CN100399928C - Preparation method of yellow gumbo freeze dried powder - Google Patents

Preparation method of yellow gumbo freeze dried powder Download PDF

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Publication number
CN100399928C
CN100399928C CNB2005100621347A CN200510062134A CN100399928C CN 100399928 C CN100399928 C CN 100399928C CN B2005100621347 A CNB2005100621347 A CN B2005100621347A CN 200510062134 A CN200510062134 A CN 200510062134A CN 100399928 C CN100399928 C CN 100399928C
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China
Prior art keywords
okra
dried powder
freeze dried
preparation
ethanol
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Expired - Fee Related
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CNB2005100621347A
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Chinese (zh)
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CN1823855A (en
Inventor
汤谷平
胡秀荣
周峻
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Zhejiang University ZJU
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Zhejiang University ZJU
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Publication of CN100399928C publication Critical patent/CN100399928C/en
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  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention provides a preparation method of lyophiled powder of okra. One part of okra seed is added into three to five parts of water to be boiled for 3 to 5 hours and is filtered; three to five parts of water is added into the mixture again to be boiled for 3 to 5 hours and is filtered, and filtrate is merged and is concentrated until okra accounts for 85 wt% to 95 wt% of the filtrate; equivalent ethanol with the concentration of 95% is added into the concentrated solution, and thus, the final concentration of the ethanol is from 50% to 55%; brown deposit is obtained and is filtered; the deposit is washed by using equivalent ethanol with the concentration of 95% for two to three times and is dissolved in equivalent water; the solution is concentrated until the okra accounts for 80 wt% to 98 wt% of the solution; the concentrated solution is lyophilized at the temperature of-25 DEG C to 10 DEG C, and the lyophiled powder can be obtained. The preparation method can fully utilize use ingredients of okra, and the lyophiled powder of the okra can be made into various okra health care foods.

Description

The preparation method of yellow gumbo freeze dried powder
Technical field
The present invention relates to a kind of preparation method of yellow gumbo freeze dried powder.
Background technology
At present a lot of about the health products of antifatigue, some is that the extract of natural plants processes, some is Bio-engineering Products, trend from present multiple disease, imbalance causes a lot of diseases because body in allegro environment is to environmental stress, need exploitation to relate to resist stress product.
Okra (Okra) belongs to Malvaceae (Malvaceae), and Abelmoschus (Abelmoschus Medic) claims (linn) plant of coffee ambrette (Abelmoschus esculentus) again.Originate in India, existing extensively the cultivation in the torrid zone and torrid areas.Because it is rich in multiple bioactive ingredients such as pectin, Arabic gum, galactan and alkaloid, in developed countries such as North America, Japan with fresh okra as the first-selected vegetables of sportsman's antifatigue and old health-care vegetable, its seed can be used as the substitute of coffee after processing, has the effect of refreshing oneself preferably, decaffeinated, okra has the effect of anti-heat stress, antifatigue and enhancing immunocompetence.
Though fresh okra can be directly as health-care vegetable, it is short to exist the shelf-life, and the okra effective ingredient can not make full use of, can not be directly edible as the health product of okra.
Summary of the invention
The purpose of this invention is to provide and a kind ofly can make full use of the okra effective ingredient, can directly make the yellow gumbo freeze dried powder preparation method of the health food of multiple okra.
Yellow gumbo freeze dried powder preparation method of the present invention is:
(1) gets a certain amount of setose abelmoschus seed, add the water of 3-5 times of weight, boiled 3-5 hour, filter;
(2) in filter residue, add the water of 3-5 times of weight again, boiled 3-5 hour, filter;
(3) step 1,2 filtrate are merged, concentrated filtrate okra weight percentage to the filtrate is 85-95%;
(4) in concentrate, add equal volume amounts 95% ethanol, make that the ethanol ultimate density is 50-55%, filter sediment;
(5) sediment cleans 2-3 time with 95% ethanol of 2-3 times of weight;
(6) sediment after the cleaning is separated with the water-soluble of 2-3 times of weight;
(7) to be concentrated into the okra weight percentage be 80-98% to lysate;
(8) with above-mentioned concentrate in-25 ∽-10 ℃ freeze drying, promptly get yellow gumbo freeze dried powder of the present invention.
Beneficial effect of the present invention:
Yellow gumbo freeze dried powder of the present invention is a raw material with the natural plants okra, has kept the function that natural plants had, and has the effect of anti-heat stress, antifatigue and enhancing immunocompetence.
Yellow gumbo freeze dried powder of the present invention can directly be made okra capsule, is used to prepare the raw material of beverage of yellow mallow, has easy preservation, guarantees the quality the advantage that effective ingredient can make full use of.
Concrete embodiment
Embodiment
(1) takes by weighing setose abelmoschus seed 500 grams, add the 1500-2500 ml distilled water, boiled 3-5 hour, filter;
(2) in filter residue, add the 1500-2500 ml distilled water again, boiled 3-5 hour, filter;
(3) step 1,2 filtrate are merged, concentrated filtrate is to the 500-700 milliliter;
(4) concentrate is joined in 500-700 milliliter 95% ethanol, makes that the ethanol ultimate density is 50-55%, filter sediment;
(5) 95% ethanol of sediment with 200-300 milliliter 95% ethanol is cleaned 2-3 time;
(6) sediment after the cleaning is separated with the water-soluble of 200-300 milliliter;
(7) lysate is concentrated into the 100-150 milliliter;
(8) with the above-mentioned concentrate of 100-150 milliliter-20 ℃ of freeze dryings, promptly get yellow gumbo freeze dried powder of the present invention.
Practical example 1
Above-mentioned yellow gumbo freeze dried powder can be made into by following prescription have anti-heat stress, the okra capsule of antifatigue.
Yellow gumbo freeze dried powder 20 grams
Food coloring 0.5 gram
Auxiliary material adds to 1000 grams
The former section of above-mentioned prescription is made every contain the capsule that weight is 0.02 gram.
Practical example 2
Above-mentioned yellow gumbo freeze dried powder can be made into by following prescription have anti-heat stress, the okra oral liquid of antifatigue.
Abelmoschus Esculentus Linn extract freeze-dried powder 20 grams
White granulated sugar 100 grams
Pure water adds to 1000 milliliters.
With the former section of above-mentioned prescription by oral liquor make contain weight be every 0.02 the gram the okra oral liquid.

Claims (3)

1. the preparation method of a yellow gumbo freeze dried powder the steps include:
(1) gets a certain amount of setose abelmoschus seed, add the water of 3-5 times of weight, boiled 3-5 hour, filter;
(2) in filter residue, add the water of 3-5 times of weight again, boiled 3-5 hour, filter;
(3) step 1,2 filtrate are merged, concentrated filtrate okra weight percentage to the filtrate is 85-95%;
(4) in concentrate, add equal volume amounts 95% ethanol, make that the ethanol ultimate density is 50-55%, filter sediment;
(5) sediment cleans 2-3 time with 95% ethanol of 2-3 times of weight;
(6) sediment after the cleaning is separated with the water-soluble of 2-3 times of weight;
(7) to be concentrated into the okra weight percentage be 80-98% to lysate;
(8) with above-mentioned concentrate in-25 ∽-10 ℃ freeze drying, promptly get yellow gumbo freeze dried powder.
2. the preparation method of yellow gumbo freeze dried powder according to claim 1 is characterized in that described freeze drying temperature is-20 ℃.
3. the preparation method of the described yellow gumbo freeze dried powder of claim 1 obtains yellow gumbo freeze dried powder, it is characterized in that being used to prepare okra capsule or okra oral liquid.
CNB2005100621347A 2005-12-21 2005-12-21 Preparation method of yellow gumbo freeze dried powder Expired - Fee Related CN100399928C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2005100621347A CN100399928C (en) 2005-12-21 2005-12-21 Preparation method of yellow gumbo freeze dried powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2005100621347A CN100399928C (en) 2005-12-21 2005-12-21 Preparation method of yellow gumbo freeze dried powder

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CN1823855A CN1823855A (en) 2006-08-30
CN100399928C true CN100399928C (en) 2008-07-09

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Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101797274B (en) * 2010-04-09 2011-12-21 三门富达果蔬专业合作社 Preparation technology of okra capsule
CN102008081B (en) * 2010-11-11 2012-09-26 浙江农林大学 Abelmoschus manihot leaf extract and production method of health-care instant tea thereof
CN102002172B (en) * 2010-11-11 2012-07-11 浙江农林大学 Method for preparing okra polysaccharide and pectin as well as pill preparation thereof
CN103070399B (en) * 2011-12-20 2014-07-02 王显奉 Processing method of okra food additive
CN102640788B (en) * 2012-04-25 2013-03-27 浙江佳伊乐食品有限公司 Processing method of nutritional frozen Hibiscus esculentus slice
CN104336259A (en) * 2014-10-30 2015-02-11 厦门如意食品有限公司 Preparation technology of okra herbal tea
CN106074868A (en) * 2016-07-15 2016-11-09 浙江省海洋开发研究院 A kind of selenizing polysaccharide immunostimulant
CN107095305A (en) * 2017-04-26 2017-08-29 湖南文理学院 A kind of preparation method of okra colloid polyoses oral liquid
CN108967789A (en) * 2018-08-21 2018-12-11 福建省农业科学院亚热带农业研究所(福建省农业科学院蔗麻研究中心) A kind of method of okra seed processing beverage

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1205878C (en) * 2002-01-15 2005-06-15 龙海市东海冷冻食品有限公司 Production process of frozen cut setose abelmoschus food

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1205878C (en) * 2002-01-15 2005-06-15 龙海市东海冷冻食品有限公司 Production process of frozen cut setose abelmoschus food

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
黄秋葵抗疲劳作用的研究. 王君耀等.中国现代应用药学杂志,第20卷第4期. 2003
黄秋葵抗疲劳作用的研究. 王君耀等.中国现代应用药学杂志,第20卷第4期. 2003 *

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