CN100393176C - Automatic thermostatic heater - Google Patents

Automatic thermostatic heater Download PDF

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Publication number
CN100393176C
CN100393176C CNB2005100201196A CN200510020119A CN100393176C CN 100393176 C CN100393176 C CN 100393176C CN B2005100201196 A CNB2005100201196 A CN B2005100201196A CN 200510020119 A CN200510020119 A CN 200510020119A CN 100393176 C CN100393176 C CN 100393176C
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CN
China
Prior art keywords
heater
temperature
heat transfer
thermal conductor
heating device
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB2005100201196A
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Chinese (zh)
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CN1645973A (en
Inventor
张新申
蒋小萍
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Sichuan University
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Sichuan University
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Priority to CNB2005100201196A priority Critical patent/CN100393176C/en
Publication of CN1645973A publication Critical patent/CN1645973A/en
Application granted granted Critical
Publication of CN100393176C publication Critical patent/CN100393176C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The present invention relates to an automatic constant temperature heating device. The present invention comprises a casing in which a heater, a heat transfer body, a heating reaction coil, a temperature controlling and measuring instrument, and a temperature sensor are arranged, wherein the heat transfer body is arranged on the heater; the heating reaction coil is wound on the heat transfer body, and the liquor inlet end and the liquor outlet end of the heating reaction coil penetrate through the casing and extend out of the casing; the temperature sensor is arranged in a temperature field formed by the heat transfer body, and the outlet end of the temperature sensor is connected with the input end of the temperature controlling and measuring instrument; the outlet end of temperature controlling and measuring instrument is connected with the power of the heater to control the on-off of the power of the heater. The present invention can also be provided with an insulating sleeve which is sheathed on the heat transfer body and the heater, and the shape and the size of the insulating sleeve can be matched with the shape and size of the combination of the heat transfer body and the heater. The heating device of the present invention is convenient for adjusting and controlling the temperature so as to avoid overheating; the heating reaction coil is evenly heated, the temperature of the fluid which flows through the heating reaction coil is constant and meets the reaction requirements, which is in favor of the assurance of the testing precision.

Description

Automatic constant temperature heating device
Technical field
The invention belongs to the heater that Flow Injection Analysis, ion chromatography, efficient liquid phase chromatographic analysis are used, particularly a kind of automatic constant temperature heating device.
Background technology
Flow Injection Analysis, ion chromatography and efficient liquid phase chromatographic analysis need heated constant temperature when analyzing some material, in such cases, fluid flow through the heating reactor coil, to react at a certain temperature be the essential condition that guarantees measuring accuracy.
Oil bath or water-bath heater and cartridge type heater are generally adopted in the heating of heating reactor coil.Oil bath or water-bath heater mainly are made of the container of heating stirrer and charge of oil or water, during use, the heating reactor coil are placed in the container that a certain amount of oil or water are housed, and oil or water are as heat transfer medium.This kind heater is oil or constantly evaporation of water in heating process, thereby needs makeup oil or water every now and then, not only make troubles to operating personnel, and the constant temperature effect is relatively poor.The cartridge type heater mainly is made of resistance heater and the heat transfer tube that is installed on the heater, and the tube that conducts heat is done by copper, during use, the heating reactor coil is placed in the tube that conducts heat and makes the fluid of the heating reactor coil of flowing through reach certain temperature.The heating of this kind heater is even inadequately, easily overheated in addition, and the fluid that heats reactor coil that causes flowing through produces steam bubble interference analysis detection.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, a kind of automatic constant temperature heating device is provided, this kind heater can make the fluid temperature (F.T.) of the heating reactor coil of flowing through constant and meet the reaction requirement, avoids fluid superheat to produce steam bubble, and is simultaneously easy to operate.
Automatic constant temperature heating device of the present invention comprises shell, is positioned at heater, thermal conductor, heating reactor coil, temperature control temperature instrumentation and the temperature sensor of shell; Thermal conductor is installed on the heater, the heating reactor coil is wrapped on the thermal conductor, its liquid feeding end and outlet end pass shell, temperature sensor is installed in the temperature field of thermal conductor formation, its output is connected with the input of temperature control temperature instrumentation, transmit actual temperature information to the temperature control temperature instrumentation, the output of temperature control temperature instrumentation is connected with the power supply of heater, the break-make of control heater power supply.
During use, the control range of design temperature on the temperature control temperature instrumentation as required, when the fluid temperature (F.T.) of the heating reactor coil of flowing through reaches the control temperature, temperature sensor sends information to the temperature control temperature instrumentation, the temperature control temperature instrumentation cuts off the power supply of heater, when the fluid temperature (F.T.) of the heating reactor coil of flowing through was lower than the control temperature, temperature sensor sent information to the temperature control temperature instrumentation, the power supply of temperature control temperature instrumentation conducting heater.
In order to realize goal of the invention better, the present invention has also taked following technical measures:
1, heater mainly by matrix, be installed in the ceramic heating element on the matrix and connect ceramic heating element and the wire assembly of power supply is formed.
2, thermal conductor constitutes by plate body with perpendicular to the heat transfer sheet of plate body setting, and the heating reactor coil is wrapped on the heat transfer sheet that is provided with perpendicular to plate body; The quantity of heat transfer sheet both can be even number, can be odd number also, but was preferably odd number and is at least three.When heat transfer sheet was odd number, the heating reactor coil was wrapped on the heat transfer sheet at interval, and the heat transfer sheet that is wound with the heating reactor coil is not wound with between the heating plate that heats reactor coil at two.
3, be provided with muff, muff is set on thermal conductor and the heater, and shape and size after its shape and size make up with thermal conductor and heater are complementary.
4, the inwall at muff top is coated with thermal insulation layer.
The present invention has following beneficial effect:
1, owing to disposed temperature control temperature instrumentation and temperature sensor, thereby is convenient to regulating and controlling temperature, makes the fluid temperature (F.T.) of the heating reactor coil of flowing through constant and meet the reaction requirement, avoid overheated.
2, since the ceramic heating element of heater when temperature is elevated to certain value, no longer raise, thereby constant in certain limit from thermal source guaranteed the to flow through fluid temperature (F.T.) of heating reactor coil.
3, the structure of thermal conductor makes the heating reactor coil be heated evenly.
4, the setting of muff and thermal insulation layer not only can improve the heat efficiency, strengthens the constant temperature effect, energy savings, and also the fluid temperature (F.T.) in the heating reactor coil is higher than 50 ℃ of useful lifes that also do not influence the temperature control temperature instrumentation.
5, all members are loaded in the housing, and are rational in infrastructure, easy to operate.
Description of drawings
Fig. 1 is a kind of structure chart of automatic constant temperature heating device of the present invention;
Fig. 2 is the vertical view of Fig. 1;
Fig. 3 is another structure chart of automatic constant temperature heating device of the present invention;
Fig. 4 is the vertical view of Fig. 3;
Fig. 5 is the circuit connection diagram of temperature control temperature instrumentation and heater.
Among the figure, 1-temperature control temperature instrumentation, 2-shell, 3-thermal conductor, 4-heating reactor coil, 5-temperature sensor, 6-matrix, 7-heating element, 8-muff, 9-thermal insulation layer.
Embodiment
Embodiment 1
The structure of the automatic constant temperature heating device in the present embodiment comprises shell 2 as shown in Figure 1 and Figure 2, is positioned at heater, thermal conductor 3, heating reactor coil 4, temperature control temperature instrumentation 1 and the temperature sensor 5 of shell.Thermal conductor 3 constitutes by rectangular slab with perpendicular to the heat transfer sheet of rectangular slab setting, and material is a cast aluminium, and heat transfer sheet has six; The heating reactor coil is wrapped on each heat transfer sheet, and its liquid feeding end and outlet end pass shell 2.Heater by insulating body 6, be installed in the ceramic heating element 7 on the matrix and connect ceramic heating element and the wire assembly of power supply constitutes, the rectangular slab of thermal conductor 3 is installed on the heater.Temperature sensor 5 and temperature control temperature instrumentation 1 are the commercial goods, temperature sensor 5 is installed in the temperature field of thermal conductor 3 formation, its output is connected with the input of temperature control temperature instrumentation 1, the output of temperature control temperature instrumentation 1 be connected with the power supply of heater, the break-make of control heater power supply, as shown in Figure 5.
Embodiment 2
The structure of the automatic constant temperature heating device in the present embodiment as shown in Figure 3, Figure 4.Difference from Example 1 is: 1, the heat transfer sheet of thermal conductor 3 is nine, and heating reactor coil 4 is wrapped on the heat transfer sheet at interval, and the heat transfer sheet that is wound with the heating reactor coil is not wound with between the heating plate that heats reactor coil at two.2, be provided with the muff 8 that compressed asbestos sheet is made, muff 8 is set on thermal conductor and the heater, and shape and size after its shape and size make up with thermal conductor and heater are complementary; The inwall at muff top is coated with the thermal insulation layer 9 that polymeric foamed material is made.

Claims (10)

1. automatic constant temperature heating device, it is characterized in that comprising shell (2), be positioned at the heater of shell, thermal conductor (3), heating reactor coil (4), temperature control temperature instrumentation (1) and temperature sensor (5), thermal conductor (3) is installed on the heater, heating reactor coil (4) is wrapped on the thermal conductor, the liquid feeding end and the outlet end of heating reactor coil pass shell (2), temperature sensor (5) is installed in the temperature field of thermal conductor (3) formation, the output of temperature sensor is connected with the input of temperature control temperature instrumentation (1), and the output of temperature control temperature instrumentation (1) is connected with the power supply of heater.
2. automatic constant temperature heating device according to claim 1, it is characterized in that heater by matrix (6), be installed in the ceramic heating element (7) on the matrix and connect ceramic heating element and the wire assembly of power supply is formed.
3. automatic constant temperature heating device according to claim 1 and 2 is characterized in that thermal conductor (3) constitutes by plate body with perpendicular to the heat transfer sheet of plate body setting, and the heating reactor coil is wrapped on the heat transfer sheet that is provided with perpendicular to plate body.
4. automatic constant temperature heating device according to claim 3, it is characterized in that being odd number and being at least three perpendicular to the quantity of the heat transfer sheet of plate body setting, the heating reactor coil is wrapped on the heat transfer sheet at interval, and the heat transfer sheet that is wound with the heating reactor coil is not wound with between the heating plate that heats reactor coil at two.
5. automatic constant temperature heating device according to claim 1 and 2, it is characterized in that also being provided with muff (8), muff is set on thermal conductor (3) and the heater, and shape and size after its shape and size make up with thermal conductor (3) and heater are complementary.
6. automatic constant temperature heating device according to claim 3 is characterized in that also being provided with muff (8), and muff is set on thermal conductor (3) and the heater, and shape and size after its shape and size make up with thermal conductor (3) and heater are complementary.
7. automatic constant temperature heating device according to claim 4 is characterized in that also being provided with muff (8), and muff is set on thermal conductor (3) and the heater, and shape and size after its shape and size make up with thermal conductor (3) and heater are complementary.
8. automatic constant temperature heating device according to claim 5 is characterized in that the inwall at muff (8) top is coated with thermal insulation layer (9).
9. automatic constant temperature heating device according to claim 6 is characterized in that the inwall at muff (8) top is coated with thermal insulation layer (9).
10. automatic constant temperature heating device according to claim 7 is characterized in that the inwall at muff (8) top is coated with thermal insulation layer (9).
CNB2005100201196A 2005-01-07 2005-01-07 Automatic thermostatic heater Expired - Fee Related CN100393176C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2005100201196A CN100393176C (en) 2005-01-07 2005-01-07 Automatic thermostatic heater

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2005100201196A CN100393176C (en) 2005-01-07 2005-01-07 Automatic thermostatic heater

Publications (2)

Publication Number Publication Date
CN1645973A CN1645973A (en) 2005-07-27
CN100393176C true CN100393176C (en) 2008-06-04

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CNB2005100201196A Expired - Fee Related CN100393176C (en) 2005-01-07 2005-01-07 Automatic thermostatic heater

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Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106841484B (en) * 2017-02-15 2019-01-22 中国工程物理研究院材料研究所 A kind of temperature programming control method for gas chromatography separation

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2630851Y (en) * 2003-06-06 2004-08-04 张晓辉 Gas-phase chromatograph and inductance coupled plasma mass spectrograph/spectrograph combined interface
JP2004281250A (en) * 2003-03-17 2004-10-07 Totoku Electric Co Ltd Temperature controlling device of liquid heating supply equipment
CN2760892Y (en) * 2005-01-07 2006-02-22 四川大学 Automatic constant temperature heating device

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004281250A (en) * 2003-03-17 2004-10-07 Totoku Electric Co Ltd Temperature controlling device of liquid heating supply equipment
CN2630851Y (en) * 2003-06-06 2004-08-04 张晓辉 Gas-phase chromatograph and inductance coupled plasma mass spectrograph/spectrograph combined interface
CN2760892Y (en) * 2005-01-07 2006-02-22 四川大学 Automatic constant temperature heating device

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Granted publication date: 20080604

Termination date: 20130107

CF01 Termination of patent right due to non-payment of annual fee