CN100452992C - Water soluble composite nutrient reinforcer - Google Patents
Water soluble composite nutrient reinforcer Download PDFInfo
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- CN100452992C CN100452992C CNB021336458A CN02133645A CN100452992C CN 100452992 C CN100452992 C CN 100452992C CN B021336458 A CNB021336458 A CN B021336458A CN 02133645 A CN02133645 A CN 02133645A CN 100452992 C CN100452992 C CN 100452992C
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- calcium
- hydrotropy
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Abstract
The present invention discloses a water-soluble organic calcium compound nutrition intensifier and a preparation method thereof. In the method, active calcium is treated by acid dissolution, acid washing, drying for acid elimination, compounding with VD, magnesium and xanthan, mixing dissolution by sterile purified water, glue milling for emulsification, micronization, high-speed spray drying or heat drying and micropowder grinding into 100 to 150 meshes, and the product is prepared. One type of product of the present invention is used for intensifying calcium nutrition of water solution foods without souring agent or ethanol substance, or preparing calcium nutrition oral liquids; the other type of product is used for intensifying calcium nutrition of dry powdery or pasty foods, or pressing calcium nutrition supplement tablets. The products of the present invention have the advantages of complete dissolution in water solution food, no precipitation or deterioration within product shelf life, no influence on carrier quality, high biologic organic calcium nutrient content, high activity, no stimulation to the intestine or stomach, good absorption and utilization and synergistic action with compatible nutrient.
Description
Technical field
The present invention relates to the food additives field.More particularly, the present invention relates to a kind of compound method that is used for the water soluble composite nutrient reinforcer of food nutrient fortifying, and the application of this nutrition fortifier.
Background technology
China's approval at present is used for the calcium-nutrition intensifying agent of fortification, belongs to undissolved inorganic calcium of water or organic calcium mostly.The undissolved calcium constituent body of water utility scale is compared and is lower than water-soluble calcium constituent.In addition, have a small amount of water-soluble as calcium gluconae, calcium lactate etc. because effective element content is low, the price height can not generally use, as " food additives handbook, " the polycalcium hardening agent of enumerating in the natural additive for foodstuff handbook.
In addition, since the interaction of calcium and other element, though calcium that can be water-soluble after making some processed, also can be after the fortification that is used for some aqueous solution food, the acidolysis of saltouing of the salt that its calcium constituent is contained in the liquid, acid becomes floccule precipitation, does not reach the intended purposes of fortification.
In recent years research also shows, replenishes the calcium merely or edible high calcium meals, can not promote the effective absorption or the deposition of calcium constituent; Can help calcium to absorb even add VD.Simple pay attention to replenishing the calcium and ignore the balanced action of other nutrient, might hinder the absorption of calcium constituent or quicken the drainage of calcium constituent.Data shows, proportioning VD, magnesium etc. in calcium constituent, and to the absorption of calcium, the balance between deposition and element can both play better synergistic function.
On the other hand, although the inorganic calcium biologically active is strong on year-on-year basis for the organic calcium made from biomaterial, calcium element content height, the performance that absorbs, but simultaneously also because this type of calcium is too strong because of the alkalescence that itself contained, to people's stomach stimulate too big and lost by widespread usage may.
Summary of the invention
The objective of the invention is to overcome above-mentioned shortcoming, calcium that can not be water-soluble is made water-soluble calcium fully by acidolysis, and utilize acetate on the alkalescence of removing in the calcium constituent, when being applied to the calcium-nutrition intensifying of some class aqueous solution food, calcium constituent is fully miscible in liquid is not saltoutd into the floccule precipitation by other material in the liquid in order to make, then make full use of xanthans and can and impel the stable effect of its calcium constituent with most of salt compatibilities, a certain amount of food-grade xanthans of proportioning makes the calcium constituent and the element that matches can play emulsification in liquid, suspend, stable effect.
Simultaneously, easily cause the shortcoming of calcium constituent and other nutrient proportional imbalance, improve the absorption and the deposition of calcium constituent in order to overcome to replenish the calcium merely, with reference to " DRIs " standard, the relevant nutrient of suitable compatibility.Also wishing simultaneously to provide a kind of biologically active strong to people in real life, and organic calcium constituent content height absorbs, and has no side effect and the water soluble composite nutrient reinforcer of the high effect of fine quality of relative low price.
This nutrition fortifier is with following nutrient proportioning:
With the effective calcium constituent of 10-1000mg calcium activated is matching criterion, proportioning VD0.2-20 μ g, magnesium 4-400mg, food-grade xanthans 100-400mg.
The technical program is achieved with following production routine:
1, the food-grade glacial acetic acid being mixed with acetic acid content by the standard of 3 parts, 2 parts, 1 part sterile purified waters of 1 part of glacial acetic acid solution proportioning, to be respectively 25%, 33%, 50% acetate hydrotropy liquid stand-by.
2, acetate hydrotropy liquid made a gesture of measuring by the solution amount of the 350-550% of the calcium powder amount of proportioning hydrotropy put in food grade plastic container or the ceramic-like container, to treat that molten calcium powder pours in the container, stir with waddy, it is real to clap leveling, closed container, after hydrotropy 5-10 hour, check as find too drying of calcium powder, then suitably replenish the acetate hydrotropy liquid of 5-10% in the calcium powder surface, continue closed container, but openable container lid after 24 hours is smashed the caked dissolving calcium powder of acid to pieces. make its continuation fully miscible, and continued closed container 30-130 hour, check during this period as hydrotropy finish then keep somewhere stand-by.
3, the calcium lysate of hydrotropy being finished is washed acid with the sterile purified water dilution that is equivalent to calcium liquid 60-120%, and calcium lysate after the acid is washed in dilution put and be warming up to 85-120 ℃ in stainless-steel pan or the heater, remove molecular acid or other smell that remains in the calcium liquid with evaporation moisture content, the dry deacidification of also available high velocity fog drying machine, it is standby to get dried dissolving calcium powder.
4, with dried dissolving calcium powder by materials such as effective calcium element content proportioning VD, magnesium, xanthans, with the batch mixing mixer or manually mix.
5, the compound calcium powder after will mixing needs to adjust its density by producing by the sterile purified water stirring and dissolving of its amount of dry matter with 80-160%, send the colloid mill glue mill twice that circles round, and is miscible to reach emulsification, the purpose of miniaturization.
6, with the calcium composite nutrient-fluid of glue mill back gained according to producing needs/or add sterile purified water and adjust its density, with making this product after the high velocity fog drying machine drying; Also the calcium composite nutrient-fluid of glue mill back gained can be put in stainless-steel pan or the heater after the intensification drying, fine with micropowder grinding to granularity 100-150 order, promptly make this product.
Different proportional quantity acetate hydrotropy liquid relatively see Table 1 to each index of calcium powder hydrotropy.
The specific embodiment
By following examples, can do further understanding to the present invention.
Example 1:100ml the make soy sauce effective calcium constituent 10-100mg of proportioning, VD0.2-2 μ g, magnesium 4-40mg, xanthans 100-150mg.
Example 2:100ml the make soy sauce effective calcium constituent 100-300mg of proportioning, VD2-6 μ g, magnesium 40-120mg, xanthans 150-200mg.
Example 3:100ml the make soy sauce effective calcium constituent 300-500mg of proportioning, VD6-10 μ g, magnesium 120-200mg, xanthans 200-250mg.
Example 4:100ml the make soy sauce effective calcium constituent 500-700mg of proportioning, VD10-14 μ g, magnesium 200-280mg, xanthans 250-300mg.
Example 5:100ml the make soy sauce effective calcium constituent 700-900mg of proportioning, VD14-18 μ g, magnesium 280-360mg, xanthans 300-350mg.
Example 6:100ml the make soy sauce effective calcium constituent 1000mg of proportioning, VD20 μ g, magnesium 400mg, xanthans 400mg.
With example 1---the various material proportional quantities of example 6 multiply by 6 respectively, make water soluble composite nutrient reinforcer by the amount that multiplier draws respectively with aforementioned production routine, add in 600ml makes soy sauce, miscible get after evenly 400ml fortification soy sauce leave standstill do each 2 months totally 4 times 8 months precipitation detect; 200ml does 5 detections such as figure, color and luster, fragrance, flavour, eating mouth feel in addition.(the eating mouth feel detection uses enriched soy sauce and poach noodles mixed edible to detect, and with other the edible respectively detection of enriched soy sauce of similar level, compares its mouthfeel, does not add other auxiliary flavoring during edible the detection).After 8 months, get again with a 400ml and leave standstill enriched soy sauce, and compare with a testing result, check its variation situation with the initial stage by same detection of above-mentioned 5 detection methods work.
Table 1, different proportional quantity acetate hydrotropy liquid are to each index of calcium powder hydrotropy relatively.
Detect stationary phase behind table 2, the water soluble composite nutrient reinforcer enriched soy sauce.
Table 3, the water soluble composite nutrient reinforcer enriched soy sauce is made 5 indexs detect.
Table 4, the water soluble composite nutrient reinforcer enriched soy sauce is remake 5 indexs detect after depositing 8 months.
Claims (7)
1, a kind of compound method of water soluble composite nutrient reinforcer, it is included in effective calcium constituent of 10-1000mg, proportioning 0.2-20 μ gVD, 4-400mg magnesium, 100-400mg food-grade xanthans is characterized in that, it is achieved with following production routine:
(1) the food-grade glacial acetic acid being mixed with acetic acid content in the ratio of 1 part, 2 parts, 3 parts sterile purified water of 1 part of glacial acetic acid proportioning, to be respectively 25%, 33%, 50% acetate hydrotropy liquid stand-by;
(2) acetate hydrotropy liquid is packed into earlier in food grade plastic container or the ceramic-like container in the solution amount ratio of the 350-550% that answers hydrotropy calcium powder amount, again calcium powder is added in the container, stir with waddy, it is real to clap leveling, closed container, after hydrotropy 5-10 hour, check as find too drying of calcium powder, the acetate hydrotropy liquid of then suitably adding 5-10% is in the calcium powder surface, closed container continues hydrotropy, but openable container lid after 24 hours, the caked dissolving calcium powder of acid smashed to pieces mix thoroughly, it is fully mixed and continue to check in sour molten 30-130 hour that hydrotropy finishes;
(3) the calcium liquid of hydrotropy being finished dilutes with the sterile purified water that is equivalent to calcium liquid 60-120%, put and be warming up to 85-120 ℃ in stainless-steel pan or the heater, fully evaporate moisture content, remove molecular acid residual in the calcium liquid or other smell, the dry deacidification of also available high velocity fog drying machine gets dry dissolving calcium powder;
(4) dried dissolving calcium powder is pressed effective element calcium content proportioning VD, magnesium, xanthans, even with batch mixing mixer or manual mixing;
(5) the compound calcium powder that mixes is added the sterile purified water stirring and dissolving in the ratio of amount of dry matter 80-160%, send the colloid mill glue mill twice that circles round, make that compound calcium powder is fully emulsified, miscible, miniaturization;
(6) with the calcium composite nutrient-fluid behind the glue mill according to producing needs or adding a small amount of sterile purified water and adjust its density, send after the high velocity fog drying machine spray-drying product; Also glue can be ground calcium composite nutrient-fluid after the emulsification and send in stainless-steel pan or the heater after the intensification drying, fine with micropowder grinding to granularity 100-150 order.
2, the compound method of water soluble composite nutrient reinforcer according to claim 1 is characterized in that, the acetic acid content of hydrotropy liquid is 33%.
3, the compound method of water soluble composite nutrient reinforcer according to claim 1 is characterized in that, the proportional quantity of acetate hydrotropy liquid and calcium powder is the 400-500% of calcium powder amount.
4, the compound method of water soluble composite nutrient reinforcer according to claim 1 is characterized in that, it is 35-120 hour that calcium powder combines the hydrotropy time with acetate hydrotropy liquid.
5, the compound method of water soluble composite nutrient reinforcer according to claim 1 is characterized in that, the calcium lysate is added the sterile purified water dilution of 80-100% and washes acid.
6, the compound method of water soluble composite nutrient reinforcer according to claim 1 is characterized in that, the temperature that the calcium lysate heating deacidification after the acid is washed in dilution is 95-105 ℃.
7, the compound method of water soluble composite nutrient reinforcer according to claim 1 is characterized in that, the sterile purified water addition of the mixed compound calcium powder of proportioning is 100-150%; Glue grinder preface is ground twice for the glue that circles round.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021336458A CN100452992C (en) | 2002-08-22 | 2002-08-22 | Water soluble composite nutrient reinforcer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021336458A CN100452992C (en) | 2002-08-22 | 2002-08-22 | Water soluble composite nutrient reinforcer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1398549A CN1398549A (en) | 2003-02-26 |
| CN100452992C true CN100452992C (en) | 2009-01-21 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB021336458A Expired - Fee Related CN100452992C (en) | 2002-08-22 | 2002-08-22 | Water soluble composite nutrient reinforcer |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102499337A (en) * | 2011-10-14 | 2012-06-20 | 浙江大学 | Preparation method of bioactive calcium jelly by using procambarus clarkii shells |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1132626A (en) * | 1994-09-26 | 1996-10-09 | 美国氰胺公司 | Improved calcium dietary supplement |
| CN1344512A (en) * | 2001-09-30 | 2002-04-17 | 张昌华 | Food nutrient fortifying method with aqueous solution containing no acetic acid and ethanol |
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2002
- 2002-08-22 CN CNB021336458A patent/CN100452992C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1132626A (en) * | 1994-09-26 | 1996-10-09 | 美国氰胺公司 | Improved calcium dietary supplement |
| CN1344512A (en) * | 2001-09-30 | 2002-04-17 | 张昌华 | Food nutrient fortifying method with aqueous solution containing no acetic acid and ethanol |
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| Publication number | Publication date |
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| CN1398549A (en) | 2003-02-26 |
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