiment
The present invention will be further described below in conjunction with embodiment, but be not limited thereto.
Embodiment 1: the preparation method of syrup special for yellow wine, and step is as follows:
(1) sizes mixing and liquefy
Is 18.5 ° of Be ' (degree Beaume) with W-Gum with clear water furnishing concentration, and adjust pH is 5.9, adds high temperature resistant α-Dian Fenmei 700ml/T (butt starch), and 90 ℃ are carried out continuous injection liquefaction, time 60min.
(2) saccharification
Above-mentioned liquefier is cooled to 60 ℃ with plate-type heat exchanger or vacuum cooler, presses 350ml/ ton (butt sugar) then and add fungal enzyme and Pullulanase, the volume ratio of fungal enzyme and Pullulanase is 2: 0.75; Saccharification time: 68h, and then add neutral protease, dosage is 30ml/T (a butt sugar), transfers pH=6.5, hydrolysis 30min.
(3) saccharification liquid decolouring
After above-mentioned saccharification finished, after saccharification liquid removed the albumen slag after filtration, the gac that adds 3kg/ ton (butt syrup) decoloured, 65 ℃ of bleaching temperatures, decolouring 30min after-filtration.
(4) evaporation concentration
It is 75% that above-mentioned filtered liquid is adopted falling liquid film triple effect vacuum-evaporator evaporation concentration to concentration, obtains the finished product syrup special for yellow wine, and its amino nitrogen content is more than 50mg/kg, and sugar component meets the requirements.
Embodiment 2:
(1) sizes mixing and liquefy
Is 19 ° of Be ' (degree Beaume) with W-Gum with clear water furnishing concentration, and adjust pH is 6.0, adds high temperature resistant α-Dian Fenmei 600ml/T (butt starch), and 100 ℃ are carried out continuous injection liquefaction, time 50min.
(2) saccharification
Liquefier is cooled to 59 ℃ with plate-type heat exchanger or vacuum cooler, presses 450ml/ ton (butt sugar) then and add fungal enzyme and Pullulanase, the volume ratio of fungal enzyme and Pullulanase is 2: 1; Saccharification time: 60h, and then add neutral protease, dosage is 40ml/T (a butt sugar), transferring pH is 7.0, hydrolysis 20min.
(3) saccharification liquid decolouring
After saccharification finished, after saccharification liquid removed the albumen slag after filtration, the gac that adds 3.4kg/ ton (butt syrup) decoloured, 70 ℃ of bleaching temperatures, decolouring 20min after-filtration.
(4) determine evaporating and concentrating process:
It is 80% that filtered liquid is adopted falling liquid film triple effect vacuum-evaporator evaporation concentration to concentration, obtains the finished product syrup special for yellow wine, and its amino nitrogen content is more than 50mg/kg, and sugar component meets the requirements.
Claims (5)
1. the preparation method of a syrup special for yellow wine, through size mixing, liquefaction, saccharification, decolouring and enrichment step, it is characterized in that, with the W-Gum is that raw material is sized mixing, liquefaction step is to add high temperature resistant α-Dian Fenmei 400～800ml/T (butt starch) to carry out continuous injection liquefaction in the W-Gum Ruzhong of 16～19 ° of Be ' of concentration (degree Beaume), 70～110 ℃ of temperature, time 20～120min.
2, the preparation method of syrup special for yellow wine as claimed in claim 1, it is characterized in that controlling in the described saccharification step saccharification temperature: 60 ℃ ± 2 ℃, add fungal enzyme and Pullulanase 300-500ml/T (butt sugar), the volume ratio of fungal enzyme and Pullulanase is 2: 0.5-1; Saccharification time: 60-72h, and then add neutral protease, dosage is 30-40ml/T (a butt sugar), transfers pH=5.6-7.0, hydrolysis 20-50min.
3, the preparation method of syrup special for yellow wine as claimed in claim 1 is characterized in that the condition that saccharification liquid decolours being: activated carbon dosage is a 1.5-5.0kg/ ton butt syrup, bleaching temperature 60-70 ℃, decoloured 20-40 minute, and filter.
4, the preparation method of syrup special for yellow wine as claimed in claim 1 is characterized in that adopting the vacuum-evaporation of falling film type triple effect to be concentrated into concentration the filtered liquid after the decolouring is 75-80%.
5, the syrup special for yellow wine that obtains by claim 1 preparation method.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2006101662457A CN100554434C (en) | 2006-12-25 | 2006-12-25 | The preparation method of syrup special for yellow wine |
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2006101662457A CN100554434C (en) | 2006-12-25 | 2006-12-25 | The preparation method of syrup special for yellow wine |
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| CN100999747A true CN100999747A (en) | 2007-07-18 |
| CN100554434C CN100554434C (en) | 2009-10-28 |
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| CNB2006101662457A Expired - Fee Related CN100554434C (en) | 2006-12-25 | 2006-12-25 | The preparation method of syrup special for yellow wine |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102334631A (en) * | 2011-08-09 | 2012-02-01 | 山东省鲁洲食品集团有限公司 | Method for preparing special corn starch syrup for moon cake |
| CN105062813A (en) * | 2015-07-25 | 2015-11-18 | 安徽陈瑶湖黄酒有限公司 | Preparation method of yin-nourishing and health-care yellow wine |
| CN105062811A (en) * | 2015-07-25 | 2015-11-18 | 安徽陈瑶湖黄酒有限公司 | Preparation method of aloe yellow rice wine capable of maintaining beauty |
| CN105062812A (en) * | 2015-07-25 | 2015-11-18 | 安徽陈瑶湖黄酒有限公司 | Preparation method of wind-dispelling and intestine-moistening wheat-flavored yellow wine |
| CN105087312A (en) * | 2015-07-25 | 2015-11-25 | 安徽陈瑶湖黄酒有限公司 | Preparation method of stomach nourishing peanut yellow wine |
| CN105087313A (en) * | 2015-07-25 | 2015-11-25 | 安徽陈瑶湖黄酒有限公司 | Preparation method of fragrant and sweet pawpaw yellow rice wine capable of tonifying kidney |
| CN112175768A (en) * | 2020-11-09 | 2021-01-05 | 常宁超喜欢食品有限公司 | Yellow wine production process method |
-
2006
- 2006-12-25 CN CNB2006101662457A patent/CN100554434C/en not_active Expired - Fee Related
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102334631A (en) * | 2011-08-09 | 2012-02-01 | 山东省鲁洲食品集团有限公司 | Method for preparing special corn starch syrup for moon cake |
| CN102334631B (en) * | 2011-08-09 | 2012-12-26 | 山东省鲁洲食品集团有限公司 | Method for preparing special corn starch syrup for moon cake |
| CN105062813A (en) * | 2015-07-25 | 2015-11-18 | 安徽陈瑶湖黄酒有限公司 | Preparation method of yin-nourishing and health-care yellow wine |
| CN105062811A (en) * | 2015-07-25 | 2015-11-18 | 安徽陈瑶湖黄酒有限公司 | Preparation method of aloe yellow rice wine capable of maintaining beauty |
| CN105062812A (en) * | 2015-07-25 | 2015-11-18 | 安徽陈瑶湖黄酒有限公司 | Preparation method of wind-dispelling and intestine-moistening wheat-flavored yellow wine |
| CN105087312A (en) * | 2015-07-25 | 2015-11-25 | 安徽陈瑶湖黄酒有限公司 | Preparation method of stomach nourishing peanut yellow wine |
| CN105087313A (en) * | 2015-07-25 | 2015-11-25 | 安徽陈瑶湖黄酒有限公司 | Preparation method of fragrant and sweet pawpaw yellow rice wine capable of tonifying kidney |
| CN112175768A (en) * | 2020-11-09 | 2021-01-05 | 常宁超喜欢食品有限公司 | Yellow wine production process method |
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| Publication number | Publication date |
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| CN100554434C (en) | 2009-10-28 |
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Owner name: LUZHOU BIO-CHEM. TECHNOLOGY (SHAANXI) CO., LTD. Free format text: FORMER OWNER: WANG DEYOU Effective date: 20111013 |
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Free format text: CORRECT: ADDRESS; FROM: 276400 LINYI, SHANDONG PROVINCE TO: 713100 XIANYANG, SHAANXI PROVINCE |
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Effective date of registration: 20111013 Address after: 713100, 54, Yu Xing Road, Xingping, Shaanxi, Xianyang Patentee after: Lu Zhou Biotechnology (Shaanxi) Co., Ltd. Address before: 276400 No. 18, Lu Chau Road, Yishui County, Shandong Province Patentee before: Wang Deyou |
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