CA2559516A1 - Detection of diamonds - Google Patents

Detection of diamonds Download PDF

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Publication number
CA2559516A1
CA2559516A1 CA002559516A CA2559516A CA2559516A1 CA 2559516 A1 CA2559516 A1 CA 2559516A1 CA 002559516 A CA002559516 A CA 002559516A CA 2559516 A CA2559516 A CA 2559516A CA 2559516 A1 CA2559516 A1 CA 2559516A1
Authority
CA
Canada
Prior art keywords
particle
diamond
particles
photons
potentially
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002559516A
Other languages
French (fr)
Other versions
CA2559516C (en
Inventor
Simon Henry Connell
Jacques Pierre Friedrich Sellschop (Deceased)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SELLSCHOP SUSAN MARIETTA
University of the Witwatersrand, Johannesburg
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2559516A1 publication Critical patent/CA2559516A1/en
Application granted granted Critical
Publication of CA2559516C publication Critical patent/CA2559516C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/22Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
    • G01N23/221Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material by activation analysis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B07SEPARATING SOLIDS FROM SOLIDS; SORTING
    • B07CPOSTAL SORTING; SORTING INDIVIDUAL ARTICLES, OR BULK MATERIAL FIT TO BE SORTED PIECE-MEAL, e.g. BY PICKING
    • B07C5/00Sorting according to a characteristic or feature of the articles or material being sorted, e.g. by control effected by devices which detect or measure such characteristic or feature; Sorting by manually actuated devices, e.g. switches
    • B07C5/34Sorting according to other particular properties
    • B07C5/346Sorting according to other particular properties according to radioactive properties

Abstract

The invention concerns a method and apparatus for detecting the presence of diamond in a particle and for sorting particles according to whether or not they include diamonds. In the method, the particle is irradiated (36) with photons of selected energy at which the GDR (giant dipole resonance) is excited for the nuclear reaction of the photons with carbon, and the particle is identified as potentially a diamond or diamond-containing particle according to its interaction within the incident photons. In the preferred embodiments, the particle is identified (42) as potentially a diamond or diamond-containing particle according to whether the isotope 11C, with a characteristic half-life of approximately twenty minutes, is produced by the photon/carbon nuclear reaction, and according to whether detectable coincident and collinear gamma ray photons at a distinctive energy level are emitted by the particle.

Claims (19)

1.
A method of detecting the presence of diamond in a particle, wherein the particle is irradiated with photons of selected energy at which the GDR (giant dipole resonance) is excited for the nuclear reaction of the photons with carbon, and identifying the particle as potentially a diamond or diamond-containing particle according to its interaction within the incident photons.
2.
A method according to claim 1 wherein the particle is irradiated with bremsstrahlung encompassing a range of energy levels including a characteristic GDR energy level for carbon.
3.
A method according to claim 2 wherein the particle is irradiated with bremsstrahlung at a range of energy levels including a characteristic energy level of 22MeV.
4.
A method according to any one of the preceding claims comprising the steps of identifying the particle as potentially a diamond or diamond-containing particle according to whether the isotope "C, with a characteristic half life of approximately twenty minutes, is produced by the photon/carbon nuclear reaction.
5.
A method according to claim 4 comprising the step of identifying the particle as potentially a diamond or diamond-containing particle according to whether coincident and collinear gamma ray photons at a distinctive energy level are emitted by the particle.
6.
A method according to claim 5 wherein the particle is identified as potentially a diamond or diamond-containing particle according to whether coincident and collinear gamma ray photons at an energy level of 0.511 MeV are emitted by the particle.
7.
A method according to either one of claims 5 or 6 comprising the step of analysing detected coincident and collinear gamma ray photons to provide an indication of the relative position of a concentrated carbon inclusion, potentially a diamond, in a particle which is host to such inclusion.
8.
An on-line particle sorting method comprising the steps of irradiating particles with photons of gamma radiation at an energy level at which GDR (giant dipole resonance) is excited for the nuclear reaction of the photons with carbon, identifying particles as potentially diamond or diamond-containing particles according to whether the isotope "C, with a characteristic half life of approximately twenty minutes, is produced by the photon/carbon nuclear reaction and whether coincident and collinear gamma ray photons at a distinctive energy level are emitted by the particles, and separating from other particles those particles which are identified as potentially diamond or diamond-containing particles.
9.
An on-line particle sorting method according to claim 8 wherein, after irradiation, the particles are retained for at least twenty minutes before further analysis steps are carried out on the particles.
10.
A method according to any one of claims 1 to 3 wherein the particle is identified as potentially a diamond or diamond-containing particle if absorption of photon energy by the particle is indicative of the presence of carbon in concentrated form.
11.
A method according to claim 10 wherein the particle is a kimberlite particle and the method comprises the steps of deriving a differential energy absorption image for the particle and determining whether that image is indicative of the presence of a concentration of carbon in the particle.
12.
An apparatus for detecting the presence of diamond in a particle, the apparatus comprising means for irradiating the particle with photons of gamma radiation at a selected energy at which the GDR (giant dipole resonance) is excited for the nuclear reaction of the photons with carbon, and means for identifying the particle as potentially a diamond or diamond-containing particle according to the interaction of the particle with the incident photons.
13.
An apparatus according to claim 12 wherein the irradiation means is arranged to irradiate the particle with gamma radiation at an energy level of 22MeV.
14.
An apparatus according to claim 12 or claim 13 comprising means for determining whether the isotope "C, with a characteristic half life of approximately twenty minutes, is produced by the photon/carbon nuclear reaction and whether pairs of coincident and collinear gamma ray photons at a distinctive energy level are emitted by the particle.
15.
An apparatus according to claim 14 comprising means for determining whether coincident and collinear gamma ray photons at an energy level of 0.511 MeV are emitted by the particle.
16.
An apparatus according to claim 14 or claim 15 comprising means for analysing detected coincident and collinear gamma ray photons to provide an indication of the relative position of a concentrated carbon inclusion, potentially a diamond, in a particle which is host to such inclusion.
17.
An on-line particle sorting apparatus comprising irradiation means for irradiating particles which are to be sorted with photons of gamma radiation at an energy level at which GDR (giant dipole resonance) is excited for the nuclear reaction of the photons with carbon and identification means for identifying particles as potentially diamond or diamond-containing particles according to whether the isotope "C, with a characteristic half-life of approximately twenty minutes, is produced by the photon/carbon nuclear reaction and whether coincident and collinear gamma ray photons at a distinctive energy level are emitted by the particles, and means for separating from other particles those particles which are identified as potentially diamond or diamond-containing particles.
18.
An on-line particle sorting apparatus according to claim 17 including temporary storage means for retaining the particles for a period of at least twenty minutes before operation of the identification means.
19.
An on-line particle sorting apparatus according to claim 18 wherein the storage means comprises a hopper for holding the particles after irradiation and for releasing the particles to the identification means after it has held them for at least twenty minutes.
CA2559516A 2004-03-12 2005-03-14 Detection of diamonds Active CA2559516C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ZA2004/2010 2004-03-12
ZA200402010 2004-03-12
PCT/IB2005/000643 WO2005088283A1 (en) 2004-03-12 2005-03-14 Detection of diamonds

Publications (2)

Publication Number Publication Date
CA2559516A1 true CA2559516A1 (en) 2005-09-22
CA2559516C CA2559516C (en) 2012-07-10

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CA2559516A Active CA2559516C (en) 2004-03-12 2005-03-14 Detection of diamonds

Country Status (7)

Country Link
CN (1) CN1942759B (en)
AP (1) AP1986A (en)
AU (1) AU2005220403B2 (en)
CA (1) CA2559516C (en)
RU (1) RU2334974C2 (en)
WO (1) WO2005088283A1 (en)
ZA (1) ZA200608025B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11415722B2 (en) * 2017-10-19 2022-08-16 University Of Johannesburg Gamma ray tomographic radiography

Families Citing this family (14)

* Cited by examiner, † Cited by third party
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AP2011005890A0 (en) * 2009-02-23 2011-10-31 Tech Resources Pty Ltd Detecting a mineral within a material.
GB2481283B (en) 2010-06-03 2013-07-17 Element Six Ltd A method of increasing the toughness and/or wear resistance of diamond tool pieces and diamond tool pieces fabricated by said method
US20130186992A1 (en) * 2010-08-04 2013-07-25 Technological Resources Pty. Limited Sorting mined material
RU2470714C1 (en) * 2011-07-21 2012-12-27 Общество с ограниченной ответственностью "Лаборатория рентгенодиагностических систем" Method of separating diamonds
GB2504052B (en) * 2012-03-16 2017-05-10 De Beers Uk Ltd Sorting aggregate material
RU2517148C1 (en) * 2012-12-28 2014-05-27 Евгений Матвеевич Лукьянченко Method of useful material particles separation and device to this end
RU2521723C1 (en) * 2013-03-01 2014-07-10 Общество с ограниченной ответственностью "Нейтронные технологии" Method and apparatus for detecting diamonds in kimberlite
RU2612734C2 (en) * 2015-08-18 2017-03-13 Общество с ограниченной ответственностью "Диамант" Installation for dry enrichment of kimberlite ore by method of labelled neutrons
CN105499156B (en) * 2015-12-02 2019-03-01 虞雅仙 A kind of water drilling inspection method
RU2670677C9 (en) * 2017-02-07 2019-09-13 Акционерная компания "АЛРОСА" (публичное акционерное общество) "АК "АЛРОСА" (ПАО)) Device for diamond separation
WO2020121214A1 (en) * 2018-12-11 2020-06-18 University Of Johannesburg Detector arrangement, detection system and method of processing data from a detector arrangement for high throughput data handling
WO2020152618A1 (en) * 2019-01-23 2020-07-30 University Of Johannesburg Detector arrangement, detection system and method of positioning a detector arrangement to reduce imaging artefacts
NL2026338B1 (en) * 2020-08-25 2022-04-29 Univ Johannesburg Material analysis method and system
CN112024451B (en) * 2020-08-28 2021-08-31 北京科技大学 Ore sorting decision-making method based on analysis of operation characteristic curve of subject

Family Cites Families (9)

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Publication number Priority date Publication date Assignee Title
EP0059033A1 (en) * 1981-02-24 1982-09-01 Sphere Investments Limited Ore sorting
US4428902A (en) * 1981-05-13 1984-01-31 Murray Kenneth M Coal analysis system
US4756866A (en) * 1985-10-09 1988-07-12 Alvarez Luis W Nitrogen detection
GB2219081B (en) * 1988-05-06 1992-12-02 Gersan Ets Identifying specific objects or zones
GB2219394B (en) * 1988-05-06 1992-09-16 Gersan Ets Sensing a narrow frequency band of radiation and examining objects or zones
US5334652A (en) * 1991-06-18 1994-08-02 Exxon Chemical Patents, Inc. Polyester-based coating compositions having high pigment-to-binder ratios
CA2138503C (en) * 1993-12-22 2004-10-12 Ulf Anders Staffan Tapper Method and apparatus for the classification of particulate matter
CA2139537C (en) * 1994-01-07 2007-04-24 Ulf Anders Staffan Tapper Method and apparatus for the classification of matter
CN1363836A (en) * 2001-08-18 2002-08-14 李晓蔚 Method for judging natural product

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11415722B2 (en) * 2017-10-19 2022-08-16 University Of Johannesburg Gamma ray tomographic radiography

Also Published As

Publication number Publication date
CN1942759A (en) 2007-04-04
AP2006003753A0 (en) 2006-10-31
RU2334974C2 (en) 2008-09-27
CA2559516C (en) 2012-07-10
WO2005088283A1 (en) 2005-09-22
AU2005220403B2 (en) 2010-12-09
AU2005220403A1 (en) 2005-09-22
CN1942759B (en) 2011-01-12
RU2006135960A (en) 2008-04-20
ZA200608025B (en) 2008-06-25
AP1986A (en) 2009-04-01

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