CH248346A - Disinfection method. - Google Patents

Disinfection method.

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Publication number
CH248346A
CH248346A CH248346DA CH248346A CH 248346 A CH248346 A CH 248346A CH 248346D A CH248346D A CH 248346DA CH 248346 A CH248346 A CH 248346A
Authority
CH
Switzerland
Prior art keywords
ethyl
phenoxy
dimethyl
dodecyl
ammonium bromide
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellschaft Ciba
Original Assignee
Ciba Geigy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Geigy filed Critical Ciba Geigy
Publication of CH248346A publication Critical patent/CH248346A/en

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Description

  

      Verfahren    zur     Desinfektion.       Es ist bekannt, dass     Aryloxyalkyl-ammo-          niumverbindungen,    die sich von zweiwertigen       Phenolen    ableiten, desinfizierend wirken.  



  Es wurde nun gefunden, dass auch     Phen-          oxv-äthy1-dimethyl    -     ammoniumver        bindungen     der Reihe der einwertigen     Phenole,    die am       quaternären    Stickstoffatom ausserdem einen  Kohlenwasserstoffrest mit     mindestens    8     Koh-          lenstoffatomen    enthalten, gut desinfizierend       wirken    und infolgedessen zur     Desinfektion     Verwendung finden können, gegebenenfalls  im Gemisch mit andern Stoffen. Der     Phenyl-          kern    kann z.

   B. auch Halogenatome oder       Alkylreste    tragen. Erwähnt seien beispiels  weise folgende Verbindungen:     (ss-Phenoxy-          äthyl)        -dimethyl-        dodecyl-ammoniumbromid,          Phenoxy    -     äthyl)        -dimethyl    -     dodecyl-ammo-          niumchlorid,        (ss-Phenoxy-äthyl)    -     dimethyl-          dodeeyl-p-toluolsulfonat,        (ss-Phenoxy-äthyl)

  -          dimethy    1-     octyl    -     ammoniumbromid,        (ss    -     Phen-          oxy-äthyl)        -dimethyl    -     äthylhexyl    -     ammonium-          bromid,        (ss-Phenoxy-äthyl)-dimethyl-hexa-          decyl-ammoniizmbromid,        [ss-(p-Chlor-phen-          oxy)

      -     äthyl    ] -     dimethyl    -     dodecyl    -     ainmonium-          bromid,        [ss-    (p -     Methyl    -     phenoxy)    -     äthyl]-        di-          methyl-dodecyl-ammoniumbromid,        [ss-(o-Me-          thyl        -phenoxy)        -äthyll    -     dimethyl-dodecyl-am-          moniumbromid,        [ss-(p-Hexyl-phenoxy)

  -äthyl]        -          dimethyl-dodecyl-ammoniumbromid,        [ss-(p-          tert.        Butyl-phenoxy)        -äthyll-dimethyl-dode-          cyl-ammoniumbromid,        [ss-(p-Isooctyl-phen-          oxy)    -     äthyl]    -     dümethyl    -     dodecyl    -     ammonium-          bromid    und     rss-(p-tert.    Octyl-phenoxy)

  -äthyll-         dimethyl-dodecyl-ammoniumbromid.    Die ge  nannten Verbindungen sind in Wasser leicht  löslich und zum Teil gut kristallisiert.  



  Das erfindungsgemässe Verfahren     zur     Desinfektion lässt sich auf den verschieden  sten Gebieten verwenden. So ist es geeignet  für die Desinfektion von Instrumenten, Ver  bandstoffen,     Wäsche    oder dergleichen.  



  Die angeführten     Phenoxy-äthyl-dimethyl-          ammoniumverbindungen    können in Form von  Lösungen oder Emulsionen gemischt mit an  dern desinfizierend wirkenden oder     inerten     Stoffen oder auch in Form von Trocken  pulvern zur Anwendung kommen.  



  Die     Phenoxy-äthyl-dimethyl-ammonium-          verbindungen    der genannten Art sind neu. Sie  lassen sich z. B. durch Behandlung der ent  sprechenden     Phenoxy    -     äthyl    -     dimethyl    -     amine     mit den     geeigneten        quaternisierenden    Mitteln  darstellen. Die     Phenoxy-äthyl-dimethyl-amine     ihrerseits sind bekannt oder können z. B. nach  üblichen Methoden hergestellt werden.

      <I>Beispiel:</I>  Ärztliche     Instrumente    werden in eine       1 /ooige    wässerige Lösung von     (ss-Phenoxy-          äthyl)    -     dimethyl    -     dodecyl    -     ammoniumbromid     (erhalten z. B. durch Erwärmen von     (ss-P'hen-          oxy-äthyl)-dimethylaminmitDodecyl-bromid)     unter Zusatz von etwas .Soda oder Natrium  nitrit     gelegt.    Nach ca. 10 Minuten sind die       Instrumente    keimfrei.



      Disinfection method. It is known that aryloxyalkylammonium compounds which are derived from dihydric phenols have a disinfecting effect.



  It has now been found that phenoxy-ethy1-dimethylammonium compounds of the series of monohydric phenols, which also contain a hydrocarbon radical with at least 8 carbon atoms on the quaternary nitrogen atom, have a good disinfecting effect and can therefore be used for disinfection, if appropriate mixed with other substances. The phenyl nucleus can, for.

   B. also carry halogen atoms or alkyl radicals. The following compounds may be mentioned, for example: (ss-phenoxy-ethyl) -dimethyl-dodecyl-ammonium bromide, phenoxy-ethyl) -dimethyl-dodecyl-ammonium chloride, (s-phenoxy-ethyl) - dimethyl-dodeeyl-p-toluenesulfonate, (ss-phenoxy-ethyl)

  - dimethy 1- octyl - ammonium bromide, (ss - phenoxy-ethyl) -dimethyl - ethylhexyl - ammonium bromide, (ss-phenoxy-ethyl) -dimethyl-hexadecyl-ammonium bromide, [ss- (p-chloro- phenoxy)

      - ethyl] - dimethyl - dodecyl - ammonium bromide, [ss- (p - methyl - phenoxy) - ethyl] - dimethyl dodecyl ammonium bromide, [ss- (o-methyl phenoxy) ethyl - dimethyl -dodecyl-ammonium bromide, [ss- (p-hexyl-phenoxy)

  -ethyl] - dimethyl-dodecyl-ammonium bromide, [ss- (p-tert. butyl-phenoxy) -ethyl-dimethyl-dodecyl-ammonium bromide, [ss- (p-isooctyl-phenoxy) - ethyl] - dimethyl - dodecyl - ammonium bromide and rss- (p-tert. octyl-phenoxy)

  -äthyll- dimethyl-dodecyl-ammonium bromide. The compounds mentioned are easily soluble in water and some of them are well crystallized.



  The inventive method for disinfection can be used in a wide variety of fields. So it is suitable for the disinfection of instruments, band fabrics, linen or the like.



  The listed phenoxy-ethyl-dimethylammonium compounds can be used in the form of solutions or emulsions mixed with other disinfecting or inert substances or in the form of dry powders.



  The phenoxy-ethyl-dimethyl-ammonium compounds of the type mentioned are new. You can z. B. by treating the corresponding phenoxy - ethyl - dimethyl - amine with the appropriate quaternizing agents. The phenoxy-ethyl-dimethyl-amines in turn are known or can be, for. B. be prepared by conventional methods.

      <I> Example: </I> Medical instruments are immersed in a 1 / o aqueous solution of (ss-phenoxy-ethyl) - dimethyl - dodecyl - ammonium bromide (obtained e.g. by heating (ss-p'henoxy -äthyl) -dimethylamine with dodecyl bromide) with the addition of some soda or sodium nitrite. The instruments are sterile after approx. 10 minutes.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Desinfektion, dadurch ge kennzeichnet, dass man Phenoxy-äthyl-di- methyl-ammoniumverbindungen der Reihe der einwertigen Phenole, die am quaternären Stickstoffatom ausserdem einen Kohlenwas serstoffrest mit mindestens 8 Kohlen,stoff- atomen enthalten, verwendet. UNTERANSPRüCHE 1. PATENT CLAIM: Process for disinfection, characterized in that phenoxy-ethyl-dimethyl-ammonium compounds from the series of monohydric phenols, which also contain a hydrocarbon residue with at least 8 carbon atoms on the quaternary nitrogen atom, are used. SUBCLAIMS 1. Verfahren zur Desinfektion nach Pa tentanspruch, dadurch gekennzeichnet, dass man Phenoxy-äthyl-dimethyl-ammoniumver- bindungen der Reihe der einwertigen Phenole, die am quaternären Stickstoffatom ausserdem einen Kohlenwasserstoffrest mit mindestens 8 Kohlenstoffatomen enthalten, im Gemisch mit andern Stoffen verwendet. 2. Process for disinfection according to patent claim, characterized in that phenoxy-ethyl-dimethyl-ammonium compounds of the series of monohydric phenols, which also contain a hydrocarbon residue with at least 8 carbon atoms on the quaternary nitrogen atom, are used in a mixture with other substances. 2. Verfahren zur Desinfektion nach Pa tentanspruch und Unteranspruch 1, dadurch gekennzeichnet, dass man (ss-Phenoxy-äthyl)- dimethyl - dodecyl - ammoniumhalogenide ver wendet. 3. Verfahren zur Desinfektion nach Pa tentanspruch und den Unteransprüchen 1 und 2, dadurch gekennzeichnet, dass man (ss-Phenogy-äthyl) -dimethyl -dodecyl-amnmo- niumbromid verwendet. Method for disinfection according to patent claim and dependent claim 1, characterized in that (s-phenoxy-ethyl) - dimethyl - dodecyl - ammonium halides are used. 3. A method for disinfection according to Pa tentan claim and the dependent claims 1 and 2, characterized in that (ss-phenogy-ethyl) -dimethyl-dodecyl-ammonium bromide is used.
CH248346D 1944-11-24 1944-11-24 Disinfection method. CH248346A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH248346T 1944-11-24

Publications (1)

Publication Number Publication Date
CH248346A true CH248346A (en) 1947-04-30

Family

ID=4466848

Family Applications (1)

Application Number Title Priority Date Filing Date
CH248346D CH248346A (en) 1944-11-24 1944-11-24 Disinfection method.

Country Status (1)

Country Link
CH (1) CH248346A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2786797A (en) * 1954-05-18 1957-03-26 Hollingshead Corp Corrosion-inhibited quaternary ammonium compositions
US3260643A (en) * 1962-04-18 1966-07-12 Ciba Ltd Combating plant diseases with phenoxy-ethyl-dimethyl-dodecyl-ammonium halides

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2786797A (en) * 1954-05-18 1957-03-26 Hollingshead Corp Corrosion-inhibited quaternary ammonium compositions
US3260643A (en) * 1962-04-18 1966-07-12 Ciba Ltd Combating plant diseases with phenoxy-ethyl-dimethyl-dodecyl-ammonium halides

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