CH493569A - Regeneration of alusial agent from vistose - Google Patents

Regeneration of alusial agent from vistose

Info

Publication number
CH493569A
CH493569A CH1059169A CH1059169A CH493569A CH 493569 A CH493569 A CH 493569A CH 1059169 A CH1059169 A CH 1059169A CH 1059169 A CH1059169 A CH 1059169A CH 493569 A CH493569 A CH 493569A
Authority
CH
Switzerland
Prior art keywords
filter medium
grain size
impurities
microns
regeneration
Prior art date
Application number
CH1059169A
Other languages
German (de)
Inventor
Hoegger Anton
Original Assignee
Mueller Hans
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from CH662163A external-priority patent/CH407950A/en
Priority claimed from CH696263A external-priority patent/CH415555A/en
Priority claimed from CH900463A external-priority patent/CH436241A/en
Priority claimed from CH950463A external-priority patent/CH467808A/en
Priority to CH1059169A priority Critical patent/CH493569A/en
Application filed by Mueller Hans filed Critical Mueller Hans
Priority to BE751298D priority patent/BE751298R/en
Priority to FR707023909A priority patent/FR2051611B2/fr
Priority to US51769A priority patent/US3674146A/en
Priority to DE19702033688 priority patent/DE2033688C3/en
Priority to JP45059403A priority patent/JPS4839767B1/ja
Priority to GB33498/70A priority patent/GB1292168A/en
Publication of CH493569A publication Critical patent/CH493569A/en

Links

Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F13/00Recovery of starting material, waste material or solvents during the manufacture of artificial filaments or the like
    • D01F13/02Recovery of starting material, waste material or solvents during the manufacture of artificial filaments or the like of cellulose, cellulose derivatives or proteins
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D41/00Regeneration of the filtering material or filter elements outside the filter for liquid or gaseous fluids
    • B01D41/02Regeneration of the filtering material or filter elements outside the filter for liquid or gaseous fluids of loose filtering material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26Synthetic macromolecular compounds
    • B01J20/261Synthetic macromolecular compounds obtained by reactions only involving carbon to carbon unsaturated bonds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004Sorbent size or size distribution, e.g. particle size
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/34Regenerating or reactivating
    • B01J20/3425Regenerating or reactivating of sorbents or filter aids comprising organic materials
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product
    • Y02P70/62Manufacturing or production processes characterised by the final manufactured product related technologies for production or treatment of textile or flexible materials or products thereof, including footwear

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

Regeneration of alluvial agent from viscose filtration. Contaminated, plastic-powder alluvial filter medium is freed from impurities by wet classification and subjected to flow classification to adjust its grain size. - Specifically, the filter medium is a mixture of polyvinyl chloride and suspension polymer whose fine particles have a grain size of 15-100 mu, its coarse particles a grain size of 80-200 mu.

Description

  

  Verfahren zur     Regeneration    von     Anschwemm-Mittel    aus der     Viskosefiltration     unter     Beeinflussung    des     Korngrösseverhältnisses       Die Erfindung betrifft ein Verfahren zur Regenera  tion des zur Filtration von Viskose gebrauchten An  schwemm-Mittels nach Hauptpatent Nr. 436 241. Nach  diesem Patent geschieht die Regeneration dadurch, dass  die Filterrückstände unter vollständiger Aufschlämmung  der     Anschwemm-Filtermittel    mit einer Flüssigkeit behan  delt und die Verunreinigungen von den     Anschwemm-          Filtermitteln    getrennt werden.

   Die Abtrennung geschieht  im wesentlichen durch     Nassklassierung.    Als Filterhilfs  mittel hat sich Kunststoffpulver, vorzugsweise     Polyvi-          nylchlorid    als     Suspensionspolymerisat    in Korngrössen  von 15 bis 200     Mikron,    bestens bewährt und es hat sich  gezeigt, dass ein Optimum in     Klärung    und     Filterstandzeit     erreichbar ist, wenn je nach der Qualität der Viskose und  der Art ihrer Verunreinigungen ein Gemisch aus Kunst  stoffpulver verschiedener Korngrösse angewandt wird,  wobei durch Änderung des Verhältnisses der Gemischan  teile eine optimale Anpassung an die jeweiligen Bedin  gungen möglich ist.  



  Für die Erfindung war die Aufgabe massgebend, die  Regeneration des     Anschwemm-Mittels    so zu leiten, dass  die zur Erreichung der optimalen Filterleistung günstigste  Mischung der     Korngrössenanteile    in dem regenerierten  Filtermittel je nach den Eigenschaften der zu filtrieren  den Viskose gewählt werden kann.  



  Das Verfahren nach der Erfindung löst die Aufgabe  dadurch, dass aus einem aus Kunststoffpulver bestehen  den, nach Gebrauch verunreinigten     Anschwemm-Filter-          mittel    zuerst die Verunreinigungen durch     Nassklassieren     entfernt werden, und dass das so gereinigte     Anschwemm-          Filtermittel    anschliessend einer     Strömungsklassierung,          zwecks    Einstellung seiner     Korngrössenverteilung    ausge  setzt wird.  



  Auf der     Zeichnung    ist ein     Hiess-Schema    der zur  Durchführung des Verfahrens beispielsweise anwendba  ren Anlage dargestellt. Von dem mit einer rotierenden  Siebtrommel ausgestatteten     Nassklassierer    1 wird das im  trichterförmigen Bodenteil dieses Apparates     gesammelte,     von groben Verunreinigungen befreite Filtermittel, ein  Gemisch aus     Polyvinylchlorid-Suspensionspolymerisat       der beiden     Korngrössenbereiche    15 bis 100     Mikron    und  80 bis     200        Mikron,

      zusammen mit dem zur     Nassklassie-          rung    verwendeten Wasser mittels einer     Exzenterschnek-          kenpumpe    2 abgesaugt und in den als     Strömungsklassie-          rer    arbeitenden Behälter 3 geleitet. In diesem Behälter  sammeln sich die     Filtermittelteilchen    im Bodenteil, wäh  rend die im     Vorreiniger    1 noch nicht entfernten feinen  Fasern und Schmutzpartikel durch einen Überlauf, zu  sammen mit dem beigemischten Waschwasser abgeleitet  werden.

   Eine Niveauregelung sorgt dafür, dass im Behäl  ter 3 das Filtermittel nur bis zu einer vorbestimmten  Höhe steigen und kein Verlust durch Überlauf eintreten  kann.  



  Aus dem Bodenteil des Behälters 3 wird durch eine       Exzenterschneckenpumpe    4 das aus Anteilen verschiede  ner Korngrösse bestehende Filtermittel zusammen mit  Wasser abgezogen und in den Behälter 5     tangential     eingeführt. Diese     Pumpe    4 ist mit einem drehzahlregu  lierbaren Antrieb versehen, so dass ihre Leistung und  damit die Strömungsgeschwindigkeit im Behälter 5 ver  ändert werden kann.

   Aus dem konischen Unterteil des  Behälters 5 wird durch eine     Dosierpumpe    7, eine     Exzen-          terschnecken-    oder     Membranpumpe    mit einstellbarer  Mengenleistung, der aus Filtermittel und Wasser beste  hende Schlamm abgezogen und in den Mischbehälter 8  gegeben, der die zu filtrierende Viskose enthält, die mit  einer Pumpe laufend der Filteranlage zugeleitet wird.  Aus dem Oberteil des Behälters 5 führt eine Leitung in  den Behälter 6, in welchem das für die     Voranschwem-          mung    der Filteranlage nötige Filtermittel gesammelt und  bis zur Neuanschwemmung bereitgehalten wird.

   Bei  starkem Zufluss in den Behälter 5 wirkt dieser nach Art  eines Hydrozyklon, die feinen Anteile werden nach oben  und zum Behälter 6 geführt, während sich die groben  Anteile des Filtermittels unten ansammeln, von wo sie  durch die     Dosierpumpe    7 abgezogen und der zu filtrie  renden Viskose im Mischbehälter 8     beigcgeben    werden.  Bei langsamem     Durchfluss,    bei langsamem Lauf der  Pumpe 4, ergibt sich im Behälter 5 nur geringe Strömung,  die keine     Klassierung    bewirkt, so dass das von der       Dosierpumpe    7 abgezogene Filtermittel etwa dieselbe           Korngrössenverteilung    aufweist wie im Behälter 3.

   Durch  Veränderung der Drehzahl der Pumpe 4 bietet sich so die  Möglichkeit, das Verhältnis der feinen und groben Antei  le des Filterhilfsmittels zu beeinflussen, wodurch die  Filterleistung bei verschiedenen     Viskosequalitäten    jeweils  zu einem optimalen Wert gebracht werden kann.



  Process for the regeneration of precoat from viscose filtration by influencing the grain size ratio The invention relates to a process for the regeneration of the precoat used for the filtration of viscose according to main patent no. 436 241. According to this patent, the regeneration is done by removing the filter residue treated with complete suspension of the precoat filter media with a liquid and the impurities are separated from the precoat filter media.

   The separation takes place essentially by wet classification. As a filter aid, plastic powder, preferably polyvinyl chloride as a suspension polymer in particle sizes of 15 to 200 microns, has proven to be very effective and it has been shown that an optimum in clarification and filter service life can be achieved if, depending on the quality of the viscose and the type of it Impurities a mixture of plastic powder of different grain sizes is used, whereby an optimal adaptation to the respective condi tions is possible by changing the ratio of the mixture.



  The main task of the invention was to direct the regeneration of the precoat in such a way that the most favorable mixture of the grain size fractions in the regenerated filter medium to achieve the optimum filter performance can be selected depending on the properties of the viscose to be filtered.



  The method according to the invention solves the problem in that the precoat filter medium made of plastic powder, contaminated after use, is first removed by wet classification, and that the precoated filter medium cleaned in this way is then flow classification for the purpose of adjusting its grain size distribution is suspended.



  The drawing shows a Hiess diagram of the system, for example applicable for carrying out the method. From the wet classifier 1, which is equipped with a rotating sieve drum, the filter medium, which has been freed from coarse impurities and collected in the funnel-shaped bottom part of this apparatus, is a mixture of polyvinyl chloride suspension polymer of the two grain size ranges 15 to 100 microns and 80 to 200 microns,

      Sucked off together with the water used for wet classification by means of an eccentric screw pump 2 and fed into the container 3, which works as a flow classifier. In this container, the filter medium particles collect in the bottom part, while the fine fibers and dirt particles not yet removed in the pre-cleaner 1 are diverted through an overflow, together with the added wash water.

   A level control ensures that the filter medium in the container 3 only rises up to a predetermined height and that no loss can occur through overflow.



  From the bottom part of the container 3, the filter medium consisting of fractions of various ner grain size is withdrawn together with water by an eccentric screw pump 4 and introduced into the container 5 tangentially. This pump 4 is provided with a speed regulatable drive so that its performance and thus the flow rate in the container 5 can be changed ver.

   From the conical lower part of the container 5, a metering pump 7, an eccentric screw or diaphragm pump with adjustable volume capacity, the existing sludge drawn from filter medium and water and given into the mixing container 8, which contains the viscose to be filtered, which with a Pump is continuously fed to the filter system. A line leads from the upper part of the container 5 into the container 6, in which the filter medium necessary for the pre-alluviation of the filter system is collected and held ready until the new alluvial surface is deposited.

   When there is a strong inflow into the container 5, this acts like a hydrocyclone, the fine fractions are led upwards and to the container 6, while the coarse fractions of the filter medium collect at the bottom, from where they are drawn off by the metering pump 7 and the viscose to be filtered be added in the mixing container 8. With slow flow, with slow running of the pump 4, there is only a small flow in the container 5, which does not cause any classification, so that the filter medium withdrawn from the metering pump 7 has approximately the same grain size distribution as in the container 3.

   By changing the speed of the pump 4, it is possible to influence the ratio of the fine and coarse fractions of the filter aid, whereby the filter performance can be brought to an optimal value for different viscose qualities.

 

Claims (1)

PATENTANSPRUCH Verfahren nach dem Patentanspruch des Hauptpaten tes, dadurch gekennzeichnet, dass aus einem aus Kunst stoffpulver bestehenden, nach Gebrauch verunreinigten Anschwemm-Filtermittel zuerst die Verunreinigungen durch Nassklassieren entfernt werden, und dass das so gereinigte Anschwemm-Filtermittel anschliessend einer Strömungsklassierung, zwecks Einstellung seiner Korn grössenverteilung, ausgesetzt wird. UNTERANSPRÜCHE 1. PATENT CLAIM Process according to the patent claim of the main patent, characterized in that the impurities are first removed from a pre-coat filter medium made of plastic powder and contaminated after use, and the pre-coat filter medium cleaned in this way is then subjected to flow classification in order to adjust its grain size distribution, is exposed. SUBCLAIMS 1. Verfahren nach Patentanspruch, dadurch gekenn zeichnet, dass das durch Nassklassierung von Fasern und anderen Verunreinigungen getrennte Filtermittel zusam men mit Flüssigkeit durch eine leistungsregelbare Exzen- terschneckenpumpe in einen Behälter tangential eingelei tet wird, aus dessen Unterteil das zur laufenden Zumi- schung in die zu filtrierende Viskose bestimmte Filter hilfsmittel, aus dessen Oberteil jedoch das zur Voran schwemmung vorgesehene Filtermittel ausgeleitet wird. Method according to patent claim, characterized in that the filter medium separated by wet classification of fibers and other impurities is introduced tangentially into a container together with liquid by a power-adjustable eccentric screw pump, from the lower part of which the ongoing admixture into the one to be filtered Viscous certain filter aid, from the upper part of which, however, the filter medium intended for Voran flooding is diverted. 2. Verfahren nach Patentanspruch, dadurch gekenn zeichnet, dass das als Anschwenun-Filtermittel verwende te Kunststoffpulver aus einem Gemisch von Polyvinyl- chlorid-Suspensionspolymerisat besteht, bei welchem der feine Anteil einen Korngrössenbereich von 15 bis<B>100</B> Mikron, der grobe Anteil einen Bereich von<B>80</B> bis 200 Mikron aufweist. 2. The method according to claim, characterized in that the plastic powder used as a swelling filter medium consists of a mixture of polyvinyl chloride suspension polymer, in which the fine fraction has a grain size range of 15 to 100 microns, the coarse portion has a range from 80 to 200 microns. Anmerkung <I>des</I> Eidg. <I>Amtes für geistiges Eigentum:</I> Sollten Teile der Beschreibung mit der im Patentan spruch gegebenen Definition der Erfindung nicht in Einklang stehen, so sei daran erinnert, dass gemäss Art.<B>51</B> des Patentgesetzes der Patentanspruch für den sachlichen Geltungsbereich des Patentes massgebend ist. Comment from <I> of the </I> Swiss Federal Office of Intellectual Property: </I> Should parts of the description not be consistent with the definition of the invention given in the patent claim, it should be remembered that according to Art. <B> 51 </B> of the Patent Act, the claim is decisive for the material scope of the patent.
CH1059169A 1963-05-28 1969-07-09 Regeneration of alusial agent from vistose CH493569A (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
CH1059169A CH493569A (en) 1963-05-28 1969-07-09 Regeneration of alusial agent from vistose
BE751298D BE751298R (en) 1969-07-09 1970-06-02 PROCESS FOR FILTRATION OF SYNTHETIC SHEET AND ARTIFICIAL SILK SPINNING MASSES BY FILTERING SURFACES CHARGED WITH AN AGENT
FR707023909A FR2051611B2 (en) 1969-07-09 1970-06-26
US51769A US3674146A (en) 1969-07-09 1970-07-02 Method of regenerating filter aids
JP45059403A JPS4839767B1 (en) 1969-07-09 1970-07-07
DE19702033688 DE2033688C3 (en) 1969-07-09 1970-07-07 Process for the filtration of viscose spinning masses
GB33498/70A GB1292168A (en) 1969-07-09 1970-07-09 Process for the filtration of viscose solutions

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
CH662163A CH407950A (en) 1963-05-28 1963-05-28 Process for the filtration of liquids that are difficult to filter
CH696263A CH415555A (en) 1963-06-05 1963-06-05 Process for the filtration of liquids with the help of easily regenerable filter aids
CH900463A CH436241A (en) 1963-07-17 1963-07-17 Process for the regeneration of precoat agents from viscose filtration
CH950463A CH467808A (en) 1963-05-28 1963-07-30 Process for the regeneration of precoat from viscose filtration
CH1429163A CH466852A (en) 1963-05-28 1963-11-20 Process for the regeneration of precoat filter media from viscose filtration
CH1059169A CH493569A (en) 1963-05-28 1969-07-09 Regeneration of alusial agent from vistose

Publications (1)

Publication Number Publication Date
CH493569A true CH493569A (en) 1970-07-15

Family

ID=27543786

Family Applications (1)

Application Number Title Priority Date Filing Date
CH1059169A CH493569A (en) 1963-05-28 1969-07-09 Regeneration of alusial agent from vistose

Country Status (1)

Country Link
CH (1) CH493569A (en)

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