CN100369299C - Forming method of lead-acid battery electrode plate transplantation - Google Patents

Forming method of lead-acid battery electrode plate transplantation Download PDF

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CN100369299C
CN100369299C CNB2005100970210A CN200510097021A CN100369299C CN 100369299 C CN100369299 C CN 100369299C CN B2005100970210 A CNB2005100970210 A CN B2005100970210A CN 200510097021 A CN200510097021 A CN 200510097021A CN 100369299 C CN100369299 C CN 100369299C
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charging
hours
stage
discharge
current
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CN1794491A (en
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包有富
王瑜
程壮成
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Zhejiang Narada Power Source Co Ltd
Hangzhou Nandu Power Technology Co Ltd
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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Abstract

The present invention provides a forming method for an electrode plate of a lead-acid accumulator. The present invention adopts inner formation and comprises many times of alternating charging and alternating discharging at the first stage and charging at the second stage. In the first stage, charging current is from 0.13 to 0.27 C/A, total charging time is from 35 to 55 hours, discharging current is from 0.13 to 0.27 C/A, discharging time is from 0.5 to 4.5 hours, and still time is from zero to three hours after the first stage is over; capacitance judgment discharging is carried out after stillness, and the charging at the second stage is carried out after the capacitance judgment discharging; in the second stage, charging current is from 0.02C to 0.1 C/A, and total charging time is from 18 to 21 hours, wherein the C expresses the rated capacity of the accumulator. The present invention overcomes the defects of outer formation processes. Compared with the existing inner formation processes, the present invention obviously reduces the forming time within 100 hours, and the productive capacity is improved by more than 30 %. A practice indicates that with the adoption of the technical scheme of the present invention, power consumption is reduced under the condition of increasing the charging current, and unforeseen effect is obtained.

Description

A kind of forming method of lead-acid battery electrode plate transplantation
Technical field
The present invention relates to the chemical synthesizing method of polar plate of lead acid storage battery.
Background technology
The pole plate of early stage lead acid accumulator adopts the outer technology that changes into, and is about to concentrated being placed in the electrolytic bath of pole plate and changes into.This production technology operation is various, and energy consumption is big, and environmental pollution is also more serious.In recent years, in order to overcome this shortcoming, domestic most of producer all adopts the battery internal formation process through technical study and production practices, promptly directly assembles green plate in battery, irritates acid, changes into then.In the present internal formation process, generally all think and adopt comparatively energy savings of trickle charge, therefore the charging current of its main charging stage can not surpass 0.1C/A, be internalized into overlong time but caused like this, the battery line duration needs more than 140 hour even longer, cause manufacturer's equipment and place anxiety, and influence product delivery date.
Summary of the invention
Technical problem to be solved by this invention provides a kind of forming method of lead-acid battery electrode plate transplantation that overcomes above-mentioned defective.The present invention by the following technical solutions; It adopts and is internalized into, it comprises charging and the discharge that the several times of phase I replace, charging current is 0.13～0.27C/A, charging total time is 35～55 hours, discharging current is 0.13～0.27C/A, be 0.5～4.5 hour discharge time, finish static 0～3 hour of back in the phase I, after static, carry out capacity judgement discharge, after judging discharge, capacity carries out the second stage charging again, charging current is 0.02C～0.1C/A, and charging total time is 18～21 hours, and wherein C represents the rated capacity of storage battery.Owing to adopt above technical scheme, the present invention has not only overcome the outer in the past defective that changes into the technology existence, and compares with present internal formation process, can obviously shorten the time of changing into, can will shorten to the time of changing in 100 hours, improve production capacity more than 30%, and, show according to practice, adopt technical scheme of the present invention, under the situation that improves charging current, reduced power consumption on the contrary, obtained beyond thought effect.Below with reference to embodiment method provided by the invention and the effect that obtains are elaborated.
Embodiment
The present invention adopts and is internalized into, promptly directly in battery, assemble green plate, irritate acid, change into then, it comprises charging and the discharge that the main several times that fill the stage replace, charging current is 0.13～0.27C/A, charging total time is 35～55 hours, discharging current is 0.13～0.27C/A, be 0.5～8 hour discharge time, finishes static 0～3 hour of back in the main stage of filling, and carries out capacity judgement discharge after static, after judging discharge, capacity carries out the second stage charging again, charging current is 0.02C～0.1C/A, and charging total time is 18～21 hours, and wherein C represents the rated capacity of storage battery.C is generally the rated capacity of 10 hour rates or 20 hour rates of battery.Indication of the present invention static is meant that pole plate is rested in the acid solution neither charging not to discharge yet.
Below be example with the 12V lead acid accumulator, change into according to technical scheme provided by the invention, table 1 for not on the same group change into the parameter summary sheet, the 1st, 2,3,4,7,8,9,10 group, every group of totally 24 storage batterys, the 5th, 6 group, every group of totally 18 storage batterys.
Table 1:
First group Second group
Step State Current setting value/A Terminal point control Step State Current setting value/A Terminal point control
1 Static 0.5 hour 1 Static 0 hour
Phase I 2 Charging 0.20C 10 hours Phase I 2 Charging 0.15C 15 hours
3 Discharge 0.20C 0.5 hour 3 Discharge 0.15C 1 hour
4 Charging 0.15C 18 hours 4 Charging 0.20C 15 hours
5 Discharge 0.15C 1 hour 5 Discharge 0.20C 1 hour
6 Charging 0.17C 11 hours 6 Charging 0.18C 10 hours
7 Static 0.5 hour 7 Static 1.5 hour
8 Capacity is judged discharge 0.05C 10.8V 8 Capacity is judged discharge 0.1C 10.8V
9 Charging 0.1C 10 hours 9 Charging 0.1C 10 hours
10 Charging 0.02 10 hours 10 Charging 0.02C 10 hours
Amount to 71.5 hours consuming time of power consumption 6.52C Amount to 73.5 hours consuming time of power consumption 6.90C
Continuous table 1:
The 3rd group The 4th group
Step State Current setting value/A Terminal point control Step State Current setting value/A Terminal point control
1 Static 1.5 hour 1 Static 1 hour
Phase I 2 Charging 0.18C 20 hours Phase I 2 Charging 0.16C 25 hours
3 Discharge 0.18C 1 hour 3 Discharge 0.16C 1 hour
4 Charging 0.20C 15 hours 4 Charging 0.20C 12 hours
5 Static 2.5 hour 5 Static 2.0 hour
6 Capacity is judged discharge 0.1C 10.8V 6 Capacity is judged discharge 0.1C 10.8V
7 Charging 0.1C 10 hours 7 Charging 0.1C 10 hours
8 Charging 0.02C 10 hours 8 Charging 0.02C 10 hours
Amount to 70 hours consuming time of power consumption 6.62C Amount to 71 hours consuming time of power consumption 6.44C
Continuous table 1:
The 5th group The 6th group
Step State Current setting value/A Terminal point control Step State Current setting value/A Terminal point control
1 Charging 0.03C 0.5 hour 1 Charging 0.01C 2 hours
Phase I 2 Charging 0.20C 15 hours Phase I 2 Charging 0.15C 20 hours
3 Discharge 0.20C 3.5 hour 3 Discharge 0.15C 2 hours
4-1 Charging 0.27C 5 hours 4-1 Charging 0.25C 5 hours
Static 2 hours Static 2 hours
4-2 Charging 0.15C 22 hours 4-2 Charging 0.13C 20 hours
5 Static 0.5 hour 5 Static 1.5 hour
6 Capacity is judged discharge 0.1C 10.8V 6 Capacity is judged discharge 0.1C 10.8V
7 Charging 0.1C 10 hours 7 Charging 0.1C 10 hours
10 Charging 0.02C 10 hours 10 Charging 0.05C 10 hours
Amount to 78.5 hours consuming time of power consumption 7.165C Amount to 82.5 hours consuming time of power consumption 7.07C
Continuous table 1:
The 7th group The 8th group
Step State Current setting value/A Terminal point control Step State Current setting value/A Terminal point control
1 Charging 0.02C 0.5 hour 1 Static 2 hours
Phase I 2 Charging 0.20C 16 hours Phase I 2 Charging 0.15C 20 hours
3 Discharge 0.20C 2 hours 3 Discharge 0.15C 1 hour
4 Charging 0.15C 13 hours 4 Charging 0.20C 15 hours
5 Discharge 0.15C 2 hours 5 Discharge 0.20C 5 hours
6 Charging 0.17C 10 hours 6 Charging 0.18C 12 hours
7 Discharge 0.1C 0.5 hour
8 Charging 0.1C 8 hours
9 Static 0.5 hour 7 Static 1 hour
10 Capacity is judged discharge 0.1C 10.8V 8 Capacity is judged discharge 0.1C 10.8V
11 Charging 0.1C 10 hours 9 Charging 0.1C 10 hours
12 Charging 0.02C 10 hours 10 Charging 0.02 10 hours
Amount to 82.5 hours consuming time of power consumption 7.11C Amount to 86 hours consuming time of power consumption 7.21C
Continuous table 1:
The 9th group The tenth group
Step State Current setting value/A Terminal point control Step State Current setting value/A Terminal point control
1 Charging 0.02C 0.5 hour 1 Static 2 hours
Phase I 2 Charging 0.14C 28 hours Phase I 2 Charging 0.23C 12 hours
3 Discharge 0.14C 4 hours 3 Discharge 0.23C 2.5 hour
4 Charging 0.25C 12 hours 4 Charging 0.13C 26 hours
5 Discharge 0.25C 4 hours 5 Discharge 0.13C 2 hours
6 Charging 0.21C 6 hours 6 Charging 0.14C 10 hours
7 Discharge 0.08C 0.5 hour 7 Discharge 0.04C 1 hour
8 Charging 0.08C 6 hours 8 Charging 0.04C 10 hours
9 Static 2.5 hour 9 Static 1.5 hour
10 Capacity is judged discharge 0.1C 10.8V 10 Capacity is judged discharge 0.1C 10.8V
11 Charging 0.1C 10 hours 11 Charging 0.1C 10 hours
12 Charging 0.02C 10 hours 12 Charging 0.02C 10 hours
Amount to 93.5 hours consuming time of power consumption 7.27C Amount to 97 hours consuming time of power consumption 7.265C
Below be example with the 12V lead acid accumulator, change into according to present internal formation process, table 2 is for changing into the parameter summary sheet, this group totally 24 storage batterys.Table 2:
The 11 group
Step State Current setting value/A Terminal point control
1 Charging 0.05C 2 hours
2 Charging 0.100C 30 hours
3 Counter filling 0.100C 0.5 hour
4 Charging 0.100C 20 hours
5 Counter filling 0.100C 0.5 hour
6 Charging 0.05C 15 hours
7 Counter filling 0.05C 15 hours
8 Charging 0.100C 10 hours
9 Charging 0.05C 20 hours
10 Counter filling 0.100C 10 hours
11 Charging 0.100C 10 hours
12 Charging 0.05C 10 hours
Amount to 143 hours consuming time of power consumption 7.5C
Table 3 is the above-mentioned result of the test statistical form of respectively organizing after changing into, and voltage unit wherein is volt.Table 3:
Group First group Second group The 3rd group The 4th group
The battery numbering Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage
1 11.10 13.259 11.17 13.438 11.15 13.780 11.03 13.159
2 11.12 13.468 11.28 13.377 11.06 13.496 11.08 13.610
3 11.17 13.640 11.32 13.550 11.13 13.806 11.12 13.547
4 11.09 13.244 11.32 13.512 11.06 13.462 11.16 13.806
5 11.08 13.260 11.23 13.587 11.17 13.504 11.06 13.358
6 11.05 13.250 11.28 13.456 11.01 13.500 11.09 13.435
7 11.12 13.605 11.27 13.477 11.05 13.454 11.05 13.160
8 11.13 13.200 11.27 13.301 11.00 13.462 11.15 13.585
9 11.14 13.264 11.14 13.484 11.09 13.482 11.08 13.386
10 11.11 13.315 11.26 13.580 11.12 13.578 11.13 13.807
11 11.11 13.206 11.22 13.360 11.13 13.520 11.10 13.806
12 11.05 13.247 11.30 13.368 11.09 13.764 11.05 13.805
13 11.17 13.468 11.27 13.670 11.12 13.536 11.27 13.544
14 11.14 13.467 11.32 13.378 11.17 13.544 11.19 13.385
15 11.13 13.494 11.30 13.420 11.15 13.510 11.17 13.235
16 11.12 13.254 11.28 13.515 11.19 13.340 11.15 13.191
17 11.18 13.580 11.30 13.645 11.15 13.701 11.24 13.418
18 11.15 13.590 11.28 13.480 11.16 13.800 11.18 13.657
19 11.10 13.465 11.29 13.601 11.13 13.786 11.01 13.184
20 11.10 13.600 11.27 13.320 11.08 13.621 11.12 13.371
21 11.04 13.456 11.26 13.290 11.13 13.562 11.23 13.325
22 11.12 13.290 11.29 13.512 11.10 13.644 11.25 13.409
23 11.14 13.308 11.28 13.280 11.14 13.626 11.14 13.188
24 11.09 13.458 11.19 13.286 11.14 13.625 11.19 13.604
Continuous table 3
Battery size The 5th group The 6th group The 7th group The 8th group
The battery numbering Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage
1 10.85 13.439 11.14 13.644 11.46 13.587 11.41 13.390
2 10.88 13.194 11.07 13.605 11.41 13.501 11.30 13.390
3 11.02 13.472 10.98 13.487 11.41 13.508 11.09 13.399
4 10.78 13.362 10.97 13.474 11.44 13.639 11.38 13.383
5 11.01 13.476 11.07 13.480 11.41 13.470 11.35 13.358
6 10.97 13.316 11.09 13.459 11.42 13.468 11.35 13.354
7 10.97 13.489 11.12 13.443 11.43 13.488 11.31 13.351
8 10.95 13.313 11.00 13.301 11.40 13.464 11.40 13.402
9 10.98 13.250 11.00 13.645 11.38 13.575 11.32 13.352
10 10.92 13.448 11.02 13.463 11.41 13.462 11.33 13.415
11 11.08 13.446 10.91 13.508 11.44 13.492 11.31 13.398
12 10.85 13.354 10.97 13.579 11.37 13.459 11.41 13.375
13 10.96 13.287 10.93 13.409 11.44 13.484 11.35 13.361
14 10.95 13.294 10.96 13.371 11.44 13.459 11.40 13.392
15 11.08 13.579 10.94 13.517 11.42 13.740 11.28 13.351
16 11.04 13.318 10.97 13.319 11.44 13.466 11.42 13.393
17 10.97 13.382 10.97 13.398 11.44 13.675 11.40 13.373
18 10.89 13.396 11.11 13.298 11.42 13.483 11.40 13.386
19 11.43 13.518 11.39 13.398
20 11.43 13.615 11.39 13.410
21 11.36 13.463 11.37 13.377
22 11.43 13.510 11.34 13.358
23 11.42 13.528 11.34 13.369
24 11.43 13.449 11.33 13.403
Continuous table 3
Battery size The 9th group The tenth group The 11 group
The battery numbering Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage Capacity is judged voltage Float charge voltage
1 11.28 13.517 11.01 13.740 11.09 13.526
2 11.15 13.342 11.03 13.537 11.07 13.559
3 11.28 13.373 11.21 13.514 11.13 13.592
4 11.14 13.438 10.89 13.686 11.19 13.670
5 11.28 13.484 10.94 13.520 11.15 13.859
6 11.16 13.439 10.96 13.477 11.15 13.739
7 11.28 13.629 10.80 13.404 11.00 13.445
8 11.19 13.454 11.17 13.760 11.14 13.551
9 11.24 13.644 11.05 13.554 11.20 13.588
10 11.26 13.207 11.02 13.531 11.18 13.782
11 11.20 13.404 11.09 13.560 11.16 13.570
12 11.25 13.466 11.05 13.554 10.85 13.615
13 11.10 13.376 10.94 13.670 11.25 13.578
14 11.12 13.424 11.18 13.526 11.18 13.821
15 11.18 13.368 10.90 13.513 11.19 13.594
16 11.25 13.592 11.02 13.543 11.19 13.944
17 11.21 13.468 11.04 13.540 11.12 11.211
18 11.30 13.654 11.00 13.505 10.99 13.457
19 11.28 13.585 11.14 13.951 11.00 13.437
20 11.24 13.450 11.02 13.521 10.85 13.316
21 11.19 13.526 11.01 13.724 10.94 13.440
22 11.18 13.507 11.07 13.741 11.02 13.453
23 11.20 13.553 11.06 13.738 11.00 13.441
24 11.28 13.423 10.91 13.487 10.87 13.424
From the foregoing description as can be seen, formation method provided by the present invention can reach the charging requirement of the formation method of present employing, simultaneously, is the formation method that energy consumption and line duration all will be lower than present employing.Wherein, fill in the stage main, charging current is 0.15～0.20C/A, and discharging current is 0.15～0.20C/A, and its effect is the most outstanding, and energy consumption and line duration are minimum.
In first and third, four, five, six, seven, eight, nine, ten group, before main charging, that pole plate is static or with the current charges of 0～0.03C/A 0.5～2 hour.Like this, can make the electrolyte in the battery that can be arranged sufficient diffusion time, help the charging of battery.From second group and first group more as can be seen, under the suitable situation of charge and discharge process and electric current, first group of line duration than second group is short.
Fill the charging process in stage the 5th, six group of master, promptly in the 4th step, interrupt charging and static a period of time.Like this, make battery obtain unpolarizing, help improving the formation effect of battery.Compare from these two groups with the 9th, ten group, they have reduced energy consumption and line duration.
The 7th group the main stage of filling finish the back and static before, also battery is carried out the discharge that discharging current is 0.1C/A, be less than 1 hour discharge time, and carry out the charging that charging current is 0.1C/A again, the charging interval is less than 10 hours.Like this, make the battery unpolarizing more be tending towards obviously helping improving the formation effect of battery, compare with the 8th group and reduced energy consumption and line duration.
The charging of second stage in the above-described embodiments, major part is divided into first step charging and the charging of second step, and first step charging current is 0.05～0.1C/A, and the charging interval is 9～11 hours, the second step charging current is 0.02～0.04C/A, and the charging interval is 9～10 hours.Like this, mainly be can guarantee full charge after making battery capacity judge discharge, need not to replenish electricity after making battery dispatch from the factory just can use.

Claims (7)

1. forming method of lead-acid battery electrode plate transplantation, it is characterized in that its employing is internalized into, it comprises charging and the discharge that the main several times that fill the stage replace, main the last of stage that fill for charging, charging current is 0.13～0.27C/A, charging total time is 35～55 hours, discharging current is 0.13～0.27C/A, be 0.5～8 hour discharge time, finishes static 0～3 hour of back in the main stage of filling, and carries out capacity judgement discharge after static, after judging discharge, capacity carries out the second stage charging again, charging current is 0.02C～0.1C/A, and charging total time is 18～21 hours, and wherein C represents the rated capacity of storage battery.
2. a kind of forming method of lead-acid battery electrode plate transplantation as claimed in claim 1 is characterized in that it is 0.15～0.20C/A that the master fills the charging current in stage, and discharging current is 0.15～0.20C/A.
3. a kind of forming method of lead-acid battery electrode plate transplantation as claimed in claim 1 is characterized in that charging that the main stage of filling comprises that secondary or three charging currents are 0.13～0.27C/A and the discharging current that lacks once than this charging times are the discharge of 0.13～0.27C/A.
4. a kind of forming method of lead-acid battery electrode plate transplantation as claimed in claim 1 is before it is characterized in that charging for the first time in the main stage of filling, static or with the current charges of 0～0.03C/A 0.5～2 hour with pole plate.
5. a kind of forming method of lead-acid battery electrode plate transplantation as claimed in claim 1 is characterized in that interrupting charging and static a period of time in the charging process of leading the stage of filling.
6. a kind of forming method of lead-acid battery electrode plate transplantation as claimed in claim 1, it is characterized in that the main stage of filling finish the back and static before, also pole plate is carried out the discharge of discharging current less than 0.1C/A, be less than 1 hour discharge time, and carry out charging current again for less than the charging of 0.1C/A, the charging interval is less than 10 hours.
7. a kind of forming method of lead-acid battery electrode plate transplantation as claimed in claim 1, it is characterized in that the second stage charging is divided into first step charging and the charging of second step, first step charging current is 0.05～0.1C/A, charging interval is 9～11 hours, the second step charging current is 0.02～0.04C/A, and the charging interval is 9～10 hours.
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