CH209544A - Process for the preparation of a new derivative of an azo dye. - Google Patents

Process for the preparation of a new derivative of an azo dye.

Info

Publication number
CH209544A
CH209544A CH209544DA CH209544A CH 209544 A CH209544 A CH 209544A CH 209544D A CH209544D A CH 209544DA CH 209544 A CH209544 A CH 209544A
Authority
CH
Switzerland
Prior art keywords
dye
preparation
aminobenzene
new derivative
azo dye
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH209544A publication Critical patent/CH209544A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B43/00—Preparation of azo dyes from other azo compounds
    • C09B43/12—Preparation of azo dyes from other azo compounds by acylation of amino groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

      Zusatzpatent    zum Hauptpatent Nr. 205164.    Verfahren zur Herstellung eines neuen Derivates eines     Azofarbstoffes.       Es wurde gefunden, dass man ein neues  Derivat eines     Azofarbstoffes    erhält, wenn man  1     Mol    des     Trisazofarbstoffes,    der erhalten  wird durch Vereinigen eines Moleküls der       1.3-Diaminobenzol-4-sulfonsäure    mit 1     Mol     des dianotierten     Disazofarbstoffes    aus diano  tierter     2-Aminonaphthalin-6.8-disulfonsäui e     und     1-Methyl-4-metboxy-3-aminobenzol,

          Wei-          terdiazotieren    und Vereinigen mit einem Mole  kül     1.4-Diinethyl-3-aminobenzol,    mit 2     Mol          Benzoylchlorid    in Gegenwart einer tertiären  Base     acyliert.     



  Der neue     Farbstoff    stellt ein dunkelbraunes  Pulver dar und färbt Baumwolle in echten  rotbraunen Tönen.  



       Beispiel:     1 Teil des     Trisazofarbstoffes,    der erhalten  wird durch Vereinigen der     1.3-Diaminobenzol-          4-sulfonsäure    mit dem dianotierten     Disazo-          farbstoff    aus dianotierter     2-Arninonaphthalin-          6.8-disulfonsäure    und     1-Methyl-4-methoxy-3-          aminobenzol,        Weiterdiazotieren    und Vereinigen       finit        1.4-Dimethyl-3-aminobenzol,    wird in 3,2  Teilen     Pyridin    suspendiert und bei 40' mit    1,

  2 Teilen     Benzoylchlorid    versetzt. Man er  wärmt allmählich auf<B>900</B> und hält diese  Temperatur 1 Stunde. Nach dieser Zeit wird  das     Dibenzoylprodukt    abgeschieden und ge  trocknet.



      Additional patent to main patent no. 205164. Process for the production of a new derivative of an azo dye. It has been found that a new derivative of an azo dye is obtained if 1 mole of the trisazo dye, which is obtained by combining a molecule of 1,3-diaminobenzene-4-sulfonic acid with 1 mole of the dianotated disazo dye from diano tated 2-aminonaphthalene-6.8- disulfonic acid and 1-methyl-4-metboxy-3-aminobenzene,

          Further diazotize and combine with one mole of 1,4-diynethyl-3-aminobenzene, acylated with 2 moles of benzoyl chloride in the presence of a tertiary base.



  The new dye is a dark brown powder and dyes cotton in real red-brown tones.



       Example: 1 part of the trisazo dye which is obtained by combining the 1,3-diaminobenzene-4-sulfonic acid with the dianotized disazo dye from dianotated 2-aminonaphthalene-6.8-disulfonic acid and 1-methyl-4-methoxy-3-aminobenzene, further diazotizing and Combine finite 1,4-dimethyl-3-aminobenzene, is suspended in 3.2 parts of pyridine and at 40 'with 1,

  2 parts of benzoyl chloride were added. It is gradually heated to <B> 900 </B> and held at this temperature for 1 hour. After this time, the dibenzoyl product is deposited and dried ge.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Derivates eines Azofarbatoffes, dadurch ge kennzeichnet, dass man 1 Mol des Trisazo- farbstoffes, der erhalten wird durch Vereinigen eines Moleküls der 1.3-Diaminobenzol-4-sul- fonsäure mit 1 ATol des dianotierten Disazo- farbstoffes aus diazotierter2-Amiiionaphtbalin- 6.8-disulfonsäure und 1=Methyl-4-methoxy-3- aminobenzol, Claim: A process for the preparation of a new derivative of an azo carbate, characterized in that 1 mol of the trisazo dye, which is obtained by combining a molecule of 1,3-diaminobenzene-4-sulphonic acid with 1 mol of the dianotated disazo dye, is obtained diazotized 2-Amiiionaphtbalin- 6.8-disulfonic acid and 1 = methyl-4-methoxy-3-aminobenzene, Weiterdiazotieren und Vereini gen mit einem Molekül 1.4-Dimethyl-3-amino- benzol, mit 2 Mol Benzoylchlorid in Gegen wart einer tertiären Base acyliert. Der neue Farbstoff stellt ein dunkelbraunes Pulver dar und färbt Baumwolle in echten rotbraunen Tönen. Further diazotizing and combining with a molecule of 1,4-dimethyl-3-aminobenzene, acylated with 2 moles of benzoyl chloride in the presence of a tertiary base. The new dye is a dark brown powder and dyes cotton in real red-brown tones.
CH209544D 1937-01-26 1937-01-26 Process for the preparation of a new derivative of an azo dye. CH209544A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH209544T 1937-01-26
CH205164T 1939-02-01

Publications (1)

Publication Number Publication Date
CH209544A true CH209544A (en) 1940-04-15

Family

ID=25724131

Family Applications (1)

Application Number Title Priority Date Filing Date
CH209544D CH209544A (en) 1937-01-26 1937-01-26 Process for the preparation of a new derivative of an azo dye.

Country Status (1)

Country Link
CH (1) CH209544A (en)

Similar Documents

Publication Publication Date Title
CH209544A (en) Process for the preparation of a new derivative of an azo dye.
CH209542A (en) Process for the preparation of a new derivative of an azo dye.
CH209543A (en) Process for the preparation of a new derivative of an azo dye.
CH209545A (en) Process for the preparation of a new derivative of an azo dye.
CH209556A (en) Process for the preparation of a new derivative of an azo dye.
CH209540A (en) Process for the preparation of a new derivative of an azo dye.
CH209541A (en) Process for the preparation of a new derivative of an azo dye.
CH209538A (en) Process for the preparation of a new derivative of an azo dye.
CH209533A (en) Process for the preparation of a new derivative of an azo dye.
CH209534A (en) Process for the preparation of a new derivative of an azo dye.
CH209539A (en) Process for the preparation of a new derivative of an azo dye.
CH209537A (en) Process for the preparation of a new derivative of an azo dye.
CH209548A (en) Process for the preparation of a new derivative of an azo dye.
CH209551A (en) Process for the preparation of a new derivative of an azo dye.
CH209546A (en) Process for the preparation of a new derivative of an azo dye.
CH209555A (en) Process for the preparation of a new derivative of an azo dye.
CH209805A (en) Process for the preparation of a new derivative of an azo dye.
CH209536A (en) Process for the preparation of a new derivative of an azo dye.
CH209547A (en) Process for the preparation of a new derivative of an azo dye.
CH209550A (en) Process for the preparation of a new derivative of an azo dye.
CH209549A (en) Process for the preparation of a new derivative of an azo dye.
CH209535A (en) Process for the preparation of a new derivative of an azo dye.
CH213566A (en) Process for the preparation of a new derivative of an azo dye.
CH209552A (en) Process for the preparation of a new derivative of an azo dye.
CH209553A (en) Process for the preparation of a new derivative of an azo dye.