CA2957098C - Procede permettant de mesurer la mouillabilite d'une roche - Google Patents
Procede permettant de mesurer la mouillabilite d'une roche Download PDFInfo
- Publication number
- CA2957098C CA2957098C CA2957098A CA2957098A CA2957098C CA 2957098 C CA2957098 C CA 2957098C CA 2957098 A CA2957098 A CA 2957098A CA 2957098 A CA2957098 A CA 2957098A CA 2957098 C CA2957098 C CA 2957098C
- Authority
- CA
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- Prior art keywords
- oil
- water
- wettability
- fluid
- saturation
- Prior art date
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Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01V—GEOPHYSICS; GRAVITATIONAL MEASUREMENTS; DETECTING MASSES OR OBJECTS; TAGS
- G01V3/00—Electric or magnetic prospecting or detecting; Measuring magnetic field characteristics of the earth, e.g. declination, deviation
- G01V3/18—Electric or magnetic prospecting or detecting; Measuring magnetic field characteristics of the earth, e.g. declination, deviation specially adapted for well-logging
- G01V3/32—Electric or magnetic prospecting or detecting; Measuring magnetic field characteristics of the earth, e.g. declination, deviation specially adapted for well-logging operating with electron or nuclear magnetic resonance
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N24/00—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
- G01N24/08—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
- G01N24/081—Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity
Landscapes
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- High Energy & Nuclear Physics (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Geology (AREA)
- Remote Sensing (AREA)
- General Life Sciences & Earth Sciences (AREA)
- General Physics & Mathematics (AREA)
- Geophysics (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Geophysics And Detection Of Objects (AREA)
- Investigation Of Foundation Soil And Reinforcement Of Foundation Soil By Compacting Or Drainage (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Sampling And Sample Adjustment (AREA)
- Lubricants (AREA)
- Testing Of Devices, Machine Parts, Or Other Structures Thereof (AREA)
- Earth Drilling (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
Linvention concerne un procédé permettant de comparer un procédé de récupération du pétrole secondaire avec un procédé de récupération du pétrole tertiaire. Les deux procédés de récupération sont appliqués à un milieu poreux sensiblement saturé par un fluide contenant une phase huileuse et une phase aqueuse. Le procédé consiste à utiliser des mesures du temps de relaxation dans le calcul dun facteur de modification de lindice de mouillabilité pour la phase huileuse et la phase aqueuse, ce qui compare le procédé de récupération de pétrole tertiaire avec le procédé de récupération de pétrole secondaire.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09252811.6 | 2009-12-16 | ||
EP09252811A EP2341372A1 (fr) | 2009-12-16 | 2009-12-16 | Procédé pour mésurer la mouillabilité de roche |
GB1007694.1 | 2010-05-06 | ||
GB201007694A GB201007694D0 (en) | 2010-05-06 | 2010-05-06 | Method for measuring wettability |
CA2782731A CA2782731C (fr) | 2009-12-16 | 2010-11-19 | Procede permettant de mesurer la mouillabilite d'une roche |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2782731A Division CA2782731C (fr) | 2009-12-16 | 2010-11-19 | Procede permettant de mesurer la mouillabilite d'une roche |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2957098A1 CA2957098A1 (fr) | 2011-06-23 |
CA2957098C true CA2957098C (fr) | 2019-08-20 |
Family
ID=43589932
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2782731A Active CA2782731C (fr) | 2009-12-16 | 2010-11-19 | Procede permettant de mesurer la mouillabilite d'une roche |
CA2957098A Active CA2957098C (fr) | 2009-12-16 | 2010-11-19 | Procede permettant de mesurer la mouillabilite d'une roche |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2782731A Active CA2782731C (fr) | 2009-12-16 | 2010-11-19 | Procede permettant de mesurer la mouillabilite d'une roche |
Country Status (10)
Country | Link |
---|---|
US (1) | US9575203B2 (fr) |
EP (4) | EP2513678B1 (fr) |
CN (4) | CN102834737B (fr) |
AU (1) | AU2010332558B2 (fr) |
BR (1) | BR112012014902B1 (fr) |
CA (2) | CA2782731C (fr) |
DK (2) | DK2513678T3 (fr) |
EA (3) | EA201500033A1 (fr) |
MX (1) | MX2012006956A (fr) |
WO (1) | WO2011073608A1 (fr) |
Families Citing this family (68)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2513678B1 (fr) * | 2009-12-16 | 2015-01-07 | BP Exploration Operating Company Limited | Procédé pour mesurer la mouillabilité d'une roche |
US8805616B2 (en) * | 2010-12-21 | 2014-08-12 | Schlumberger Technology Corporation | Method to characterize underground formation |
GB2492795B (en) * | 2011-07-12 | 2013-11-20 | Schlumberger Holdings | Testing imbibition of liquid |
US9422470B2 (en) | 2011-09-15 | 2016-08-23 | Multi-Chem Group, Llc | Method for selection of surfactants in well stimulation |
US20140373616A1 (en) * | 2013-06-19 | 2014-12-25 | Conocophillips Company | Mechanical characterization of core samples |
WO2015017190A2 (fr) * | 2013-08-01 | 2015-02-05 | Conocophillips Company | Mesure dynamique in situ d'une mouillabilité de réservoir |
US9746576B2 (en) * | 2014-05-27 | 2017-08-29 | Baker Hughes Incorporated | Wettability estimation using magnetic resonance |
US9903826B2 (en) | 2014-09-17 | 2018-02-27 | Saudi Arabian Oil Company | Multi-objective core-flood test system for oil recovery evaluation |
CN104316554B (zh) * | 2014-10-27 | 2016-07-06 | 中国石油天然气股份有限公司 | 储层孔隙水可动性测试方法 |
US10023787B2 (en) | 2014-12-04 | 2018-07-17 | Halliburton Energy Services, Inc. | Surfactant selection methods for fluid recovery in subterranean formations |
US10983077B2 (en) * | 2015-01-29 | 2021-04-20 | Halliburton Energy Services, Inc. | Determining the oleophilic to aqueous phase fluid ratio for drilling fluids |
US10324222B2 (en) | 2015-02-26 | 2019-06-18 | Halliburton Energy Services, Inc. | Methods and systems employing NMR-based prediction of pore throat size distributions |
CN104730099A (zh) * | 2015-04-09 | 2015-06-24 | 上海理工大学 | 含油污泥含水率和含油率同时测量方法 |
US9599581B2 (en) * | 2015-04-22 | 2017-03-21 | Saudi Arabian Oil Company | Nuclear magnetic resonance gas isotherm technique to evaluate reservoir rock wettability |
US11353443B2 (en) | 2015-07-14 | 2022-06-07 | Conocophillips Company | Enhanced recovery response prediction |
WO2017023459A1 (fr) * | 2015-07-31 | 2017-02-09 | Halliburton Energy Services, Inc. | Appareil et procédé de traitement et d'interprétation de données de diagraphie par rmn |
CN105891250B (zh) * | 2016-03-30 | 2017-12-19 | 中国石油天然气股份有限公司 | 致密砂岩储层原始含水饱和度的确定方法 |
WO2018039038A1 (fr) * | 2016-08-26 | 2018-03-01 | Board Of Regents, The University Of Texas System | Mesure d'angles de contact entre une paire solide-fluide au moyen d'une imagerie par rayons x de l'interface solide-fluide-fluide à l'intérieur d'un capillaire |
CN106525888B (zh) | 2016-09-26 | 2018-10-16 | 中国石油天然气股份有限公司 | 一种测试致密油藏润湿性的方法及装置 |
US10443363B2 (en) | 2016-10-31 | 2019-10-15 | Exxonmobil Upstream Research Company | Method and system for core flood testing for reservoir souring studies |
AU2018212812A1 (en) | 2017-01-26 | 2019-08-15 | Dassault Systemes Simulia Corp. | Multi-phase flow visualizations based on fluid occupation time |
US11163923B2 (en) * | 2017-02-14 | 2021-11-02 | Landmark Graphics Corporation | Automated upscaling of relative permeability and capillary pressure in multi-porosity systems |
CN106990131B (zh) * | 2017-02-21 | 2019-08-06 | 上海大学 | 一种纳米流体改变岩心润湿性的快速评价方法 |
CN106841009B (zh) * | 2017-04-10 | 2023-10-03 | 中国石油大学(华东) | 一种振动辅助多孔介质渗吸的实验装置及方法 |
US10416063B2 (en) | 2017-11-02 | 2019-09-17 | Saudi Arabian Oil Company | Measuring rock wettability |
CN108020488B (zh) * | 2017-11-21 | 2019-11-19 | 中国石油大学(北京) | 核磁共振评价致密砂岩油气储层润湿性的方法与装置 |
US10451571B2 (en) | 2017-12-11 | 2019-10-22 | Saudi Arabian Oil Company | Measuring the wettability of porous media based on the temperature sensitivity of nuclear magnetic resonance relaxation time |
CN108303348B (zh) * | 2017-12-20 | 2020-07-14 | 中国石油化工股份有限公司 | 聚合物在油藏孔喉中拉伸降解特性模拟装置及系统 |
US11714040B2 (en) * | 2018-01-10 | 2023-08-01 | Dassault Systemes Simulia Corp. | Determining fluid flow characteristics of porous mediums |
US11340208B2 (en) * | 2018-01-23 | 2022-05-24 | Total Se | Method and apparatus for analyzing a rock sample |
CN108489864B (zh) * | 2018-02-11 | 2020-03-27 | 中国石油大学(北京) | 一种用核磁共振技术表征非均质润湿孔隙介质润湿性的方法 |
FR3079931B1 (fr) * | 2018-04-04 | 2021-04-30 | Ifp Energies Now | Procede de mesure de l'imbibition spontanee et/ou de la diffusion d'une phase aqueuse dans un milieu poreux par une methode de resonance magnetique nucleaire |
US10495589B2 (en) | 2018-04-17 | 2019-12-03 | Saudi Arabian Oil Company | Determining permeability of porous media based on nuclear magnetic resonance measurement |
CN108627533A (zh) * | 2018-05-25 | 2018-10-09 | 中国石油大学(华东) | 一种测定多孔介质中流体动用特征的核磁共振实验方法及装置 |
US10732316B2 (en) | 2018-08-14 | 2020-08-04 | Saudi Arabian Oil Company | Assessment of inaccessible pore volume for polymer flooding |
US11530598B2 (en) | 2018-08-21 | 2022-12-20 | Dassault Systemes Simulia Corp. | Determination of oil removed by gas via miscible displacement in reservoir rock |
CN109030292B (zh) * | 2018-09-26 | 2019-12-17 | 西南石油大学 | 一种致密岩石润湿性确定的新方法 |
US11314909B2 (en) * | 2018-10-05 | 2022-04-26 | Qatar Foundation For Education, Science And Community Development | Methods and systems for simulating multiphase flow through porous media |
US11249002B2 (en) * | 2019-03-28 | 2022-02-15 | Halliburton Energy Services, Inc. | Measuring size and shape of pore throat using digital porous plate experiments |
US10895543B2 (en) * | 2019-05-23 | 2021-01-19 | Saudi Arabian Oil Company | Wettability determination of rock samples |
US11249001B2 (en) | 2019-05-23 | 2022-02-15 | Saudi Arabian Oil Company | Determination of scanning loops of capillary pressure and relative permeability curves and wettability distribution of rock samples |
CN110261274B (zh) * | 2019-06-06 | 2021-10-26 | 西安石油大学 | 自发渗吸作用对水驱驱油效率静态贡献率的评价方法 |
CN110687612B (zh) * | 2019-09-17 | 2020-09-08 | 中国石油天然气股份有限公司 | 吸附油和游离油含量连续表征的页岩油分析方法及装置 |
CN110687613B (zh) * | 2019-09-25 | 2020-09-04 | 中国石油天然气股份有限公司 | 连续表征页岩油储层相对润湿性指数的方法 |
US11299986B2 (en) * | 2020-02-03 | 2022-04-12 | King Fahd University Of Petroleum And Minerals | Method for acid fracturing and acid stimulation based on NMR diffusion measurements |
CN113294146B (zh) * | 2020-02-05 | 2023-09-26 | 中国石油天然气股份有限公司 | 含沥青质储层的有效孔隙度计算的方法和装置 |
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US11131186B1 (en) * | 2020-03-04 | 2021-09-28 | King Fahd University Of Petroleum And Minerals | Method for determining wettability index of rock from T2 NMR measurements |
CN111553047B (zh) * | 2020-03-16 | 2023-04-11 | 中国地质大学(北京) | 润湿性评价参数获取方法及终端设备 |
US11555812B2 (en) | 2020-04-27 | 2023-01-17 | Saudi Arabian Oil Company | Methods of determining cation exchange sites occupied by crude oil and the wettability of cation exchange sites in rock core samples in a non-preserved state |
US11391683B2 (en) | 2020-06-05 | 2022-07-19 | Saudi Arabian Oil Company | Method to determine pore size distribution of rocks with rough surface from capillary pressure by nuclear magnetic resonance |
CN111855498B (zh) * | 2020-06-24 | 2023-04-07 | 同济大学 | 一种基于表面能理论的沥青混合料拌和温度确定方法 |
CN111520117B (zh) * | 2020-06-24 | 2022-04-22 | 陕西延长石油(集团)有限责任公司 | 一种适用于浅层水平缝油藏底部注水方法及验证 |
US11847391B2 (en) | 2020-06-29 | 2023-12-19 | Dassault Systemes Simulia Corp. | Computer system for simulating physical processes using surface algorithm |
US11187766B1 (en) | 2020-07-09 | 2021-11-30 | Saudi Arabian Oil Company | Methods and systems for determining fluid content in formation samples using low field nuclear magnetic resonance |
US11907625B2 (en) | 2020-12-29 | 2024-02-20 | Dassault Systemes Americas Corp. | Computer simulation of multi-phase and multi-component fluid flows including physics of under-resolved porous structures |
US11454097B2 (en) | 2021-01-04 | 2022-09-27 | Saudi Arabian Oil Company | Artificial rain to enhance hydrocarbon recovery |
US11821861B2 (en) | 2021-04-22 | 2023-11-21 | Baker Hughes Oilfield Operations Llc | Wettability estimation using magnetic resonance |
US11493461B1 (en) * | 2021-06-28 | 2022-11-08 | Baker Hughes Oilfield Operations Llc | Wettability estimation using T2 distributions of water in wetting and non-wetting phases |
US11614417B2 (en) | 2021-07-06 | 2023-03-28 | Saudi Arabian Oil Company | Determining saturation in low resistivity pay zones |
CN113916926B (zh) * | 2021-09-09 | 2024-06-07 | 西安石油大学 | 致密储层co2驱沥青质沉积作用下孔喉堵塞特征评价方法 |
CN113933333B (zh) * | 2021-09-09 | 2024-06-07 | 西安石油大学 | 致密储层co2驱沥青质沉积对岩石润湿性变化特征评价方法 |
US11566503B1 (en) | 2021-09-21 | 2023-01-31 | Saudi Arabian Oil Company | Oil recovery of a reservoir based on residual oil saturation |
AU2022389452A1 (en) * | 2021-11-16 | 2024-05-23 | Conocophillips Company | Systems and methods for determining surfactant impact on reservoir wettability |
CN114235879B (zh) * | 2021-12-22 | 2024-04-30 | 重庆大学 | 应力加载条件下测试盖层润湿性与毛细管压力的方法 |
US11746623B2 (en) | 2022-01-27 | 2023-09-05 | Halliburton Energy Services, Inc. | System and method to calibrate digital rock wettability |
CN116187140B (zh) * | 2023-03-09 | 2023-10-13 | 成都流体动力创新中心 | 动态冰弹性模量预测方法 |
CN116930244B (zh) * | 2023-09-19 | 2023-12-01 | 东北石油大学三亚海洋油气研究院 | 一种稠油裂缝的核磁图版绘制方法 |
Family Cites Families (30)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3213356A (en) * | 1962-10-22 | 1965-10-19 | California Research Corp | Methods for investigating the properties of fluid (materials) within porous media |
US3213357A (en) * | 1962-10-22 | 1965-10-19 | California Research Corp | Earth formation and fluid material investigation by nuclear magnetism relaxation rate determination |
US4089650A (en) * | 1971-12-20 | 1978-05-16 | Petrolite Corporation | Use of Diels-Alder adducts of dihydro-nitrogen heterocyclic phosphoramidates as corrosion inhibitors |
US3821232A (en) * | 1971-12-20 | 1974-06-28 | Petrolite Corp | 1,2-dihydro-pyridine-n-phosphonates and thiophosphonates |
US3965264A (en) * | 1971-12-20 | 1976-06-22 | Petrolite Corporation | Process for controlling microbiological organisms in aqueous or petroleum hydrocarbon systems |
US3998833A (en) * | 1971-12-20 | 1976-12-21 | Petrolite Corporation | Diels-alder adducts of dihydro-nitrogen heterocyclic phosphoramidates |
US3923490A (en) * | 1971-12-20 | 1975-12-02 | Petrolite Corp | Use of 1,2-dihydro-pyridine-N-phosphonates and thiophosphonates as microbiocides |
US3997293A (en) * | 1974-03-19 | 1976-12-14 | Petrolite Corporation | Use of dihydro-nitrogen heterocyclic phosphoramidates as corrosion inhibitors |
US4022276A (en) * | 1976-02-13 | 1977-05-10 | Marathon Oil Company | Method of selecting oil recovery fluids using nuclear magnetic resonance measurements |
US5162733A (en) * | 1991-02-26 | 1992-11-10 | Phillips Petroleum Company | Method for determining relative wettability |
US6392409B1 (en) * | 2000-01-14 | 2002-05-21 | Baker Hughes Incorporated | Determination of T1 relaxation time from multiple wait time NMR logs acquired in the same or different logging passes |
CN1049719C (zh) * | 1994-04-22 | 2000-02-23 | 郑金安 | 用普通取心-测试资料求水淹油层饱和度的方法 |
FR2811760B1 (fr) * | 2000-07-17 | 2002-09-13 | Inst Francais Du Petrole | Methode pour modeliser des deplacements de fluides dans un milieu poreux tenant compte d'effets d'hysteresis |
US6765380B2 (en) * | 2002-05-23 | 2004-07-20 | Schlumberger Technology Corporation | Determining wettability of an oil reservoir using borehole NMR measurements |
FR2844355B1 (fr) * | 2002-09-11 | 2005-03-25 | Inst Francais Du Petrole | Methode de mesure de la mouillabilite de roches par resonnance magnetique nucleaire |
ATE528659T1 (de) * | 2004-10-29 | 2011-10-15 | Green Imaging Technologies Inc | Verfahren und gerät zum messen des kapillardrucks in einer probe |
US7363164B2 (en) * | 2004-12-20 | 2008-04-22 | Schlumberger Technology Corporation | Method of evaluating fluid saturation characteristics in a geological formation |
WO2006110451A2 (fr) * | 2005-04-08 | 2006-10-19 | Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College | Drainage par gravite au moyen de gaz (gagd) permettant une meilleure recuperation de l'huile |
US7741841B2 (en) * | 2007-12-28 | 2010-06-22 | Schlumberger Technology Corporation | Time-lapsed diffusivity logging for monitoring enhanced oil recovery |
EP2144053A1 (fr) * | 2008-07-08 | 2010-01-13 | Services Pétroliers Schlumberger | Détermination de paramètres de formations géologiques par mesures RMN de dispersion du temps de relaxation longitudinal T1 |
MX2011000484A (es) * | 2008-07-14 | 2011-02-22 | Schlumberger Technology Bv | Instrumento de evaluacion de formacion y metodo. |
BRPI1008278B1 (pt) * | 2009-02-13 | 2019-05-21 | Shell Internationale Research Maatschappij B.V. | Método para intensificar a recuperação de óleo cru de uma formação subterrânea porosa. |
US8278922B2 (en) * | 2009-03-23 | 2012-10-02 | Schlumberger Technology Corporation | Continuous wettability logging based on NMR measurements |
WO2011063023A2 (fr) * | 2009-11-17 | 2011-05-26 | Board Of Regents, The University Of Texas System | Détermination de la saturation en pétrole dans une roche-réservoir à l'aide de nanoparticules paramagnétiques et d'un champ magnétique |
EP2513678B1 (fr) * | 2009-12-16 | 2015-01-07 | BP Exploration Operating Company Limited | Procédé pour mesurer la mouillabilité d'une roche |
EA026873B9 (ru) * | 2010-08-06 | 2017-08-31 | Бп Эксплорейшн Оперейтинг Компани Лимитед | Установка и способ испытаний многопорционных проб |
WO2013101752A1 (fr) * | 2011-12-29 | 2013-07-04 | Schlumberger Canada Limited | Caractérisation in situ de constituants d'une formation |
US9201158B2 (en) * | 2012-01-24 | 2015-12-01 | Schlumberger Technology Corporation | Estimating and displaying molecular size information of a substance |
US9140117B2 (en) * | 2012-07-13 | 2015-09-22 | Ingrain, Inc. | Method for evaluating relative permeability for fractional multi-phase, multi-component fluid flow through porous media |
US9244188B2 (en) * | 2012-08-03 | 2016-01-26 | Chevron U.S.A. Inc. | System and method for estimating a nuclear magnetic resonance relaxation time cutoff |
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US20120241149A1 (en) | 2012-09-27 |
US9575203B2 (en) | 2017-02-21 |
CN104849765A (zh) | 2015-08-19 |
CN104730586A (zh) | 2015-06-24 |
EP2513678A1 (fr) | 2012-10-24 |
MX2012006956A (es) | 2012-07-30 |
EP2801844A2 (fr) | 2014-11-12 |
EP2801844A3 (fr) | 2015-02-18 |
DK2513678T3 (en) | 2015-03-30 |
EP2513678B1 (fr) | 2015-01-07 |
EP2801845B1 (fr) | 2017-02-01 |
BR112012014902A2 (pt) | 2017-03-14 |
EA201200864A1 (ru) | 2013-02-28 |
EP2801845A1 (fr) | 2014-11-12 |
EA201500768A1 (ru) | 2015-12-30 |
WO2011073608A1 (fr) | 2011-06-23 |
CA2782731C (fr) | 2017-10-31 |
AU2010332558A1 (en) | 2012-07-12 |
DK2801845T3 (en) | 2017-05-01 |
EA023601B1 (ru) | 2016-06-30 |
CA2782731A1 (fr) | 2011-06-23 |
CN104730587A (zh) | 2015-06-24 |
EA029719B1 (ru) | 2018-05-31 |
CA2957098A1 (fr) | 2011-06-23 |
BR112012014902B1 (pt) | 2020-02-04 |
EP2804021A1 (fr) | 2014-11-19 |
CN102834737B (zh) | 2016-04-13 |
CN102834737A (zh) | 2012-12-19 |
AU2010332558B2 (en) | 2014-08-07 |
CN104849765B (zh) | 2017-10-24 |
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