A kind of constant temperature vacuum storage device
Technical field
The present invention relates to a kind of container of sample retention under constant temperature and specified pressure condition that make.
Background technology
Materials such as medical, microelectronic semiconductor chip often need be stored under specified temp and the vacuum condition, especially need be when storage and transportations and big gas phase insulation, and to avoid because of contact the problem that produces surface oxidation with air.
In recent years in the archaeology field, also produce a problem, article in 1,100 have promptly been buried, suitable dark and specific temperature environment, long-time if these article exposed under air and photoenvironment and nonspecific temperature environment, all can it quicken rotten rotten.Rotten in order to prevent archaeological samples, particularly some sample that just has been unearthed is rotten, also should to be isolated in the environment with atmosphere and illumination, it is under the specific temperature conditions with sample storage in specific environment.Be that particular sample with this class is positioned in the glass drying basin in the prior art, glass dish is placed the device of lucifuge or indoor, to the application of vacuum of bleeding of glass drying basin, simultaneously device or the indoor constant temperature that carries out of placing the glass drying basin are handled again.Obviously, archaeology scene or transportation, be difficult to the aforesaid condition of realization from the scene of engaging in archaeological studies to experiment collection place.And because of the glass drying basin is very heavy, printing opacity, frangible, carries and transport and very inconvenient, if sample needs certain malleation to preserve, preserve more difficult with the glass drying basin.
With the progress of science, produced some special materials in recent years, and the storage of some material, the transportation also need under conditions such as specified pressure, specified temp lucifuge, carry out.Realize under the prior art that this special storage and transportation also are comparatively difficult.
Lack in the prior art and can carry out the preservation under constant temperature and the specified pressure and the device of the special use that is suitable for transporting material or sample.
China's utility model patent 03248544.1 discloses a kind of historical relic's protection cabinet; it is made up of double-deck cabinet; interior cabinet external diameter is less than outer cabinet internal diameter; between two cabinets, make vacuum; in the side of cabinet the pipeline that links to each other with interior cabinet is housed, pipeline opening installation and control switch, deposit article after; form vacuum in the cabinet, at the bottom of the cabinet, the top adopts the double-layer vacuum structure.According to disclosed content as can be known, inside and outside cabinet is made of two cabinet plates respectively in the practical structures of this patent, forms vacuum interlayer between two cabinet plates.Because have double-deck two vacuum structure, the moisture effect of this patent is good.But the destruction (as in transportation) that the inside and outside cabinet of working as this patent meets accident can directly influence the article that memory space is stored in it, and therefore this device is not suitable for the storage for special article, more is unfavorable for transporting and using in the open air.
Summary of the invention
The invention provides and a kind ofly can carry out the preservation under constant temperature and the specified pressure and the device of the special use that is suitable for transporting material or sample.
This constant temperature vacuum storage device of the present invention is made of: body skin, inner housing and compound lid, and wherein: body skin constitutes the container of cup-shaped by the double wall shell, forms a vacuum interlayer between the double wall shell; In the inwall of body skin, be located at inner housing, had a space between inner housing and body skin inwall;
Opening part at container is provided with the negative thread that connects with compound lid.Compound lid of the present invention is by the flange of end, its pipe that is positioned at the flange bottom is provided with the externally threaded tubular structure that connects with body skin and constitutes, in the tubular structure hollow space, be provided with the negative thread that connects with inner housing, on flange, be provided with the connecting pipeline that can be communicated with, be provided with vacuum valve at the connecting pipeline end with inner housing.Inner housing of the present invention is provided with the negative thread joining externally threaded cup-like structure set with the tubular structure of compound lid by its open end, and inner housing inside is the storage specimen chamber of storing sample.Compound in the present invention lid is equipped with packing seal with the part that body skin and inner housing connect.
Also be communicated with vacuum manometer on the compound connecting pipeline that covers of the present invention, so that to being detected timely by the pressure of the environment stored.
Space outside body skin of the present invention inside and the inner housing can be provided with device and the temperature measuring equipment that changes system temperature, and flange is provided with to the lead-in wire of the device provisioning electric power that changes system temperature and the lead-in wire that the temperature measuring equipment signal feeds out.The device of the change system temperature that the space outside body skin of the present invention inside and the inner housing is provided with can be an annular electro heating tape, also can be the quartz conductor heating-cooling device, and when adopting the latter except that can heating, also can freeze within the specific limits.
The tube wall of the compound tubular structure that covers of the present invention is provided with second connecting pipeline that is communicated with the space outside extraneous and body skin inside and the inner housing, is provided with valve on second connecting pipeline.Can between inner casing and body skin, inject ultralow temperature cooling medias such as liquid nitrogen by the second set connecting pipeline, to be suitable for more special storage requirement, as the requirement of ultralow temperature storage.
Body skin of the present invention preferably adopts the stainless steel material manufacturing, and its inner housing can require to adopt different materials according to institute's storage material, as glass, High molecular material, perhaps metallic material.
The present invention makes the interior soak zones that forms of inner chamber of body skin, for storage special material in it provides the constant temperature guarantee because of the outer shell construction feature of its double-walled; Owing to be provided with the inner housing that is used to preserve article again in the body skin, the memory space variation of temperature in the inner housing more tended towards stability; And inner housing can make the interior space of inner housing be in the particular pressure condition by being located at pipeline set on the multiple lid operation of pressurizeing or reduce pressure, and this requires to provide assurance for pressure of special material storage again; Again because of inner housing is to be within the body skin, so the material of storage in the inner housing is under the state of lucifuge naturally.Use thread connection between multiple lid of the present invention and inside and outside housing, make its manufacturing process comparatively convenient, also convenient the use, the particularly placement of convenient built-in article, and because of having adopted thread connection, make in the inner housing not only can be vacuum state, also can be in barotropic state, and its pressure inside state can keep after closing the compound vacuum valve that covers, and this also brings convenience for the storing of material.Therefore the present invention can make inner housing be among the suitable temperature environment because of be provided with the device that system changes temperature between body skin and inner housing.In addition, from the structure of the present invention introduced previously as can be known, can also between body skin and inner housing, charge into strong cooling medias such as liquid nitrogen by second set on the compound box connecting pipeline, can realize that the ultralow temperature of material is preserved and storing.And temperature measuring equipment provided thereon and vacuum indicator also can reflect at any time by the preservation environmental parameters of storage article.
Also can find out from aforesaid architectural feature, the present invention can make the size that volume is less, be convenient to transport, this just can satisfy light, high-mobility, multipurpose, wheeled vehicle, and multiple operating needs that volume is little, be easy to carry about with one has made things convenient for special article specific (special) requirements to aspects such as pressure, temperature in accumulating.In addition, during the present invention's operation in the open air, under power free condition, can also vacuumize, vegeto-animal sample is carried out processing fresh-keeping or that remove moisture, drying by manual vacuum pump.The present invention also has characteristics cheap for manufacturing cost, durable, stable and reliable for performance.
Description of drawings
Accompanying drawing 1 is the stepped generalized section of one embodiment of the present of invention structure, and accompanying drawing 2 is the cross-sectional schematic of compound lid and inner housing disassembly status among Fig. 1.
In the accompanying drawing: 1 for to constitute the lagging casing body by double wall, is vacuum area between double wall; 2 for being located at the annular heating tape between inner and outer shell; 3 is the space between inner and outer shell; 4 is inner housing, and its inside is exactly the sample storeroom; 5 is position, temperature measuring equipment signal pig-tail wire hole in the sample storeroom; 6 are the compound flange that covers; 7 is vacuum manometer; 8 is vacuum valve; 9 is vacuum valve switch knob; 10 is vacuum pumping opening; 11 are second connecting pipeline on the tube wall of being located at tubular structure; 12 are the thermal insulation sealing arrangement between lid and sample storeroom; 13 pay for the joining screw thread of tube cavity of inner housing and compound lid tubular structure; 14 for be located at outside the compound lid tubular structure with the joining outside thread of body skin; 15 is seal groove; 16 are the heating power supply lead-in wire.
The specific embodiment
One embodiment of the present of invention as shown in Figure 1, its body skin 1 and compound lid all adopt the stainless steel material manufacturing, the brass material manufacturing of inner housing 4 usefulness 2 millimeters thick.Wherein shut after the vacuum pumping between the double wall of body skin, to guarantee its heat preservation effect.On the inwall of body skin 1 end opening, make negative thread, and make outside thread (referring to accompanying drawing 2), and pay by screw thread body skin 1 and inner housing 4 and compound lid are linked together in the upper end open of inner housing 4.One through hole is arranged in the middle of the compound lid flange 6, forms the pipeline with inner housing 4 internal communication, and on this section pipeline with one section pipe of screw thread, and fixedly vacuum valve 8 and vacuum manometer 7 thereon.The used vacuum valve of present embodiment is a threeway vacuum needle-valve.The pipe 10 that links to each other with the vacuum valve extracting vacuum that can link to each other with vacuum also can link to each other with pump, gives pressurization in the inner housing 4.Be provided with the heating tape 2 of annular in the body skin 1 of present embodiment and the space between the inner housing 4, and heating tape 2 required electric power introduced in it, so constitute the device that changes system temperature by being located at the compound lead-in wire that covers 16.By going between 5 with temperature element, as thermocouple, measured temperature signal extracts simultaneously.In inner housing, also be provided with the thermocouple that is used for thermometric, but all not expressions in the drawings.In addition, also be provided with second connecting pipeline 11 that is communicated with the space between the inner and outer shell, on pipeline 11, also be provided with valve compound covering.Second pipeline 11 can have following several purposes: the first in use links to each other it with vacuum pump, makes its inside that certain degree of vacuum be arranged, and this can further improve the heat-insulating property of apparatus; Its two be space between inner and outer shell be under the antivacuum state and need be to system's heating so that when keeping certain temperature in the sample storeroom, open the valve of pipe 11 slightly, make heating cause gas to expand and be released, prevent accident; It three is samples that requirement is stored when preserving at low temperatures, can charge into cooling media in 11 interlayers that form cool off between inner and outer shell by managing, as charge into media such as cool brine or liquid nitrogen.From figure, be also shown in addition, be equipped with the insulated enclosure pad in the connection place of compound lid and inner and outer shell.
Its outer dia of apparatus by a reality of the structure manufacturing of accompanying drawing 1 is 155 millimeters, and the gap between the double wall of body skin is 10.5 millimeters, and the internal diameter of inner housing is 165 millimeters, highly is 185 millimeters, and the weight of whole apparatus when zero load is 2.8Kg.Obviously this size is very convenient carries, carries and transport.Through the field service test test, the accessible final vacuum in storage sample cell in the inner housing of this charmed embodiment is less than 5 * 10
-2MmH, and the maximum pressure that can carry is 0.80MPa.When adopting annular heating tape structure to heat, its sample storeroom temperature can reach 300 ℃; And when charging into liquid nitrogen between inner and outer shell, sample storeroom temperature can reach-173 ℃.And the apparatus of present embodiment possesses suitable insulating power, after system reaches a preset temperature, close thermal source after, apparatus still keeps original temperature in considerable time under outdoor environment.For example, after the sample cell temperature was heated to 95 ℃, PTO Power Take Off placed 20~25 ℃ of room temperature environments after following 15 hours, and the temperature in its sample cell has only descended 5~8 ℃.In addition, also find,, use vacuum pump (comprise and make vacuum pump by hand) to bleed again, sample is dehydrated to a certain extent from managing 10 when plant sample being put into the sample storeroom and whole apparatus being assembled through actual test.
Also can make the bigger apparatus of volume for special operating needs by basic thought of the present invention.And when changing the annular heating tape in the previous embodiment into semiconductor heat booster, can become an alternative embodiment of the invention.