CN100494440C - Sintering aluminium rod and its preparation method - Google Patents
Sintering aluminium rod and its preparation method Download PDFInfo
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- CN100494440C CN100494440C CNB2005100097991A CN200510009799A CN100494440C CN 100494440 C CN100494440 C CN 100494440C CN B2005100097991 A CNB2005100097991 A CN B2005100097991A CN 200510009799 A CN200510009799 A CN 200510009799A CN 100494440 C CN100494440 C CN 100494440C
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Abstract
The invention relates to a sintering aluminum stick and the manufacture method that each 93 portions of alloy of active aluminum contains Al2O3 9-11, iron 0.4-0.7, water 0.05-0.1, grease and 0.1-0.30. It could satisfy the special demand for aviation and war industry.
Description
Technical field
The present invention relates to a kind of powder metallurgy and add sintering aluminium bar and the manufacture method thereof that the TT skill combines and makes with aluminium alloy.
Background technology
The aluminium alloy of existing smelting process casting is subjected to the restriction of alloying element solubleness when alloying, the add-on of alloying element can not be too high, uneven crystallization exists component segregation and internal stress during casting, has influenced product strength thus, also can't satisfy the requirement of special purpose on performance.
Summary of the invention
The sintering aluminium bar and the manufacture method thereof that the purpose of this invention is to provide a kind of special purpose are to satisfy the special requirement of aerospace and military project aspect.
Above-mentioned purpose realizes by following technical scheme:
The sintering aluminium bar, its composition comprises: aluminium, contain aluminium sesquioxide 9-11, iron 0.4-0.7, water 0.05-0.1, grease 0.1-0.30 in the alloy of the described active aluminum that contains per 93 parts of weight.
The sintered aluminium rod manufacturing method, its process comprises: the raw material aluminium powder is dusted sieve after grinding, the aluminium powder that granularity is qualified carries out a change, be pressurized to the 160-180MPa pressurize and formed blank in 30 minutes, the blank ingot of moulding is put into watertight chest send into the soaking pit heating then, insulation heats up, and furnace cooling, pier are thick, heat-insulation pressure keeping, extruding:
A. the Heating temperature in the described soaking pit is 300 ℃;
B. described soaking time is 18-30 hour;
C. described intensification is meant and rises to 470-480 ℃;
D. the described course of processing adopts nitrogen protection;
E. thick temperature 450-480 ℃ on described pier;
F. extrusion temperature 490-500 ℃, extrusion speed is a per second 8-14 millimeter.
Above-mentioned sintered aluminium rod manufacturing method, described nitrogen protection fed nitrogen 10-15 minute every 30 minutes when heating in soaking pit, be incubated 10-18 hour altogether, after the intensification, fed nitrogen continuously, were incubated 10 hours.
Above-mentioned sintered aluminium rod manufacturing method, the soaking time that described pier is thick is 2-4 hour, the dwell time is 5 minutes, slowly releases after the pressure release.
Above-mentioned sintered aluminium rod manufacturing method, thermal treatment is incubated 2-4 hour for the agglomerating aluminium ingot being heated to after the described temperature before the described extruding.
This technical scheme has following beneficial effect:
1 method of the present invention realizes pre-alloyed by ball milling, guaranteed the requirement of the ratio of weight and number of strengthening phase aluminium sesquioxide in the aluminium powder at 9-11 and other compositions, AI
2O
3The subgrain boundary place that is distributed in matrix AI of even dispersion behind, the attrition crushing thick through subsequently coldmoulding, pier, intensive has hindered the migration of dislocation and subgrain boundary thus, even the higher temperature of reheat afterwards, AI
2O
3Mutually also still pinning dislocation and subgrain boundary strongly hinder its migration.Make present method product processed have unusual good thermal stability thus, still have higher intensity at 500 ℃, high-temperature behavior is very high.
2. powder metallurgic method of the present invention and broken after processing avoided the generation of component segregation and stress corrosion, the corrosion resistance that makes this material is near rafifinal, avoided stress corrosion fully, thermal expansivity is very little, is satisfying the particular requirement of military industry on the intensity and on the performance.
3. the product that method of the present invention is produced is distributed in the matrix with can guaranteeing the alloying element even dispersion, and the anti-stress corrosion performance of fabricated product is near rafifinal simultaneously, and resistance to elevated temperatures then is much higher than the aluminium alloy that traditional fusion casting is produced.
The specific embodiment of the present invention:
Embodiment 1:
The sintering aluminium bar, its composition comprises: aluminium, contain aluminium sesquioxide 9, iron 0.4, water 0.05, grease 0.1 in the alloy of the described active aluminum that contains per 93 parts of weight.
Embodiment 2:
The sintering aluminium bar, its composition comprises: aluminium, contain aluminium sesquioxide 11, iron 0.7, water 0.1, grease 0.30 in the alloy of the described active aluminum that contains per 93 parts of weight.
Embodiment 3:
The sintering aluminium bar, its composition comprises: aluminium, contain aluminium sesquioxide 10, iron 0.6, water 0.07, grease 0.2 in the alloy of the described active aluminum that contains per 93 parts of weight.
Embodiment 4:
The manufacture method of embodiment 1 to embodiment 3 described sintering aluminium bar:
1. the preparation of sintered aluminium powder
Select 99.7% commercially pure aluminium ingot for use, dust as the aluminium powder raw material of sintering aluminium bar.
With above-mentioned raw material aluminium powder dust grind after, sieve, obtain the aluminium powder that the granularity conformance with standard requires, carry out a change.
Various raw materials are carried out proportioning, and the alloying constituent of sintered aluminium powder is aluminium sesquioxide 9-11%, active aluminum≤93%, grease≤0.3%, iron≤0.7%, water≤0.1%.
2. cold pressing forming process
Aluminium powder is incapsulated, be put in the support tube, put into the container of isostatic pressing machine with support tube, boosted to behind the 160-180MPa pressurize 30 minutes, slowly pressure release, do not have press after, take out the blank ingot after the moulding in the capsule, the blank ingot diameter is generally at 158-160mm.
3. oil removing degasification sintering process
The blank ingot of moulding is put into special watertight chest, send into soaking pit, be heated to 300 ℃ with stove; fed nitrogen 10-15 minute every 30 minutes this moment, is incubated after 18-30 hour, is warmed up to 470-480 ℃; feed nitrogen protection gas this moment continuously, is incubated after 10 hours to have a power failure furnace cooling.
4. upsetting process
Slightly with 2000 tons of water pressure engine, diameter 170mm container, extrusion temperature are 450 ℃ to pier, and the thick temperature of pier is 450-480 ℃, soaking time 2-4 hour, and total head 270-300MPa, pressurize 5 minutes is slowly released after the pressure release, and railway carriage is to diameter 162mm.
5. extrusion process
Extruding is with 2000 tons of water pressure engine, railway carriage is heated to 490-500 ℃ to the sintering aluminium ingot of diameter 162mm is incubated 2-4 hour, and the container temperature is 450 ℃, and total head 270-300MPa, extrusion speed are 8-14mm/s.
The ambient temperature mechanical properties of this sintering aluminium bar, σ
b〉=320M Pa, δ 〉=4%.
Mechanical behavior under high temperature σ under 500 ℃
b〉=90M Pa, δ 〉=1%.
Claims (4)
1. sintering aluminium bar, its composition comprises: aluminium is characterized in that: contain aluminium sesquioxide 9-11, iron 0.4-0.7, water 0.05-0.1, grease 0.1-0.30 in the alloy of the described active aluminum that contains per 93 parts of weight.
2. sintered aluminium rod manufacturing method as claimed in claim 1, its process comprises: the raw material aluminium powder is dusted sieve after grinding, the aluminium powder that granularity is qualified carries out a change, be pressurized to the 160-180MPa pressurize and formed blank in 30 minutes, the blank ingot of moulding is put into watertight chest send into the soaking pit heating then, insulation heats up, furnace cooling, pier are thick, heat-insulation pressure keeping, extruding, it is characterized in that:
A. the Heating temperature in the described soaking pit is 300 ℃;
B. described soaking time is 18-30 hour;
C. described intensification is meant and rises to 470-480 ℃;
D. the described course of processing adopts nitrogen protection;
E. thick temperature 450-480 ℃ on described pier;
F. extrusion temperature 490-500 ℃, extrusion speed is a per second 8-14 millimeter.
3. sintered aluminium rod manufacturing method according to claim 2 is characterized in that: described nitrogen protection fed nitrogen 10-15 minute every 30 minutes when heating in soaking pit, be incubated 10-18 hour altogether, after the intensification, fed nitrogen continuously, was incubated 10 hours.
4. according to claim 2 or 3 described sintered aluminium rod manufacturing methods, it is characterized in that: the soaking time that described pier is thick is 2-4 hour, and the dwell time is 5 minutes, slowly releases after the pressure release.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100097991A CN100494440C (en) | 2005-03-08 | 2005-03-08 | Sintering aluminium rod and its preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100097991A CN100494440C (en) | 2005-03-08 | 2005-03-08 | Sintering aluminium rod and its preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1831170A CN1831170A (en) | 2006-09-13 |
| CN100494440C true CN100494440C (en) | 2009-06-03 |
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ID=36993666
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100097991A Expired - Fee Related CN100494440C (en) | 2005-03-08 | 2005-03-08 | Sintering aluminium rod and its preparation method |
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| CN (1) | CN100494440C (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113751682A (en) * | 2021-08-12 | 2021-12-07 | 西安鼎鑫科技新材料有限公司 | Casting process and equipment for casting ultrahigh-strength aluminum alloy hub material for vehicle |
-
2005
- 2005-03-08 CN CNB2005100097991A patent/CN100494440C/en not_active Expired - Fee Related
Non-Patent Citations (2)
| Title |
|---|
| 用等静压法制坯试生产直径45毫米烧结铝棒. 王文政.轻合金加工技术，第11期. 2004 |
| 用等静压法制坯试生产直径45毫米烧结铝棒. 王文政.轻合金加工技术，第11期. 2004 * |
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| Publication number | Publication date |
|---|---|
| CN1831170A (en) | 2006-09-13 |
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Granted publication date: 20090603 Termination date: 20190308 |