CA3012028A1 - Procede et appareil de traitement d'un residu de lixiviation d'un concentre de metal contenant du soufre - Google Patents
Procede et appareil de traitement d'un residu de lixiviation d'un concentre de metal contenant du soufre Download PDFInfo
- Publication number
- CA3012028A1 CA3012028A1 CA3012028A CA3012028A CA3012028A1 CA 3012028 A1 CA3012028 A1 CA 3012028A1 CA 3012028 A CA3012028 A CA 3012028A CA 3012028 A CA3012028 A CA 3012028A CA 3012028 A1 CA3012028 A1 CA 3012028A1
- Authority
- CA
- Canada
- Prior art keywords
- particles
- reactor
- inert
- gas
- leaching residue
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002386 leaching Methods 0.000 title claims abstract description 48
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 46
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 29
- 239000011593 sulfur Substances 0.000 title claims abstract description 29
- 239000012141 concentrate Substances 0.000 title claims abstract description 12
- 239000002184 metal Substances 0.000 title claims abstract description 11
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 11
- 239000002245 particle Substances 0.000 claims abstract description 112
- 239000007789 gas Substances 0.000 claims abstract description 79
- 230000001590 oxidative effect Effects 0.000 claims abstract description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 38
- 239000000463 material Substances 0.000 claims description 19
- 239000008187 granular material Substances 0.000 claims description 11
- 239000002002 slurry Substances 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 229910052681 coesite Inorganic materials 0.000 claims description 4
- 229910052906 cristobalite Inorganic materials 0.000 claims description 4
- 235000012239 silicon dioxide Nutrition 0.000 claims description 4
- 229910052682 stishovite Inorganic materials 0.000 claims description 4
- 229910052905 tridymite Inorganic materials 0.000 claims description 4
- 239000005864 Sulphur Substances 0.000 claims description 3
- 239000000428 dust Substances 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 229960005349 sulfur Drugs 0.000 claims 1
- 235000001508 sulfur Nutrition 0.000 claims 1
- 239000004576 sand Substances 0.000 description 26
- 238000005243 fluidization Methods 0.000 description 13
- 239000007787 solid Substances 0.000 description 13
- 238000002485 combustion reaction Methods 0.000 description 11
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 10
- 238000004140 cleaning Methods 0.000 description 10
- 229910052760 oxygen Inorganic materials 0.000 description 10
- 239000001301 oxygen Substances 0.000 description 10
- 238000000926 separation method Methods 0.000 description 10
- 238000005245 sintering Methods 0.000 description 9
- 238000001816 cooling Methods 0.000 description 7
- 239000011133 lead Substances 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 229910052709 silver Inorganic materials 0.000 description 6
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 5
- 239000004332 silver Substances 0.000 description 5
- 239000011701 zinc Substances 0.000 description 5
- 229910052725 zinc Inorganic materials 0.000 description 5
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 4
- 238000005054 agglomeration Methods 0.000 description 4
- 230000002776 aggregation Effects 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000002918 waste heat Substances 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000012065 filter cake Substances 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000004064 recycling Methods 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 229910052745 lead Inorganic materials 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000012265 solid product Substances 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- 230000007306 turnover Effects 0.000 description 2
- KEQXNNJHMWSZHK-UHFFFAOYSA-L 1,3,2,4$l^{2}-dioxathiaplumbetane 2,2-dioxide Chemical compound [Pb+2].[O-]S([O-])(=O)=O KEQXNNJHMWSZHK-UHFFFAOYSA-L 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 229910052924 anglesite Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 238000001033 granulometry Methods 0.000 description 1
- 229910052595 hematite Inorganic materials 0.000 description 1
- 239000011019 hematite Substances 0.000 description 1
- 230000003455 independent Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 1
- 239000011028 pyrite Substances 0.000 description 1
- 229910052683 pyrite Inorganic materials 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000002311 subsequent effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003463 sulfur Chemical class 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical class [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/20—Obtaining zinc otherwise than by distilling
- C22B19/22—Obtaining zinc otherwise than by distilling with leaching with acids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J6/00—Heat treatments such as Calcining; Fusing ; Pyrolysis
- B01J6/001—Calcining
- B01J6/004—Calcining using hot gas streams in which the material is moved
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/48—Sulfur dioxide; Sulfurous acid
- C01B17/50—Preparation of sulfur dioxide
- C01B17/508—Preparation of sulfur dioxide by oxidation of sulfur compounds
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/02—Roasting processes
- C22B1/10—Roasting processes in fluidised form
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/005—Separation by a physical processing technique only, e.g. by mechanical breaking
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23C—METHODS OR APPARATUS FOR COMBUSTION USING FLUID FUEL OR SOLID FUEL SUSPENDED IN A CARRIER GAS OR AIR
- F23C10/00—Fluidised bed combustion apparatus
- F23C10/02—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed
- F23C10/04—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed the particles being circulated to a section, e.g. a heat-exchange section or a return duct, at least partially shielded from the combustion zone, before being reintroduced into the combustion zone
- F23C10/08—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed the particles being circulated to a section, e.g. a heat-exchange section or a return duct, at least partially shielded from the combustion zone, before being reintroduced into the combustion zone characterised by the arrangement of separation apparatus, e.g. cyclones, for separating particles from the flue gases
- F23C10/10—Fluidised bed combustion apparatus with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed the particles being circulated to a section, e.g. a heat-exchange section or a return duct, at least partially shielded from the combustion zone, before being reintroduced into the combustion zone characterised by the arrangement of separation apparatus, e.g. cyclones, for separating particles from the flue gases the separation apparatus being located outside the combustion chamber
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Combustion & Propulsion (AREA)
- General Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
La présente invention concerne un procédé de traitement d'un résidu de lixiviation généré dans une lixiviation d'un concentré de métal contenant du soufre. Le résidu de lixiviation est introduit dans un réacteur, un gaz de fluidisation étant injecté dans le réacteur pour former un lit fluidisé contenant au moins une partie du résidu de lixiviation. Ainsi, le résidu de lixiviation est chauffé en présence de particules inertes à une température comprise entre 600 et 900 °C dans une atmosphère oxydante pour produire des particules calcinées et SO2. Au moins 60 % en poids des particules inertes est retiré du lit fluidisé, tandis qu'au moins 60 % en poids des particules calcinées est retiré conjointement avec un flux gazeux contenant des dégagements gazeux et le gaz de fluidisation.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102016101362 | 2016-01-26 | ||
| DE102016101362.5 | 2016-01-26 | ||
| PCT/EP2016/082772 WO2017129341A1 (fr) | 2016-01-26 | 2016-12-28 | Procédé et appareil de traitement d'un résidu de lixiviation d'un concentré de métal contenant du soufre |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA3012028A1 true CA3012028A1 (fr) | 2017-08-03 |
Family
ID=57799692
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA3012028A Pending CA3012028A1 (fr) | 2016-01-26 | 2016-12-28 | Procede et appareil de traitement d'un residu de lixiviation d'un concentre de metal contenant du soufre |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP3408018A1 (fr) |
| AU (1) | AU2016390040B2 (fr) |
| BR (1) | BR112018014777B1 (fr) |
| CA (1) | CA3012028A1 (fr) |
| EA (1) | EA037686B1 (fr) |
| MX (1) | MX2018008747A (fr) |
| WO (1) | WO2017129341A1 (fr) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110172595A (zh) * | 2019-06-24 | 2019-08-27 | 东北大学 | 一种钒渣悬浮态氧化焙烧-酸浸提钒的装置及方法 |
| EP3932534B1 (fr) * | 2020-06-30 | 2022-12-07 | AURA Technologie GmbH | Procédé et dispositif de recyclage des déchets contenant des métaux nobles |
| WO2023242465A1 (fr) * | 2022-06-17 | 2023-12-21 | Metso Metals Oy | Procédé et dispositif de traitement de résidus fins |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2785050A (en) * | 1952-08-21 | 1957-03-12 | Allied Chem & Dye Corp | Two-stage fluid-suspension roasting of iron sulfide ore |
| US2789034A (en) * | 1954-03-30 | 1957-04-16 | Allied Chem & Dye Corp | Process and apparatus for converting finely divided metal sulfide ore into sulfur dioxide and agglomerates of low sulfur cinder |
| US3941867A (en) * | 1974-09-04 | 1976-03-02 | Canadian Patents And Development Limited | Production of molybdenum trioxide from molybdenite in a fluidized bed |
| US4415540A (en) * | 1978-05-05 | 1983-11-15 | Provincial Holdings Ltd. | Recovery of non-ferrous metals by thermal treatment of solutions containing non-ferrous and iron sulphates |
| DE3322159A1 (de) * | 1983-06-21 | 1985-01-03 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur abtrennung von schadstoffen aus abgasen |
| ES2117028T3 (es) * | 1991-04-12 | 1998-08-01 | Metallgesellschaft Ag | Procedimiento para el tratamiento de mineral con valor de metales recuperables incluyendo componentes que contienen arsenico. |
| DE19609284A1 (de) * | 1996-03-09 | 1997-09-11 | Metallgesellschaft Ag | Verfahren zum Behandeln sulfidischer Erze, welche Gold und/oder Silber und als Begleitmetall mindestens Eisen enthalten |
| US20030198584A1 (en) * | 2002-04-19 | 2003-10-23 | Mason Bradley J. | Single stage denitration |
| DE10260735B4 (de) * | 2002-12-23 | 2005-07-14 | Outokumpu Oyj | Verfahren und Anlage zur Wärmebehandlung von sulfidischen Erzen |
| FI122447B (fi) * | 2009-12-22 | 2012-01-31 | Outotec Oyj | Menetelmä sulfidirikasteiden liuotuksessa syntyvän rikkipitoisen poisteen hyödyntämiseksi |
-
2016
- 2016-12-28 EP EP16826355.6A patent/EP3408018A1/fr active Pending
- 2016-12-28 MX MX2018008747A patent/MX2018008747A/es unknown
- 2016-12-28 AU AU2016390040A patent/AU2016390040B2/en active Active
- 2016-12-28 CA CA3012028A patent/CA3012028A1/fr active Pending
- 2016-12-28 WO PCT/EP2016/082772 patent/WO2017129341A1/fr active Application Filing
- 2016-12-28 BR BR112018014777-0A patent/BR112018014777B1/pt active IP Right Grant
- 2016-12-28 EA EA201891531A patent/EA037686B1/ru unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EA037686B1 (ru) | 2021-05-04 |
| AU2016390040B2 (en) | 2019-10-31 |
| WO2017129341A1 (fr) | 2017-08-03 |
| BR112018014777A2 (pt) | 2018-12-11 |
| MX2018008747A (es) | 2018-11-29 |
| EA201891531A1 (ru) | 2019-01-31 |
| BR112018014777B1 (pt) | 2022-07-26 |
| AU2016390040A1 (en) | 2018-08-16 |
| EP3408018A1 (fr) | 2018-12-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20211221 |
|
| EEER | Examination request |
Effective date: 20211221 |
|
| EEER | Examination request |
Effective date: 20211221 |
|
| EEER | Examination request |
Effective date: 20211221 |
|
| EEER | Examination request |
Effective date: 20211221 |
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| EEER | Examination request |
Effective date: 20211221 |
|
| EEER | Examination request |
Effective date: 20211221 |
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| EEER | Examination request |
Effective date: 20211221 |
|
| EEER | Examination request |
Effective date: 20211221 |