CN100488653C - Method for preparing high-temperature-room type plasticity magnesium alloy sheet material - Google Patents
Method for preparing high-temperature-room type plasticity magnesium alloy sheet material Download PDFInfo
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- CN100488653C CN100488653C CNB2007100111593A CN200710011159A CN100488653C CN 100488653 C CN100488653 C CN 100488653C CN B2007100111593 A CNB2007100111593 A CN B2007100111593A CN 200710011159 A CN200710011159 A CN 200710011159A CN 100488653 C CN100488653 C CN 100488653C
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- magnesium alloy
- alloy plate
- temperature
- sheet material
- room type
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- 229910000861 Mg alloy Inorganic materials 0.000 title claims abstract description 61
- 238000000034 method Methods 0.000 title claims abstract description 30
- 239000000463 material Substances 0.000 title claims abstract description 15
- 230000008569 process Effects 0.000 claims abstract description 12
- 238000001192 hot extrusion Methods 0.000 claims description 10
- 238000003754 machining Methods 0.000 claims description 4
- 238000010008 shearing Methods 0.000 claims description 4
- 238000001125 extrusion Methods 0.000 abstract description 11
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 4
- 230000008901 benefit Effects 0.000 abstract description 2
- 239000011148 porous material Substances 0.000 abstract 4
- 239000004753 textile Substances 0.000 abstract 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 5
- 239000011777 magnesium Substances 0.000 description 5
- 229910052749 magnesium Inorganic materials 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 229910045601 alloy Inorganic materials 0.000 description 4
- 239000000956 alloy Substances 0.000 description 4
- 229910000838 Al alloy Inorganic materials 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000007712 rapid solidification Methods 0.000 description 3
- 238000005275 alloying Methods 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000005242 forging Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 229910001008 7075 aluminium alloy Inorganic materials 0.000 description 1
- 229910018137 Al-Zn Inorganic materials 0.000 description 1
- 229910018573 Al—Zn Inorganic materials 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 240000005373 Panax quinquefolius Species 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000003913 materials processing Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000010137 moulding (plastic) Methods 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 238000005482 strain hardening Methods 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21C—MANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
- B21C23/00—Extruding metal; Impact extrusion
- B21C23/02—Making uncoated products
- B21C23/04—Making uncoated products by direct extrusion
- B21C23/06—Making sheets
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Extrusion Of Metal (AREA)
Abstract
The invention is a method for preparing magnesium alloy plate with high room temperature plasticity, belonging to the plastic processing technology field of nonferrous material. It relates to the extrusion moulding method for magnesium alloy plate, especially the method that thermal extrusion process is used to prepare magnesium alloy plate with high room temperature plasticity. It is characterized in that the extrusion mould with special figure mould pore is used to extrude magnesium alloy plate in heat and the special figure mould pore is a rectangle mould pore, which is asymmetric in upper and lower. The mould pore can generate shear stress in thermal extruding process to magnesium alloy plate and is favor of generating shear plastic deformation in thermal extruding process to magnesium alloy plate so that the magnesium alloy plate after extrusion has the base surface textile {0002} with lower intensity to improve the room temperature plasticity of magnesium alloy plate. The benefit of invention is that as the prior processing equipment is used to improve moulds in little it can be carried into execution, the preparing cost is low and it is suitable for thermal extrusion process to magnesium alloy with any grade.
Description
Technical field
The invention belongs to technical field of nonferrous metal plastic molding, relate to the extrusion process of magnesium alloy plate, particularly a kind of method for preparing high-temperature-room type plasticity magnesium alloy sheet material.
Background technology
Magnesium alloy has low-density, high specific strength, high damping, high conductivity, good electromagnetic wave shielding and dimensional stability, particularly magnesium alloy has aboundresources, low cost of manufacture such as easily reclaims, pollution-free at environmental protection characteristic, is regarded as current " green metal ".As a kind of important light structures metal material, magnesium alloy is with a wide range of applications at industrial circles such as automobile making, communication electronics, Aero-Space.
Because magnesium is close-packed hexagonal (HCP) structural material, its plastic deformation at room temperature only limit to basal plane 0001}＜11-20〉slippage and the conical surface 10-12}＜10-11〉twin, so the temperature-room type plasticity working ability of magnesium alloy is relatively poor.Thereby, the processing of most of magnesium alloy products only limits to particularly die cast of casting (Casting), the wrought magnesium alloy goods of the forging and pressing of industrial extensive use (Forging), extruding (Extrusion), rolling plastic workings such as (Rolling) preparation have then seldom greatly limited the Application of Magnesium scope.Therefore, improving the magnesium alloy temperature-room type plasticity effectively is to solve magnesium alloy engineering key in application.
Mainly laying particular emphasis on aspects such as design of alloy (alloying), precipitation strength, grain refinement and materials processing forming technique aspect the wrought magnesium alloy research both at home and abroad at present, trying hard to improve performances such as the intensity, plasticity of magnesium alloy, anticorrosive, creep resistant and fatigue with this.In magnesium, add lithium (Li), indium (In) and silver alloying elements such as (Ag) can make axial ratio (1.633) be reduced to 1.618, can excite prismatic surface 10-10}＜11-20〉slippage, and then can improve temperature-room type plasticity.
Studies show that, grain refinement is to the raising of the mechanical property of magnesium alloy, its potentiality will be far longer than aluminium alloy, and therefore the obdurability that utilizes advanced material processing method refinement magnesium alloy crystal grain to improve magnesium alloy is one of important channel of improving the wrought magnesium alloy performance.(Liu just according to document, Zhang Kui, Ceng Xiaoqin work, " magnesium base alloy in lightweight theoretical foundation and application thereof ", China Machine Press, in September, 2002 front page: 34) report, adopt the ZK60 high-strength deforming magnesium alloy of extruding+heat-treating methods preparation, its intensity and fracture toughness can be equivalent to the A17075 or the A17475 alloy of timeliness state; Adopting the Mg-Al-Zn of rapid solidification (RS)+powder metallurgy (PM)+hot extrusion combination process exploitation is the EA55RS wrought magnesium alloy, become the magnesium alloy of performance the best of hitherto reported, its performance not only substantially exceeds conventional magnesium alloy, the yield strength 343MPa of its representative extrusion magnesium alloy, percentage elongation 13%, specific strength even surpass 7075 aluminium alloys, and have (300 ℃ of superplasticity, 436%), corrosion rate is suitable with the 2024-T6 aluminium alloy; The high-strength magnesium alloy Mg-2at% Y-1at% Zn that adopts rapid solidification method to make with 100～200nm crystallite dimension, its intensity is 3 times of super aluminium alloy, also has superplasticity, high-fire resistance and high corrosion-resistant; Document (T.Mukai, M.Yamanoi, H.Watanabe, H.Higashi, Ductility enhancement in AZ31 magnesium alloyby controlling its grain structure, Scripta Mater., 45 (2001), 89-94) report, utilize equal channel angular extruding (Equal Channel Angle Press, ECAP) the method texture intensity for preparing the AZ31 magnesium alloy obviously dies down, and its room temperature tensile plasticity (～50%) exceeds nearly three times than the AZ31 magnesium alloy (～17%) of conventional extruded method preparation, has high work hardening rate simultaneously.Though said method can significantly have been improved the temperature-room type plasticity of magnesium alloy, preparation equipment needed thereby costliness and complex technical process only limit to experimental study usually, are difficult in industrial extensive use.Utilize the existing process equipment of present industrial quarters, prepare the good magnesium alloy of plasticity by the improvement of technology and method and have important engineering application value.
Summary of the invention
The present invention wants the technical solution problem to provide the method that a kind of low cost prepares high-temperature-room type plasticity magnesium alloy sheet material.
Principle of the present invention is:
When the die hole of the dissymmetrical structure up and down that adopts by the present invention without the magnesium alloy of plastic deformation, the plastic flow that will on the position of the both sides up and down of the die hole of dissymmetrical structure, produce different rates, this asymmetric plastic flow that produces by shearing stress will cause magnesium alloy { the 0002} basal slip carries out along the shear direction, make in the magnesium alloy plate after the hot extrusion { the 0002} basal plane has taken place to vert, { the 0002} crystal face is parallel to the basal plane texture intensity reduction of plate face, improved the orientation factor of 0002} face sliding system, thereby acquisition has the magnesium alloy plate than high-temperature-room type plasticity.
Technical scheme of the present invention is to adopt to have up and down the mould of asymmetric rectangle nib and carry out hot extrusion and prepare magnesium alloy plate, and this rectangle nib of dissymmetrical structure up and down is traditional rectangle nib upside or downside to be carried out chamfer machining handle and obtain.Utilize the die hole of this up and down dissymmetrical structure in the magnesium alloy plate hot extrusion process, to introduce shearing stress, that the sheet material after causing pushing has is more weak 0002} basal plane texture, thus obtain to have magnesium alloy plate than high-temperature-room type plasticity.
Rectangle nib upside or downside can be the plane chamferings, and the angle of chamfering is 20-60 °, and the best is 45 °.Rectangle nib upside or downside can be bent angle chamferings, and the radius of curvature of chamfering is 1-10mm, and the best is 3mm.
Effect of the present invention and benefit are:
Under the condition that does not change magnesium alloy composition and technology, utilize existing extrusion machining equipment that mould is improved slightly and can implement the present invention, preparation cost is low, is suitable for modern industry large-scale production, and is applicable to the magnesium alloy hot extrusion processing of any trade mark.
Description of drawings
Fig. 1 is a technical process schematic diagram of the present invention.
1 extruder head; 2 extruders are contained the ingot bucket; 3 magnesium alloy ingots to be extruded; 4 hot-extrusion molds;
The sheet material that 5 hot extrudes extrude; 6 die hole chamfer angles.
The specific embodiment
The AZ31 magnesium alloy ingot is buied in market.Employing has the extrusion die of the rectangle nib of dissymmetrical structure up and down, and the angle that the rectangle nib upside of mould or downside have chamfering is 45 °.Magnesium alloy ingot is processed into the bar of Φ 60mm * 100mm, places in the Sheng ingot bucket of extruder.Be heated to 350 ℃, insulation 1h carries out an extrusion modling afterwards, and resultant magnesium alloy plate is of a size of 30mm * 2mm.Its microstructure is an equiax crystal, and average grain size is 8 μ m; Room temperature percentage elongation δ average is 26%.
Claims (4)
1. method for preparing high-temperature-room type plasticity magnesium alloy sheet material, have up and down the mould of asymmetric rectangle nib with employing and carry out hot extrusion and prepare magnesium alloy plate, this rectangle nib of dissymmetrical structure up and down is traditional rectangle nib upside or downside to be carried out chamfer machining handle and obtain; This die hole of dissymmetrical structure is up and down introduced shearing stress in the magnesium alloy plate hot extrusion process, sheet material after causing pushing has more weak { 0002} basal plane texture, acquisition has the magnesium alloy plate than high-temperature-room type plasticity, it is characterized in that: rectangle nib upside or downside are the plane chamferings, and the angle of chamfering is 20～60 °.
2. a kind of method for preparing high-temperature-room type plasticity magnesium alloy sheet material according to claim 1, the angle that it is characterized in that chamfering is 45 °.
3. method for preparing high-temperature-room type plasticity magnesium alloy sheet material, have up and down the mould of asymmetric rectangle nib with employing and carry out hot extrusion and prepare magnesium alloy plate, this rectangle nib of dissymmetrical structure up and down is traditional rectangle nib upside or downside to be carried out chamfer machining handle and obtain; This die hole of dissymmetrical structure is up and down introduced shearing stress in the magnesium alloy plate hot extrusion process, sheet material after causing pushing has more weak { 0002} basal plane texture, acquisition has the magnesium alloy plate than high-temperature-room type plasticity, it is characterized in that rectangle nib upside or downside are the curved surface chamferings, the radius of curvature of chamfering is 1～10mm.
4. a kind of method for preparing high-temperature-room type plasticity magnesium alloy sheet material according to claim 3, the radius of curvature that it is characterized in that chamfering is 3mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100111593A CN100488653C (en) | 2007-04-26 | 2007-04-26 | Method for preparing high-temperature-room type plasticity magnesium alloy sheet material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100111593A CN100488653C (en) | 2007-04-26 | 2007-04-26 | Method for preparing high-temperature-room type plasticity magnesium alloy sheet material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101041167A CN101041167A (en) | 2007-09-26 |
| CN100488653C true CN100488653C (en) | 2009-05-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB2007100111593A Expired - Fee Related CN100488653C (en) | 2007-04-26 | 2007-04-26 | Method for preparing high-temperature-room type plasticity magnesium alloy sheet material |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101066817B1 (en) * | 2010-05-18 | 2011-09-23 | 강릉원주대학교산학협력단 | Asymmetric extracting method, extracted materials fabricated by using the method, dice for asymmetric extraction and asymmetric extraction apparatus |
| CN102172662A (en) * | 2010-12-31 | 2011-09-07 | 重庆大学 | Magnesium alloy thin plate strip blank extruding die |
| CN108772430B (en) * | 2018-06-05 | 2019-08-02 | 重庆大学 | A kind of magnesium alloy sheet made-up belt pressurizing unit and extrusion process |
| CN108787771B (en) * | 2018-06-05 | 2019-07-26 | 重庆大学 | A kind of acquisition room temperature high plastic magnesium alloy thin sheet strip plate pressurizing unit and extrusion process |
| CN109940094B (en) * | 2019-04-19 | 2021-04-16 | 重庆科技学院 | Mold and method for regulating and controlling formability of magnesium alloy plate through gradient strain |
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- 2007-04-26 CN CNB2007100111593A patent/CN100488653C/en not_active Expired - Fee Related
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| CN101041167A (en) | 2007-09-26 |
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Granted publication date: 20090520 Termination date: 20120426 |