CA2643896A1 - Method and apparatus for high mass concentration nano particle generation - Google Patents
Method and apparatus for high mass concentration nano particle generation Download PDFInfo
- Publication number
- CA2643896A1 CA2643896A1 CA002643896A CA2643896A CA2643896A1 CA 2643896 A1 CA2643896 A1 CA 2643896A1 CA 002643896 A CA002643896 A CA 002643896A CA 2643896 A CA2643896 A CA 2643896A CA 2643896 A1 CA2643896 A1 CA 2643896A1
- Authority
- CA
- Canada
- Prior art keywords
- particles
- chamber
- dilution
- vaporization chamber
- flow
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 239000002105 nanoparticle Substances 0.000 title claims abstract description 48
- 238000000034 method Methods 0.000 title claims abstract description 38
- 239000002245 particle Substances 0.000 claims abstract description 127
- 238000010790 dilution Methods 0.000 claims abstract description 70
- 239000012895 dilution Substances 0.000 claims abstract description 70
- 239000007789 gas Substances 0.000 claims abstract description 65
- 238000009834 vaporization Methods 0.000 claims abstract description 56
- 230000008016 vaporization Effects 0.000 claims abstract description 56
- 239000013590 bulk material Substances 0.000 claims abstract description 38
- 239000000463 material Substances 0.000 claims abstract description 37
- 239000008275 solid aerosol Substances 0.000 claims abstract description 28
- 238000010438 heat treatment Methods 0.000 claims abstract description 22
- 239000011261 inert gas Substances 0.000 claims abstract description 21
- 238000004891 communication Methods 0.000 claims abstract description 10
- 239000012808 vapor phase Substances 0.000 claims abstract description 6
- 238000005054 agglomeration Methods 0.000 claims abstract 5
- 230000002776 aggregation Effects 0.000 claims abstract 5
- 239000000443 aerosol Substances 0.000 claims description 39
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 11
- 239000001301 oxygen Substances 0.000 claims description 11
- 229910052760 oxygen Inorganic materials 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- 229910052786 argon Inorganic materials 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 239000002041 carbon nanotube Substances 0.000 claims description 3
- 229910021393 carbon nanotube Inorganic materials 0.000 claims description 3
- 229910000420 cerium oxide Inorganic materials 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 claims description 3
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- 238000003801 milling Methods 0.000 claims description 2
- 238000009826 distribution Methods 0.000 description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
- 239000011364 vaporized material Substances 0.000 description 10
- 239000012071 phase Substances 0.000 description 9
- 239000000843 powder Substances 0.000 description 9
- 238000001228 spectrum Methods 0.000 description 9
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 238000002474 experimental method Methods 0.000 description 7
- 229910052757 nitrogen Inorganic materials 0.000 description 7
- 238000005070 sampling Methods 0.000 description 7
- 231100000041 toxicology testing Toxicity 0.000 description 7
- 238000003917 TEM image Methods 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 238000012546 transfer Methods 0.000 description 5
- 238000001069 Raman spectroscopy Methods 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 239000012159 carrier gas Substances 0.000 description 4
- 229910003472 fullerene Inorganic materials 0.000 description 4
- 238000004128 high performance liquid chromatography Methods 0.000 description 4
- 238000001237 Raman spectrum Methods 0.000 description 3
- 238000012512 characterization method Methods 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 238000005087 graphitization Methods 0.000 description 3
- 231100000037 inhalation toxicity test Toxicity 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 230000037361 pathway Effects 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 238000001878 scanning electron micrograph Methods 0.000 description 3
- 231100000419 toxicity Toxicity 0.000 description 3
- 230000001988 toxicity Effects 0.000 description 3
- 238000004566 IR spectroscopy Methods 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000012377 drug delivery Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000003384 imaging method Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002086 nanomaterial Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- -1 Argon Ion Chemical class 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000976924 Inca Species 0.000 description 1
- 229920000034 Plastomer Polymers 0.000 description 1
- 238000003991 Rietveld refinement Methods 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 230000002730 additional effect Effects 0.000 description 1
- 229910003481 amorphous carbon Inorganic materials 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- XKRFYHLGVUSROY-UHFFFAOYSA-N argon Substances [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000008499 blood brain barrier function Effects 0.000 description 1
- 210000001218 blood-brain barrier Anatomy 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000001427 coherent effect Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 238000000445 field-emission scanning electron microscopy Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 238000002186 photoelectron spectrum Methods 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
- B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/85—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/51—Particles with a specific particle size distribution
- C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Manufacturing & Machinery (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Composite Materials (AREA)
- Medicinal Preparation (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Carbon And Carbon Compounds (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US77911906P | 2006-03-03 | 2006-03-03 | |
| US60/779,119 | 2006-03-03 | ||
| US83705706P | 2006-08-10 | 2006-08-10 | |
| US60/837,057 | 2006-08-10 | ||
| PCT/US2007/005499 WO2007103256A2 (en) | 2006-03-03 | 2007-03-02 | Method and apparatus for high mass concentration nano particle generation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2643896A1 true CA2643896A1 (en) | 2007-09-13 |
Family
ID=38475442
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002643896A Abandoned CA2643896A1 (en) | 2006-03-03 | 2007-03-02 | Method and apparatus for high mass concentration nano particle generation |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9845242B2 (enExample) |
| EP (1) | EP2001796A2 (enExample) |
| JP (1) | JP2009531256A (enExample) |
| KR (1) | KR20080102268A (enExample) |
| CA (1) | CA2643896A1 (enExample) |
| WO (1) | WO2007103256A2 (enExample) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012058246A1 (en) * | 2010-10-25 | 2012-05-03 | Battelle Memorial Institute | Nano-aerosol generation system and methods |
| NO334282B1 (no) | 2012-04-27 | 2014-01-27 | Reactive Metal Particles As | Apparatur og metode for fremstilling av partikulært materiale |
| KR20150114290A (ko) * | 2014-04-01 | 2015-10-12 | 주식회사 에코픽쳐스 | 나노입자 생성장치 |
| US9951420B2 (en) | 2014-11-10 | 2018-04-24 | Sol Voltaics Ab | Nanowire growth system having nanoparticles aerosol generator |
| KR101953751B1 (ko) * | 2016-12-01 | 2019-03-08 | (주)차세대소재연구소 | 향상된 분산성을 가지는 열정제된 고순도 나노다이아몬드의 제조방법 |
| CN112664936B (zh) * | 2020-12-29 | 2023-03-24 | 华中科技大学 | 一种多喷嘴喷雾燃烧合成纳米颗粒的系统 |
| WO2024014991A1 (ru) * | 2022-07-09 | 2024-01-18 | Алексей Николаевич ГОЛДАЕВ | Способ получения одиночных наночастиц на поверхности связующей основы |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1161164A1 (ru) * | 1983-12-13 | 1985-06-15 | Черкасский Филиал Киевского Ордена Ленина Политехнического Института Им.50-Летия Великой Октябрьской Социалистической Революции | Способ создани концентраций примесей масел в газах |
| JP4188091B2 (ja) | 2001-05-15 | 2008-11-26 | イー インク コーポレイション | 電気泳動粒子 |
| GB0114033D0 (en) * | 2001-06-09 | 2001-08-01 | Innovata Biomed Ltd | Process |
| CN101061064B (zh) * | 2002-07-03 | 2011-03-30 | Nano-C公司 | 富勒烯的分离和提纯 |
| CN101262939A (zh) | 2002-12-17 | 2008-09-10 | 纳幕尔杜邦公司 | 通过反应室等离子体反应器系统利用蒸发-冷凝过程制备纳米颗粒的方法 |
| US20060024435A1 (en) * | 2003-10-20 | 2006-02-02 | Dean Holunga | Turbulent mixing aerosol nanoparticle reactor and method of operating the same |
| US7527824B2 (en) * | 2004-06-25 | 2009-05-05 | Becker Michael F | Methods for producing coated nanoparticles from microparticles |
| US20090317937A1 (en) | 2008-06-20 | 2009-12-24 | Atul Gupta | Maskless Doping Technique for Solar Cells |
-
2007
- 2007-03-02 CA CA002643896A patent/CA2643896A1/en not_active Abandoned
- 2007-03-02 WO PCT/US2007/005499 patent/WO2007103256A2/en not_active Ceased
- 2007-03-02 US US12/281,057 patent/US9845242B2/en active Active
- 2007-03-02 EP EP07752214A patent/EP2001796A2/en not_active Withdrawn
- 2007-03-02 JP JP2008557426A patent/JP2009531256A/ja active Pending
- 2007-03-02 KR KR1020087023931A patent/KR20080102268A/ko not_active Withdrawn
-
2017
- 2017-11-06 US US15/805,022 patent/US10392252B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| KR20080102268A (ko) | 2008-11-24 |
| US10392252B2 (en) | 2019-08-27 |
| EP2001796A2 (en) | 2008-12-17 |
| WO2007103256A3 (en) | 2008-02-07 |
| US9845242B2 (en) | 2017-12-19 |
| US20180065853A1 (en) | 2018-03-08 |
| US20090317336A1 (en) | 2009-12-24 |
| JP2009531256A (ja) | 2009-09-03 |
| WO2007103256A2 (en) | 2007-09-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Discontinued |
Effective date: 20130304 |