CH107776A - Process for the preparation of a unilaterally acylated derivative of ethylene diamine. - Google Patents

Process for the preparation of a unilaterally acylated derivative of ethylene diamine.

Info

Publication number
CH107776A
CH107776A CH107776DA CH107776A CH 107776 A CH107776 A CH 107776A CH 107776D A CH107776D A CH 107776DA CH 107776 A CH107776 A CH 107776A
Authority
CH
Switzerland
Prior art keywords
preparation
unilaterally
acylated derivative
ethylene diamine
salts
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH107776A publication Critical patent/CH107776A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Description

  

      1'erfaliren    zur Darstellung eines einseitig     acylierten    Derivates des     ithylendiamins.       Es     wurda    gefunden, dass man zu einem  einseitig     acylierten    Derivat des Äthylen  diamins gelangen kann, indem man     asym.          Diäthyläthylendiamin    mit einer das Radikal  der     Leinölsäure    enthaltenden Verbindung,  wie zum Beispiel     Leinölsäure,        Leinölsäure-          halogeniden        bezw.        -estern,

      oder     Leinölsäure-          anhydrid,    in üblicher Weise behandelt.  



  Das     Linoleyl-diäthyläthylendiamid    stellt  ein dickes, nicht destillierbares Öl dar, das  in     \krasser    nicht, in organischen Lösungs  mitteln löslich ist. Es bildet mit Säuren       wasseilösliche    Salze. Die neue     Verbindun,     soll     entweder    als solche oder in Form ihrer  Salze zu technischen und therapeutischen  Zwecken Verwendung finden.    <I>Beispiel:</I>    252 Teile     Leinölsäure    werden mit 116  Teilen     asym.        Diäthyläthylendiamin    sechs  Stunden im     Autoklaven    oder offen auf    180 bis 200   erhitzt.

   Das Reaktionsprodukt  wird bei 100   im Vakuum von gebildetem  Wasser befreit.



      1'erfaliren for the preparation of a unilaterally acylated derivative of ethylenediamine. It was found that a unilaterally acylated derivative of ethylene diamine can be obtained by reacting asym. Diethylethylenediamine with a compound containing the radical of linoleic acid, such as linoleic acid, linoleic acid halides or. -star,

      or linoleic anhydride, treated in the usual way.



  Linoleyl diethyl ethylenediamide is a thick, non-distillable oil that is not soluble in organic solvents. It forms water-soluble salts with acids. The new compound is to be used either as such or in the form of its salts for technical and therapeutic purposes. <I> Example: </I> 252 parts of linoleic acid and 116 parts of asym.

   The reaction product is freed from water formed at 100 in vacuo.

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung eines einseitig acylierten Derivates des Athylendiamins, dadurch gekennzeichnet, dass man asym. Di- äthyläthylendiamin mit einer das Radikal der Leinölsäure enthaltenden Verbindung in üblicher Weis_2 behandelt. Das Linoleyl-diäthyläthylendiamid stellt ein dickes, nicht destillierbares Öl dar, das in Wasser nicht, in organischen Lösungs mitteln löslich ist. Es bildet mit Säuren wasserlösliche Salze. Claim: Process for the preparation of a one-sided acylated derivative of ethylenediamine, characterized in that asym. Diethylethylenediamine is treated with a compound containing the radical of linoleic acid in the usual manner. Linoleyl diethylethylenediamide is a thick, non-distillable oil that is not soluble in water or in organic solvents. It forms water-soluble salts with acids. Die neue Verbindung soll entweder als solche oder in Form ihrer Salze zu technischen und therapeutischen Zwecken Verwendung finden. The new compound is intended to be used either as such or in the form of its salts for technical and therapeutic purposes.
CH107776D 1923-07-17 1923-07-17 Process for the preparation of a unilaterally acylated derivative of ethylene diamine. CH107776A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH107776T 1923-07-17
CH107202T 1923-07-17

Publications (1)

Publication Number Publication Date
CH107776A true CH107776A (en) 1924-11-17

Family

ID=25707127

Family Applications (1)

Application Number Title Priority Date Filing Date
CH107776D CH107776A (en) 1923-07-17 1923-07-17 Process for the preparation of a unilaterally acylated derivative of ethylene diamine.

Country Status (1)

Country Link
CH (1) CH107776A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1098001B (en) * 1957-09-12 1961-01-26 Knoll Ag Process for the preparation of N- (Diaethylaminoalkyl) -salicylamiden
WO1993000326A1 (en) * 1991-06-25 1993-01-07 Basf Aktiengesellschaft Omega-3 polyunsaturated fatty-acid derivatives, their preparation and their use

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1098001B (en) * 1957-09-12 1961-01-26 Knoll Ag Process for the preparation of N- (Diaethylaminoalkyl) -salicylamiden
WO1993000326A1 (en) * 1991-06-25 1993-01-07 Basf Aktiengesellschaft Omega-3 polyunsaturated fatty-acid derivatives, their preparation and their use

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