CH88116A - Process for the preparation of a substantive o-oxyazo dye. - Google Patents

Process for the preparation of a substantive o-oxyazo dye.

Info

Publication number
CH88116A
CH88116A CH88116DA CH88116A CH 88116 A CH88116 A CH 88116A CH 88116D A CH88116D A CH 88116DA CH 88116 A CH88116 A CH 88116A
Authority
CH
Switzerland
Prior art keywords
dye
substantive
oxyazo
preparation
alkali
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH88116A publication Critical patent/CH88116A/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/24Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
    • C09B29/28Amino naphthols
    • C09B29/30Amino naphtholsulfonic acid
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B33/00Disazo and polyazo dyes of the types A->K<-B, A->B->K<-C, or the like, prepared by diazotising and coupling
    • C09B33/02Disazo dyes
    • C09B33/08Disazo dyes in which the coupling component is a hydroxy-amino compound
    • C09B33/10Disazo dyes in which the coupling component is a hydroxy-amino compound in which the coupling component is an amino naphthol
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B45/00Complex metal compounds of azo dyes
    • C09B45/02Preparation from dyes containing in o-position a hydroxy group and in o'-position hydroxy, alkoxy, carboxyl, amino or keto groups
    • C09B45/14Monoazo compounds
    • C09B45/18Monoazo compounds containing copper

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

      Verfahren    zur Herstellung eines     direktziehenden        o-Oiyazofarbstoffe,.       Es wurde gefunden, dass durch Kuppeln  von     diazotiertem        2-Amino-5-nitro-l-oxyben-          zol    mit     m-Aminobe,rizoyl-2:5-aminonaphtol-          i-sulfosäure    ein direktziehender     o-Oxyazo-          farbstoff    erhalten wird, welcher Baumwolle  in licht- und     alkaliempfin.dlichen    violetten  Tönen anfärbt.

   Durch Nachkupfern oder  noch besser durch Färben in der für direkt  ziehende Farbstoffe üblichen Weise unter  Zusatz von     Kupferverbindungen        zum    Bade  werden     hervorra@:end    licht- und     alkalieclite     graue Töne erhalten.

           Beispiel:       15,4 kg     2-Amino-5-nitro-1-oxybenzol    wer  den in die     Diazowerbindung        übergeführt    und  diese in eine Lösung von 37     kg        m-Amino-          benzoyl=?        :i)aniiiioriaphtol-7-sulfosäure        und     30 kg Soda     einfliessen        gelassen.        Nach    1          Stunden        wird    der Farbstoff     aasgesalzen,     filtriert, und getrocknet



      Process for the preparation of a substantive o-olyazo dye. It has been found that by coupling diazotized 2-amino-5-nitro-1-oxybenzene with m-aminobe, rizoyl-2: 5-aminonaphthol-1-sulfonic acid, a substantive o-oxyazo dye is obtained, which is cotton colors in light- and alkali-sensitive violet tones.

   By re-coppering or, even better, by dyeing in the manner customary for direct dyestuffs with the addition of copper compounds to the bath, excellent light and alkaline gray tones are obtained.

           Example: 15.4 kg of 2-amino-5-nitro-1-oxybenzene are converted into the diazo bond and this is converted into a solution of 37 kg of m-amino-benzoyl =? : i) aniiiioriaphtol-7-sulfonic acid and 30 kg of soda are allowed to flow in. After 1 hour, the dyestuff is washed with salt, filtered and dried

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines direkt- ziehenden o-Oxyazofa.rbstoffes, dadurch ge kennzeichnet, class diazotiertes 2-Amino-5- iiitro-l-oxybenzol mit ziii-Aminobenzoyl-2- : 5- Aminoiial,ht.ol-7-sulfosiiui-e kombiniert wird. PATENT CLAIM: Process for the production of a direct o-oxyazofa dye, characterized in that class diazotized 2-amino-5-nitro-1-oxybenzene with ziii-aminobenzoyl-2-: 5- aminoiial, ht.ol-7- sulfosiiui-e is combined. Der erhaltene Oxvazofarbstoff färbt. direkt Baumwolle in licht- und alkaliempfind- lichen violetten Tönen. Durch Nachkupfern oder besser durch Färben in der für direki- ziehende Farbstoffe üblichen Weise unter Zusatz von Kupferverbindungen zum Bade werden hervorragend iiclit- und alkaliechte ;raue Töne erhalten. The oxvazo dye obtained stains. directly cotton in light- and alkali-sensitive violet tones. By re-coppering or, better still, by dyeing in the manner customary for directing dyes with the addition of copper compounds to the bath, outstandingly white and alkali-fast, rough tones are obtained.
CH88116D 1915-12-30 1915-12-30 Process for the preparation of a substantive o-oxyazo dye. CH88116A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH88116T 1915-12-30
CH86850T 1919-05-01

Publications (1)

Publication Number Publication Date
CH88116A true CH88116A (en) 1921-02-16

Family

ID=25703636

Family Applications (1)

Application Number Title Priority Date Filing Date
CH88116D CH88116A (en) 1915-12-30 1915-12-30 Process for the preparation of a substantive o-oxyazo dye.

Country Status (1)

Country Link
CH (1) CH88116A (en)

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