CA952424A - Separation by crystallization in presence of water - Google Patents

Separation by crystallization in presence of water

Info

Publication number
CA952424A
CA952424A CA127,827A CA127827A CA952424A CA 952424 A CA952424 A CA 952424A CA 127827 A CA127827 A CA 127827A CA 952424 A CA952424 A CA 952424A
Authority
CA
Canada
Prior art keywords
crystallization
separation
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA127,827A
Other versions
CA127827S (en
Inventor
Roberto Lee
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Monsanto Co
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Application granted granted Critical
Publication of CA952424A publication Critical patent/CA952424A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/16Separation; Purification; Stabilisation; Use of additives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0009Crystallisation cooling by heat exchange by direct heat exchange with added cooling fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/005Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/07Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms
    • C07C205/11Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms having nitro groups bound to carbon atoms of six-membered aromatic rings
    • C07C205/12Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms having nitro groups bound to carbon atoms of six-membered aromatic rings the six-membered aromatic ring or a condensed ring system containing that ring being substituted by halogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00Purification; Separation; Use of additives
    • C07C7/14Purification; Separation; Use of additives by crystallisation; Purification or separation of the crystals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CA127,827A 1970-11-17 1971-11-16 Separation by crystallization in presence of water Expired CA952424A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US9047670A 1970-11-17 1970-11-17

Publications (1)

Publication Number Publication Date
CA952424A true CA952424A (en) 1974-08-06

Family

ID=22222934

Family Applications (1)

Application Number Title Priority Date Filing Date
CA127,827A Expired CA952424A (en) 1970-11-17 1971-11-16 Separation by crystallization in presence of water

Country Status (5)

Country Link
BE (1) BE775337A (en)
CA (1) CA952424A (en)
DE (1) DE2156880A1 (en)
FR (1) FR2114772A5 (en)
GB (1) GB1319870A (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TR23271A (en) * 1987-02-06 1989-08-09 Krupp Koppers Gmbh PROCEDURE FOR THE GAIN OF P-KSILOL AT THE MINIMUM OF 95.5% PURITY
DE58902934D1 (en) * 1988-05-05 1993-01-21 Krupp Koppers Gmbh METHOD FOR OBTAINING P-XYLOL WITH A PURITY OF AT LEAST 99.5%.
CN113845506B (en) 2021-10-18 2022-09-23 惠州市宙邦化工有限公司 Dynamic crystallization purification method of ethylene carbonate

Also Published As

Publication number Publication date
DE2156880A1 (en) 1972-05-25
FR2114772A5 (en) 1972-06-30
GB1319870A (en) 1973-06-13
BE775337A (en) 1972-05-16

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