CN100546925C - Utilize the method that fluidized-bed process disposes of sewage and the preparation method of organism compatibility filling and filler thereof - Google Patents
Utilize the method that fluidized-bed process disposes of sewage and the preparation method of organism compatibility filling and filler thereof Download PDFInfo
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- CN100546925C CN100546925C CNB2006101519035A CN200610151903A CN100546925C CN 100546925 C CN100546925 C CN 100546925C CN B2006101519035 A CNB2006101519035 A CN B2006101519035A CN 200610151903 A CN200610151903 A CN 200610151903A CN 100546925 C CN100546925 C CN 100546925C
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
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Abstract
The invention discloses a kind of method that fluidized-bed process disposes of sewage and preparation method of organism compatibility filling and filler thereof of utilizing, this method may further comprise the steps: filled biomass compatibility filling in fluidized-bed, pretreated sewage in regular turn through the anaerobism pulsed fluidized bed oxygen cycle fluidized-bed of becoming reconciled, is carried out biochemical treatment; At last, the sewage of carrying out a biological disposal upon is carried out mud-water separation by second pond or air supporting, and when being necessary, carry out aftertreatment as disinfecting, to reach emission standard.Mud is entered sludge thickener or is back to anaerobic pond, Aerobic Pond.Described organism compatibility filling main component comprises urethane, rare earth metal and ferrous oxide.Add organism compatibility filling in the fluidized-bed, increased the biomass in the biochemical system, improved biochemical treatment system clearance, increased system's operation stability, can reduce the activated sludge bulking phenomenon effectively, and greatly improve the nitric efficiency of system.
Description
Technical field
The present invention relates to a kind of processing method of sewage disposal and the preparation method of filler and filler thereof.
Background technology
In the existing sewage biochemical processing process, the method for being used always mainly contains activated sludge process and biological contact oxidation process, and it handles mechanism all is to utilize the biological bacterium in the sewage that the organic pollutant in the sewage is decomposed into carbonic acid gas CO
2With water H
2O realizes the purification to sewage.
But all there is weak point in these two kinds of methods: 1) the biochemical system pollutant load is relatively low, and impact resistance is less; 2) thread fungus easily being taken place expands the operational management difficulty; Clearance is lower during organic waste water that 3) concentration of treatment is relatively very low or very high; 4) system's denitrification effect is relatively poor.
Summary of the invention
Provide a kind of system stability, treatment effect excellence for the shortcoming that overcomes prior art, be easy to the method for utilizing fluidized-bed process to dispose of sewage of operational management.
Another object of the present invention is to provide a kind of organism compatibility filling and preparation method thereof, improved clearance, the increase system operation stability of sewage biochemical treatment system.
For solving the problems of the technologies described above, technical scheme of the present invention is that the method for utilizing fluidized-bed process to dispose of sewage may further comprise the steps:
(1) dose the high-performance bio compatibility filling in pulsed fluidized bed He in the circulating fluidized bed, sewage is introduced into pulsed fluidized bed and carries out the anaerobic biological processing, enters circulating fluidized bed then and carries out the aerobic biochemical processing;
(2) sewage after the biochemical treatment carries out mud-water separation by second pond or air supporting.Sewage qualified discharge after the separation, mud enter sludge thickener or are back to anaerobic pond, Aerobic Pond;
Further improvement in the technical proposal is: can carry out pre-treatment and aftertreatment according to the water quality situation of sewage.Pre-treatment mainly is to remove the material of major part to material, part difficult degradation and the high chroma of the toxic effect of microorganism; Aftertreatment is as disinfecting.
Describedly sewage is carried out pre-treatment comprise: regulate water temperature, the pH value of sewage and add coagulating agent and carry out coagulating and precipitate and separate or dissolved air flotation.
Described sewage carries out pre-treatment and comprises that effluent stream is through preliminary sedimentation tank, equalizing tank.
Another technical scheme of the present invention is the high-performance bio compatibility filling, and moiety comprises Polyurethane, rare earth metal and ferrous oxide.
This filler component weight part is: urethane 95-98 rare earth metal 0.1-0.5 ferrous oxide 1.5-3.
Described rare earth metal is the one or more combination in scandium (Sc), yttrium (Y), samarium (Ln), lanthanum (La), cerium (Ce), praseodymium (Pr), neodymium (Nd), promethium (Pm), europium (Eu), gadolinium (Gd), terbium (Tb), dysprosium (Dy), holmium (Ho), erbium (Er), thulium (Tm), ytterbium (Yb), the lutetium (Lu).
Another technical scheme of the present invention is the preparation method of high-performance bio compatibility filling, includes the following step:
Batch mixing: according to dosage sneak into additive in the urethane raw;
Foaming: utilize the polyurethane foam forming technique to foam;
Ingress: the numerical control cutting equipment by special use is cut apart;
Finished product: obtain qualified finished product through screening.
Urethane raw is a polyethers; Finished product grain size is 8mm * 8mm * 8mm--30mm * 30mm * 30mm.
Compared with prior art, pulsed fluidized bed circulating fluidized bed sewage treatment process of the present invention has the following advantages in actual applications: at first, add the high-performance bio compatibility filling in the fluidized-bed, increase the biomass in the biochemical system, improved the clearance of biochemical system, the stability of increase system operation.Secondly, the high-performance bio compatibility filling can reduce the activated sludge bulking phenomenon effectively, what solved traditional built-up type or other form fillers fills out a series of difficult problems such as extension, maintenance, replacing, for the low treatment project of ask for something input cost and the transformation of old treatment project remarkable advantages is arranged.In addition, the filler in the pulsed fluidized bed has kept the sludge concentration of anaerobic pond effectively, makes the content of anerobe reach higher level; The part filler of ciculation fluidized bed unit inner suspension has solved a large amount of foamy phenomenons of oxidation pond surface flotation in the past.
The present invention provides a kind of organism compatibility filling for sewage disposal, and this filler has huge specific surface; Has biological affine function; In current water, have from respiratory function; When biochemical treatment sewage, has the self-align tendency of function; Has adsorption function to gas; Advantages such as bulk density 0.95-1.10g/cm because the singularity of filling-material structure, make to there are differences the content difference of the inside and outside dissolved oxygen of filler attached to the microbial profile on the filler, have just formed the A/O processing unit and have denitrification functions.The denitrifying bacterium of filler inside utilize organism in the water inlet as carbon source with the NO in the sewage
3-N is converted into N
2, realize denitrification denitrogenation.Simultaneously, the NH in filler outside and the sewage
3-N is converted into NO
3-N realizes nitration reaction.In Waste Water Treatment, just form numerous " miniature " A/O denitrification system like this, greatly improved nitric efficiency.And the filler that adds has increased microbial biomass, has prolonged the microorganism residence time in the system, and promptly sludge age obtains prolonging, and more helps the removal of ammonia nitrogen.Its preparation method is simple, and is easy to use.
Description of drawings
Fig. 1 is the process flow diagram that the present invention utilizes the method that fluidized-bed process disposes of sewage.
Embodiment
The invention provides a kind of method of utilizing fluidized-bed process to dispose of sewage, may further comprise the steps:
(1) dose the high-performance bio compatibility filling in pulsed fluidized bed He in the circulating fluidized bed, sewage is introduced into pulsed fluidized bed and carries out the anaerobic biological processing, enters circulating fluidized bed then and carries out the aerobic biochemical processing;
(1) sewage after the biochemical treatment carries out mud-water separation by second pond or air supporting.Sewage qualified discharge after the separation, mud enter sludge thickener or are back to anaerobic pond, Aerobic Pond.
(2) can carry out pre-treatment and aftertreatment according to the water quality situation of sewage.Pre-treatment mainly is to remove most of material that microorganism is had material, part difficult degradation and the high chroma of toxic action; Aftertreatment is as disinfecting.
In invention, pulsed fluidized bed circulating fluidized bed sewage treatment process also further comprises: preliminary sedimentation tank 101, equalizing tank 102, second pond 105 and sludge thickener 106.The equipment that is adopted mainly comprises: running type scraping and sucking machine, plate-type heat exchanger, pulse water distribution device, underwater propeller and second pond radial-flow full-bridge type are scraped ooze sucker.Sewage passes through preliminary sedimentation tank 101, equalizing tank 102, pulsed fluidized bed 103, circulating fluidized bed 104 and second pond 105 in regular turn in the described fluidized-bed sewage treatment process, and is last, discharges after sterilizing.Specifically describe as follows in conjunction with the accompanying drawings.
With reference to shown in Figure 1, in step (1), sewage is introduced preliminary sedimentation tank 101, regulated the pH value of sewage, and add coagulating agent and carry out coagulating, remove most of sulfide, part difficult degradation and high chroma material.Then, carry out mud-water separation by the running type scraping and sucking machine in the preliminary sedimentation tank 101, mud is entered sludge thickener, sewage imports equalizing tank 102, is furnished with plate-type heat exchanger in the described equalizing tank 102, by the sewage temperature in the plate-type heat exchanger adjusting equalizing tank 102, control its temperature and be no more than the biochemical treatment requirement.Described pulsed fluidized bed 103 is built-in with the pulse water distribution device, described circulating fluidized bed 104 is built-in with underwater propeller, all be filled with organism compatibility filling in pulsed fluidized bed 103 and the circulating fluidized bed 104, then, in step (2), sewage is passed through pulsed fluidized bed 103 and circulating fluidized bed 104 in regular turn, sewage is carried out biochemical treatment by the high-performance bio compatibility filling.At last, in step (3), full-bridge type scraping and sucking machine by second pond 105 carries out separating treatment with muddy water, mud enters the sludge thickener precipitation, comparatively muddy sewage backflow to the pulsed fluidized bed 103 of part carries out anaerobic biological again, the comparatively clarifying treating water of part is outwards discharging after sterilization reaches environmental protection standard, finishes scavenging process.
In one embodiment of the invention, this project construction, when installing into the water commissioning test, the biochemical treatment unit adds the biochemical sludge bacterial classification, is used for sewage disposal, and the formation of filling carrier surface biological film, growth and the characteristic that waste water is degraded thereof are organism fluidization bed technique key in application.The forming process of high-performance bio compatibility filling of the present invention is as described below: the biochemical sludge bacterial classification is after domestication, cultivating tens days, when the fluidized bed active sludge concentration reaches the 0.7g/l left and right sides, begin to add the high-performance bio compatibility filling to pulsed fluidized bed, circulating fluidized bed, the ratio of adding is 30%.Most of filler floats over the reaction tank surface when initial, after 2 days, filler begins biofilm, about 5-7 days, microbial biomass breeding on the ciculation fluidized bed fillers rapidly, microbial film is thicker, the filler major part is in suspended state, under waterpower plug-flow and mixed flow effect, sewage microorganism abundant and in the filler is contacted, microorganism shoots up because of having absorbed the nutrient that sewage provides (pollutent), behind the two weeks, the high-performance bio compatibility filling also reaches good fluidized state in the pulsed fluidized bed, and the one and a half months left and right sides time, total system reaches the designing treatment water yield.
In the fluidized-bed sewage treatment process of the present invention, average removal rate is as follows:
In the present invention, described high-performance bio compatibility filling is to be processed by urethane and a certain proportion of multiple rare earth metal and ferrous oxide proportioning.In preferred embodiment, described high-performance bio compatibility filling main component comprises urethane, rare earth metal and ferrous oxide therein, and the weight part of its each component is:
Urethane 95-98 rare earth metal 0.1-0.5 ferrous oxide 1.5-3
Wherein, described rare earth metal is the one or more combination in scandium (Sc), yttrium (Y), samarium (Ln), lanthanum (La), cerium (Ce), praseodymium (Pr), neodymium (Nd), promethium (Pm), europium (Eu), gadolinium (Gd), terbium (Tb), dysprosium (Dy), holmium (Ho), erbium (Er), thulium (Tm), ytterbium (Yb), the lutetium (Lu).
In the present invention, the preparation method of high-performance bio compatibility filling comprises the following steps:
Batch mixing: according to dosage sneak into additive in the urethane raw;
Foaming: utilize the polyurethane foam forming technique to foam;
Ingress: the numerical control cutting equipment by special use is cut apart;
Finished product: through the finished product that screens qualifiedly.
Wherein, urethane raw is a polyethers; Finished product grain size is preferably between 8mm * 8mm * 8mm-30mm * 30mm * 30mm.
Finally, this filler of acquisition can be porosity 90%-95%, and density is between 1.0-1.05, and bulk density is 0.95-1.10g/cm
3
Ferrous oxide has better biocompatibility, add in the organism compatibility filling, play the effect of biofilm development physical platform, increased electron transfer function simultaneously, thereby become functional biocatalysis carrier, microorganism carries out metabolism with iron as electron acceptor(EA), improves greatly with the rate of metabolism of the dissolved oxygen in the water as electron acceptor(EA) when using conventional fillers, thereby obviously improved the waste water treatment efficiency of biological fluidized bed on macroscopic view.
This filler has good elasticity, bigger specific surface reaches stronger biological affine function, in current water, have from respiratory function, under the stirring of waterpower, air-flow, impacting, subtle change can take place in filler self shape, and this change of shape has guaranteed to form between filler inside, the outside good exchange of substance condition.In the biochemical treatment sewage process, have the self-align tendency of function, simultaneously gas is had adsorption function.The multiple rare metal that contains in the filler has promoted the biochemical reaction of microorganism.
And because the singularity of filling-material structure, make to there are differences the content difference of the inside and outside dissolved oxygen of filler attached to the microbial profile on the filler, just form the A/O processing unit and had denitrification functions.The denitrifying bacterium of filler inside utilize organism in the water inlet as carbon source with the NO in the sewage
3-N is converted into N
2, realize denitrification denitrogenation.Simultaneously, the NH in filler outside and the sewage
3-N is converted into NO
3-N realizes nitration reaction.In Waste Water Treatment, just form numerous " miniature " A/O denitrification system like this, greatly improved nitric efficiency.And the filler that adds has increased microbial biomass, has prolonged the microorganism residence time in the system, and promptly sludge age obtains prolonging, and more helps the removal of ammonia nitrogen.
Empirical pilot scale and engineering practical application prove, result of use the best when the physical dimension of organism compatibility filling is 1cm * 1cm * 1cm.In the biochemical reaction unit, the filler filling ratio is controlled at 15%-40% and is advisable.
Organism compatibility filling is understood the working cycle of spontaneous formation one " suspension-precipitation " under the situation of attached growth of microorganisms.Filler is added to the biochemical reaction tank initial stage, and apposition growth a spot of microorganism on the filler, and filler is the suspension growth state in reaction tank.Along with the increase gradually of microorganism on the filler, the proportion of filler integral body increases, and this moment, filler was deposited in the bottom of reaction tank.Be deposited in microorganism on the filler of bottom because material transfer weakens and biological self aging oxidation, and beginning is peeled off with filler, organism compatibility filling returns to suspended state gradually again, is repeating the working cycle of " suspension-precipitation ".
Pulse fluidisation bed unit 103 in the pulsed fluidized bed circulating fluidized bed sewage treatment process is to use the acidication reaction principle of anaerobic reaction, add the organism compatibility filling of certain volume ratio in the pulse fluidisation bed unit 103, utilize the pulse water distribution effect of pulse water distribution device, filler reaches the fluidized state of " suspension-precipitation " at reactor.Circulating fluidized bed 104 is to use aerobic microbiological oxidizing reaction principle, organism compatibility filling is added in the circulating fluidized bed, under the impact and stirring of waterpower, air-flow, reach good fluidized state, the circulating fluidized bed water side is back to the circulating fluidized bed feed-water end by pusher under water with filler, finishes the full cycle fluid mapper process.
Utilize the method for fluidized bed processing sewage to have the following advantages in actual applications:
At first, add the high-performance bio compatibility filling in the fluid bed, increased the biomass in the biochemical system, Removal rate, the increase system operation stability of biochemical system have been improved.
Secondly, organism compatibility filling can reduce the activated sludge bulking phenomenon effectively, than traditional combination Formula or other form filler costs are low, easy to use, drop into the low processing engineering of cost for ask for something and reach The transformation of old processing engineering has obvious advantage.
In addition, the part filler of ciculation fluidized bed unit inner suspension, it is floating big to have solved in the past the oxidation pool surface The phenomenon of amount foam.
And, the use of high-performance bio compatibility filling in this technology, to design, the no special requirement of construction, Adding, replenish, upgrading of filler is simple to operate.
Claims (10)
1. method of utilizing fluidized-bed process to dispose of sewage comprises above step:
(1) dose organism compatibility filling in pulsed fluidized bed He in the circulating fluidized bed, described organism compatibility filling comprises urethane, rare earth metal and ferrous oxide;
(2) sewage is introduced into pulsed fluidized bed and carries out anaerobic biological and handle, and enters circulating fluidized bed then and carries out aerobic biochemical and handle.
2. the method for utilizing fluidized-bed process to dispose of sewage according to claim 1, it is characterized in that: the sewage that finishes after the biochemical treatment carries out mud-water separation by second pond or air supporting, sewage qualified discharge after the separation, mud enter sludge thickener or are back to anaerobic pond, Aerobic Pond.
3. the method for utilizing fluidized-bed process to dispose of sewage according to claim 1 is characterized in that: can carry out pre-treatment and aftertreatment according to the water quality situation of sewage.
4. the method for utilizing fluidized-bed process to dispose of sewage according to claim 3 is characterized in that: describedly sewage is carried out pre-treatment comprise: effluent stream is through water temperature, the pH value of preliminary sedimentation tank, equalizing tank, adjusting sewage and add coagulating agent and carry out coagulating and precipitate and separate or dissolved air flotation.
5. the method for utilizing fluidized-bed process to dispose of sewage according to claim 3 is characterized in that: described sewage carries out aftertreatment and comprises and disinfecting.
6. an organism compatibility filling that is used for the described sewage water treatment method of claim 1 is characterized in that: comprise urethane, rare earth metal and ferrous oxide.
7. organism compatibility filling according to claim 6 is characterized in that: this filler component weight part is: urethane 95-98, rare earth metal 0.1-0.5, ferrous oxide 1.5-3.
8. according to claim 6 or 7 described organism compatibility fillings, it is characterized in that: described rare earth metal is the one or more combination in scandium (Sc), yttrium (Y), samarium (Sm), lanthanum (La), cerium (Ce), praseodymium (Pr), neodymium (Nd), promethium (Pm), europium (Eu), gadolinium (Gd), terbium (Tb), dysprosium (Dy), holmium (Ho), erbium (Er), thulium (Tm), ytterbium (Yb), the lutetium (Lu).
9. the preparation method of the described organism compatibility filling of claim 6 includes the following step:
Batch mixing: additive is according to dosage sneaked in the urethane raw, and described additive is rare earth metal and ferrous oxide;
Foaming: utilize the polyurethane foam forming technique to foam;
Ingress: the numerical control cutting equipment by special use is cut apart;
Finished product: through the finished product that screens qualifiedly.
10. the preparation method of organism compatibility filling according to claim 9, it is characterized in that: urethane raw is a polyethers; Finished product grain size is 8mm * 8mm * 8mm---30mm * 30mm * 30mm.
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| CN101549930B (en) * | 2008-04-03 | 2012-08-15 | 上海百峰环保工程有限公司 | System and method for processing high-concentration printing and dyeing wastewater |
| CN101648102B (en) * | 2009-08-31 | 2012-01-25 | 青岛华世洁环保科技有限公司 | Cold and hot type adsorption-desorption device and adsorption-desorption method thereof |
| CN101941758A (en) * | 2010-08-19 | 2011-01-12 | 国核电力规划设计研究院 | Method for treating nitrogen-containing wastewater from power plants by nitrifying bacteria immobilized on polyurethane |
| CN102174253B (en) * | 2011-01-29 | 2013-03-13 | 浙江省环境保护科学设计研究院 | Preparation method and application of porous hydrophilic denitrification biological carrier |
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| CN102432098B (en) * | 2011-11-15 | 2013-06-05 | 广州中环万代环境工程有限公司 | PAFR-B (pulse anaerobic fluidized bed reactor) and organic waste water processing method |
| CN105060651B (en) * | 2015-08-25 | 2018-01-09 | 广州汇智源环保科技有限公司 | A kind of advanced treating technology for industrial sewage and device |
| CN105060467B (en) * | 2015-08-25 | 2018-05-18 | 桂琪 | A kind of multiporous biological filler and its preparation method and application |
| CN105800869B (en) * | 2016-04-18 | 2018-09-25 | 江苏金梓环境科技股份有限公司 | A kind of recirculating fluidized bed family sewage disposal device |
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| CN106007200A (en) * | 2016-07-04 | 2016-10-12 | 宜兴市永加化工有限公司 | Method for treating wastewater |
| CN107055785A (en) * | 2017-06-01 | 2017-08-18 | 浙江永续环境工程有限公司 | Flow microorganism bed biomembrance process |
| CN110482800A (en) * | 2019-09-11 | 2019-11-22 | 东莞市正大纺织科技有限公司 | A kind of sewage treatment facility |
| CN113336315B (en) * | 2021-07-05 | 2022-04-12 | 华北电力大学（保定） | System and method for treating sewage by using microbial fuel cell |
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Assignee: GUANGZHOU CHINAEVER ENVIRONMENTAL ENGINEERING CO.,LTD. Assignor: Liu Depei Contract record no.: 2010440020212 Denomination of invention: Method of processing sewage utilizing fluidized bed technique, organism compatibility filling thereof and preparing method of filling Granted publication date: 20091007 License type: Exclusive License Open date: 20070808 Record date: 20101118 |
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Granted publication date: 20091007 Termination date: 20210829 |