CA2521675C - Method of preparing an integrated circuit die for imaging - Google Patents

Method of preparing an integrated circuit die for imaging Download PDF

Info

Publication number
CA2521675C
CA2521675C CA002521675A CA2521675A CA2521675C CA 2521675 C CA2521675 C CA 2521675C CA 002521675 A CA002521675 A CA 002521675A CA 2521675 A CA2521675 A CA 2521675A CA 2521675 C CA2521675 C CA 2521675C
Authority
CA
Canada
Prior art keywords
metal
integrated circuit
layer
circuit die
metal layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA002521675A
Other languages
French (fr)
Other versions
CA2521675A1 (en
Inventor
Lev Klibanov
Sherri Lynn Griffin
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TechInsights Inc
Original Assignee
Chipworks Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chipworks Inc filed Critical Chipworks Inc
Priority to CA002521675A priority Critical patent/CA2521675C/en
Priority to PCT/CA2006/001590 priority patent/WO2007036034A1/en
Priority to CN2006800360250A priority patent/CN101287994B/en
Publication of CA2521675A1 publication Critical patent/CA2521675A1/en
Application granted granted Critical
Publication of CA2521675C publication Critical patent/CA2521675C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R31/00Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
    • G01R31/28Testing of electronic circuits, e.g. by signal tracer
    • G01R31/2851Testing of integrated circuits [IC]
    • G01R31/2898Sample preparation, e.g. removing encapsulation, etching

Abstract

Integrated circuit dies are prepared for imaging by completely etching away all metal from the metal lines without removing barrier layers that underlie the metal lines. The metal vias may also be removed, especially if they are formed from the same metal as the metal lines, as in copper damascene circuits. This provides high contrast images that permits circuit layout extraction software to readily distinguish between metal lines and vias.

Description

OR File No. 14774-20CA
METHOD OF PREPARING AN INTEGRATED CIRCUIT DIE
FOR IMAGING
TECHNICAL FIELD
The invention relates in general to examination and analysis of integrated circuits and, in particular, to methods of preparing an integrated circuit die for imaging to permit a structure and layout of the integrated circuit to be extracted.
BACKGROUND OF THE INVENTION
As is well known in the art, the examination and analysis of integrated circuits requires sophisticated sample preparation techniques and imaging tools. In the past, integrated circuits were generally constructed using aluminum for metal lines in each of the metal layers of the integrated circuit and tungsten for vias interconnecting the metal lines with components formed on a polycrystalline silicon layer. Since aluminum and tungsten can be selectively etched, integrated circuits could be deconstructed using selective etching techniques that permit the vias to be segregated from the metal lines, as will be explained below in more detail with reference to Fig. 1. Furthermore, modern integrated circuits generally require sophisticated imaging equipments such as a scanning electron microscope because components are frequently too small to be visible under an optical microscope. In order to distinguish vias from metal lines, it is therefore necessary to acquire images that show contrast between the vias and the metal lines. Tungsten and aluminum are readily distinguished in scanning electron microscope images.
- 2 -OR File No. 14774-20CA
Consequently, a prior art technique illustrated in Figs. 1a-1d for preparing an integrated circuit die for imaging is commonly used to acquire tile images of a deconstructed area of interest of an integrated circuit die. Fig. 1a is a schematic cross sectional diagram of two metal layers of an integrated circuit die generally indicated by the reference 10. As is well known in the art, each metal layer is covered by an interlayer dielectric (ILD) 12 of a suitable material well known in the art. A metal layer N+1 is separated from the interlayer dielectric 18 on which it is deposited by a barrier layer 16, also composed of a suitable material well known in the art. The barrier layers 16, 22 prevent the deposited metal layers N+1, N from migrating into the interlayer dielectric 18, 24 onto which they are deposited.
A metal line 14 of metal layer N+1 is connected to a metal line 20 of metal layer N by a via 26, which is also formed in a manner well known in the art. The barrier layer 16 that separates via 26 from metal layer N is conductive and provides an electrical connection between the via 26 and the metal line 20.
In order to acquire tile images of the integrated circuit 10, passivation layer 12, and any optional barrier material (Fig. 1a) is first removed using a wet or dry etching process or a chemical and/or mechanical polishing process to expose metal lines 14 of metal layer N+1. The integrated circuit die 10 is then placed on a precision stage of the imaging equipment, a scanning electron microscope for example, and tile images are acquired of the area of interest in a manner well known in the art. After the tile images of metal layer N+1 have been acquired, the metal layer N+1 is removed using, for example, a wet or dry etching process or a chemical and/or mechanical polishing
- 3 -OR File No. 14774-20CA
process. The process is controlled to remove the metal layer N+1 while preserving the integrity of the vias 26, as shown in Fig. 1c. Thereafter, an etching solution is selected that will remove the barrier layer 16 as well as the interlayer dielectric 18 while leaving the via 26 intact. The results of that etching step are shown schematically in Fig. 1d. If the etching is carefully controlled, the via 26 remains intact and portions of the barrier layer 16r that are shielded by the via 26 and surround the via 26 remain after etching is complete. Thus metal lines 20 of metal layer N and the via 26 are exposed and tile images of the exposed via 26 and metal layer N are acquired in a manner well known in the art.
This prior art process can be referred to as a "bottom up" process because the vias are imaged in conjunction with the metal lines to which they are connected at their bottom ends. While this prior art technique works well for integrated circuits constructed using aluminum metal lines and tungsten vias due to the different etching characteristics of the two metals, integrated circuits are now being manufactured using copper metal lines and copper vias. This makes the prior art method very difficult to perform and complicates layout extraction, as will be explained below with reference to FIG. 2.
FIG. 2 is a reproduction of an image of a copper damascene integrated circuit prepared using the prior art process described above with reference to FIGs 1a-1d. The image 30 was acquired using a scanning electron microscope.
The integrated circuit die was prepared for imaging using a controlled etching process that removed the metal lines of metal layer N+1 and the interlayer dielectric 18 while leaving, to an extent possible, the vias 26. As can be
- 4 -OR File No. 14774-20CA
understood by those skilled in the art, the etching process is difficult to control when the vias and the metal lines are made of the same metal. Consequently, some of the vias 26 are eroded and have an oblong shape in the image. As well, the copper lines 32 and the vias 26 are very similar in shade and it is not consistently clear to which metal line 32 a via 26 is connected. Circuit layout information is therefore difficult to extract and prone to errors.
There therefore exists a need for a method of preparing an integrated circuit die for imaging to permit a structure and layout of the integrated circuit to be extracted, regardless of metals used to construct the integrated circuit.
SUN~lARY OF THE INVENTION
It is therefore an object of the invention to provide methods of preparing an integrated circuit die for imaging that permits a structure and layout of the integrated circuit to be reliably extracted.
In accordance with one aspect of the present invention there is provided a method of preparing an integrated circuit die for imaging, comprising: removing interlayer dielectric material from a metal layer of the integrated circuit die to expose the metal layer; and removing all metal from metal lines of the metal layer without removing a barrier layer that underlies each metal line.
In accordance with another aspect of the present invention there is provided a method for extracting circuit information from an integrated circuit die, comprising:
removing all material covering a first metal layer of the integrated circuit die; etching away all metal from the first layer to completely expose a barrier layer underlying
- 5 -OR File No. 14774-20CA
each metal line in the first metal layer; placing the integrated circuit die on a precision stage and acquiring tile images of an area of interest of the integrated circuit die; repeating the removing, etching and placing for each other metal layer; and removing an interlayer dielectric material covering a polycrystalline silicon layer of the integrated circuit die, placing the integrated circuit die on the precision stage and acquiring tile images of polycrystalline silicon layer.
In accordance with yet another aspect of the present invention there is provided a method of preparing an integrated circuit for imaging for the purpose of extracting circuit information, comprising removing all material including all metal from the metal lines and metal vias of a metal layer of the integrated circuit die, and acquiring tile images of barrier Layers exposed after all of the metal has been removed from the metal lines and the metal vias of the metal layer.
BRIEF DESCRIPTION OF THE DRAWINGS
Further features and advantages of the present invention will become apparent from the following detailed description, taken in combination with the appended drawings, in which:
Figs. 1a-1d are schematic diagrams illustrating a technique for preparing an integrated circuit die for imaging in accordance with the prior art;
Fig. 2 is a reproduction of an image of a copper damascene integrated circuit prepared using the method shown in Figs. 1a-1d;
- 6 -OR File No. 14774-20CA
Fig. 3 is a flow chart providing a high level overview of methods for preparing an integrated circuit die for imaging in accordance with the invention;
Figs. 4a-4d are schematic diagrams illustrating a process for preparing an integrated circuit die for imaging in accordance with the invention;
Fig. 5 is a reproduction of an image of an integrated circuit prepared in accordance with a process illustrated in Figs. 4a-4c; and Fig. 6 is a reproduction of an image of an integrated circuit prepared in accordance with a process illustrated in Figs 4a, 4b and 4d.
It will be noted that throughout the appended drawings, like features are identified by like reference numerals.
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENT
The invention provides methods of preparing an integrated circuit die for imaging that is useful for preparing integrated circuit dies constructed using any process in which both the metal lines and vias of the integrated circuit are made of the same metal. The methods are very useful for integrated circuits made using an all-copper or an all-aluminum process. However, the process is equally useful for preparing traditional aluminum/tungsten integrated circuits for imaging. In accordance with the method, after a metal layer of an integrated circuit is exposed, all the metal lines in the metal layer are etched away leaving behind barrier layer material. When images are acquired using a scanning electron microscope, the barrier layer material appears as a first color, typically
- 7 _ OR File No. 14774-20CA
light grey. If the chip is a copper/copper or aluminum/aluminum construction, etching away the metal lines likewise etches away the vias, leaving a barrier layer that surrounds each via. When imaged, etched away vias appear in a contrasting color, i.e. dark grey or black. The contrasting colors permit feature extraction software and/or an engineer analyst to readily discriminate between the barrier layer material for the metal lines and the barrier material lining cavities previously occupied by the metal vial.
Fig. 3 is a flow chart providing a high level overview of the methods in accordance with the invention. As is well understood in the art, before an integrated circuit die can be imaged it must be de-capsulated from a package (step 40). After the integrated circuit die is de-capsulated, a passivation layer 42 covering the first metal layer (metal layer N+1) is removed (step 42), as shown in Fig. 4b. The passivation layer may be removed using an etching process well known in the art.
The integrated circuit is then subjected to a wet or dry etching process to etch away metal lines 14 and vias 26 in order to expose an underlying barrier layer 16 (step 44). After the metal lines 14 and vias 26 are etched away (see FIG. 4c), the chip is placed on a precision stage (step 46) and tile images (step 48) are acquired of any area of interest. It is then determined (step 50) whether another metal layer of the integrated circuit exits. If so, an interlayer dielectric (ILD) 18 and any barrier material (not shown) that covers the metal lines is also removed. As is understood by those skilled in the art, a barrier layer is always applied under metal lines but the barrier layer is not always applied over the metal lines.

_ g _ OR File No. 14774-20CA
Nonetheless, any process used to remove a passivation layer or an ILD will also remove any barrier material covering metal lines, while leaving the metal lines and any barrier material underlying them. When all material has been removed from that metal layer 20 (step 52), the process branches back to step 44.
After all metal layers have been exposed, etched away and imaged, any remaining interlayer dialectic is removed and the die is once again placed on the precision stage and images are acquired of a polycrystalline layer on which circuit components are formed (step 54). The tile images for each layer are stitched together in a manner well known in the art (step 56) to form image mosaics. The image mosaics are then vertically aligned, typically using via connections between layers to ensure correct inter-mosaic alignment (step 58). The aligned image mosaics are then passed to a feature extraction algorithm to reconstruct a parametric representation of the circuit die based on the aligned mosaic images (step 60). Circuit information is then extracted from the parametric representation (step 62), and it is determined whether logical errors exist in the circuit information (step 64). If so, a report with error exceptions is generated. The report including the error exceptions is passed to engineer analysts who must study the image mosaics and correct any missing or incorrect connections based on information retrieved from the mosaic images. If no errors were detected a report without error exceptions is generated (step 68) and the process ends.
Figs. 4a-4c illustrate the process described above with reference to Fig. 3 for an integrated circuit constructed using a copper damascene process. The OR File No. 14774-20CA
integrated circuit 10 shown in Fig. 4a includes an passivation layer 12 that covers metal lines 14 of metal layer N+1 . A via 2 6 interconnects the metal line 14 with the metal line 20 in the metal layer N. A barrier layer 16 segregates the metal line 14 from interlayer dielectric material 18. Barrier layer 16 is conductive and provides a connection between via 26 and metal line 20 of metal layer N. A barrier layer 22 separates metal line 20 from the interlayer dielectric 24 to ensure that no metal migrates into the interlayer dielectric, which would change its properties. As explained above, a barrier material (not shown) is applied over metal lines in some integrated circuit manufacturing processes.
Fig. 4b shows the integrated circuit die 10 after the passivation layer material 12 has been removed from the metal lines 14 of metal layer N+1. A wet or dry etching process is then used to etch away the metal lines 14 and the vias 26 leaving the barrier layer 16 shown in Fig. 4c.
The integrated circuit shown in Fig. 4c is then ready for imaging.
As will be appreciated by those skilled in the art, the methods in accordance with the invention produce images in which vias 26 are shown in conjunction with the metal lines 14 to which they are connected at a top end, which is opposite to the methods used in the prior art. The process can therefore by described as a "top down" process. As will further be appreciated by those skilled in the art, layout extraction algorithms may require adjustment to ensure proper layout extraction using mosaic images acquired using integrated circuit die preparation methods in accordance with the invention.

OR File No. 14774-20CA
Fig. 5 is a reproduction of an image of a copper/copper integrated circuit prepared for imaging using the process shown in Figs. 4a-4c. The image 80 is a scanning electron microscope image of an area of interest of the integrated circuit die. The barrier layers 82 that underlaid metal lines of the integrated circuit are light grey. The barrier layers that underlaid the vias 84 are dark grey or black, and are easily distinguishable from the barrier layers that underlaid the etched-away metal lines.
The vias are also well defined and there is no ambiguity about the metal line with which each via is associated.
Since the barrier layers that underlaid the vias are easily distinguished from the barrier layers that underlaid the metal lines, automated layout extraction is very efficient and completes with an extremely low error rate.
Fig. 4d shows the integrated circuit 10 prepared in accordance with the invention when the integrated circuit is constructed using aluminum lines 14 and tungsten vias 26. When that is the case, the etching processes shown in FIGS. 4a and 4b removes the aluminum lines but leaves the tungsten vias 26, as shown in Fig. 4d.
Fig. 6 is a reproduction of an image of an area of interest of an integrated circuit constructed with aluminum lines and tungsten vias prepared for imaging in accordance with the invention. The image 90 was acquired using a scanning electron microscope. The barrier layers 92 appear as light grey lines while the tungsten vias 94 appear as bright white spots. Once again, feature extractions software is readily able to distinguish between background, the barrier layers 92 and the vias 94. Feature extractions is therefore facilitated and automated layout extraction errors are significantly reduced.

OR File No. 14774-20CA
The invention therefore provides a less time consuming, simpler and more efficient method of preparing an integrated circuit die for imaging. The process provides images with better contrast and is particularly well adapted to use with integrated circuits manufactured using a copper damascene process, although it provides excellent results when used with any known integrated circuit construction.
The embodiments of the invention described above are intended to be exemplary only. The scope of the invention is therefore intended to be limited solely by the scope of the appended claims.

Claims (12)

I/WE CLAIM:
1. A method of imaging an integrated circuit die, comprising:

removing all material covering a metal layer of the integrated circuit die to expose the metal layer;
removing all metal from metal lines of the metal layer while preserving a barrier layer that underlies each metal line; and acquiring tile images of the barrier layer within an area of interest of the integrated circuit die;
wherein removing all metal from the metal lines further comprises removing all metal from vias descending downwards from the metal layer while preserving a barrier layer that surrounds each of the vias.
2. The method as claimed in claim 1 wherein removing all material covering the metal layer comprises etching away a passivation layer or an interlayer dielectric material using a dry etching process.
3. The method as claimed in claim 1 wherein removing all material from the metal layer comprises etching away a passivation layer or an interlayer dielectric material using a wet etching process.
4. The method as claimed in claim 1 wherein removing all material covering the metal layer comprises removing a passivation layer or an interlayer dielectric material using a chemical or mechanical polishing process.
5. The method as claimed in claim 1 wherein removing all metal from the metal lines comprises etching away the metal lines using a wet or a dry etching process.
6. The method as claimed in claim 1 wherein acquiring tile images comprises acquiring the tile images using a scanning electron microscope.
7. The method as claimed in claim 1 further comprising stitching together the tile images to form an image mosaic of the exposed barrier layer.
8. The method as claimed in claim 9 further comprising vertically aligning image mosaics of a plurality of exposed layers to form a three-dimensional model of the integrated circuit.
9. The method as claimed in claim 10 further comprising extracting features of the integrated circuit to reconstruct a parametric representation based on the aligned mosaic images.
10. The method as claimed in claim 11 further comprising extracting circuit information from the parametric representation.
11. The method as claimed in claim 12 further comprising preparing a report based on the circuit information.
12. A method for extracting circuit information from an integrated circuit die, comprising:

for each metal layer of the integrated circuit die:
removing all material covering the metal layer;

removing metal lines from the metal layer to expose a barrier layer underlying each metal line;

placing the integrated circuit die on a precision stage and acquiring tile images of the barrier layer in an area of interest of the integrated circuit die; and removing an interlayer dielectric material covering a polycrystalline silicon layer of the integrated circuit die, placing the integrated circuit die on the precision stage and acquiring tile images of the polycrystalline silicon layer;

wherein removing metal lines from the metal layer further comprises removing metal from vias descending downwards from the metal layer to expose a barrier layer surrounding each of the vias.
CA002521675A 2005-09-29 2005-09-29 Method of preparing an integrated circuit die for imaging Expired - Fee Related CA2521675C (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CA002521675A CA2521675C (en) 2005-09-29 2005-09-29 Method of preparing an integrated circuit die for imaging
PCT/CA2006/001590 WO2007036034A1 (en) 2005-09-29 2006-09-27 Method of preparing an integrated circuit die for imaging
CN2006800360250A CN101287994B (en) 2005-09-29 2006-09-27 Method of preparing an integrated circuit die for imaging

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CA002521675A CA2521675C (en) 2005-09-29 2005-09-29 Method of preparing an integrated circuit die for imaging

Publications (2)

Publication Number Publication Date
CA2521675A1 CA2521675A1 (en) 2007-03-29
CA2521675C true CA2521675C (en) 2009-11-24

Family

ID=37899318

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002521675A Expired - Fee Related CA2521675C (en) 2005-09-29 2005-09-29 Method of preparing an integrated circuit die for imaging

Country Status (3)

Country Link
CN (1) CN101287994B (en)
CA (1) CA2521675C (en)
WO (1) WO2007036034A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7498181B2 (en) * 2005-09-29 2009-03-03 Chipworks Inc. Method of preparing an integrated circuit die for imaging
US8394721B2 (en) * 2011-05-11 2013-03-12 Nanya Technology Corp. Method for obtaining a layout design for an existing integrated circuit
PL2764376T3 (en) * 2011-09-27 2017-03-31 Chipworks, Incorporated A method to differentiate p-channel or n-channel devices based on different etching rates.
CN111430219B (en) * 2019-06-27 2022-11-25 合肥晶合集成电路股份有限公司 Metal wire layer removing method and device defect detection method

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2247345B (en) * 1990-07-05 1995-04-05 Haroon Ahmed Integrated circuit structure analysis
US5694481A (en) * 1995-04-12 1997-12-02 Semiconductor Insights Inc. Automated design analysis system for generating circuit schematics from high magnification images of an integrated circuit
CA2260510A1 (en) * 1998-01-28 1999-07-28 Chipworks Focused ion beam imaging method
US6263098B1 (en) * 1998-09-11 2001-07-17 The United States Of America As Represented By The Secretary Of The Army Determination of functionality for integrated circuit modules
CA2358729C (en) * 2001-10-12 2008-07-08 Semiconductor Insights Inc. Computer aided method of circuit extraction
CN1494120A (en) * 2002-10-28 2004-05-05 华泰电子股份有限公司 Metal electroplating method of integrated circuit packaging substrate
US6803284B2 (en) * 2003-02-10 2004-10-12 Macronix International Co., Ltd. Method for manufacturing embedded non-volatile memory with two polysilicon layers

Also Published As

Publication number Publication date
WO2007036034A1 (en) 2007-04-05
CN101287994B (en) 2011-06-01
CA2521675A1 (en) 2007-03-29
CN101287994A (en) 2008-10-15

Similar Documents

Publication Publication Date Title
CN104078343B (en) Failure analysis method for gate oxide defect original appearance
CN104576433B (en) The method that defect is detected in diffused barrier layer
CA2521675C (en) Method of preparing an integrated circuit die for imaging
CA2260436C (en) Automated method of circuit analysis
DE102004027663B4 (en) Maskless array protection process sequence for forming via connections in random access magnetic memories
DE102005057076A1 (en) Increasing adhesion of metal layers comprises determination of regions of reduced contact hole density and formation of position-holding contacts with metal
CN101625302B (en) Method for preparing transmission electron microscope sample
US7498181B2 (en) Method of preparing an integrated circuit die for imaging
JPH044525B2 (en)
CN107112220A (en) Semiconductor devices, the method being used for producing the semiconductor devices, solid-state imaging element, image device and electronic installation
DE102018210539A1 (en) Interconnections with hybrid metallization
US7329550B2 (en) Method for analyzing the structure of deep trench capacitors and a preparation method thereof
EP0547906A1 (en) Method for forming contact vias in integrated circuits
DE102006004428B4 (en) Non-destructive Metal Detachment Monitoring Technology in Semiconductor Devices
US7402914B2 (en) Semiconductor device featuring overlay-mark used in photolithography process
Waite et al. Preparation, imaging, and design extraction of the front-end-of-line and middle-of-line in a 14 nm node finfet device
US6580072B1 (en) Method for performing failure analysis on copper metallization
JPH06101498B2 (en) Semiconductor device failure analysis method
CN110687138B (en) Method and device for measuring semiconductor structure and extracting boundary characteristic
CN109148315B (en) Method for distinguishing through hole connection between two metal layers in chip
JP4300795B2 (en) Semiconductor device and inspection method thereof
JP2699663B2 (en) Failure analysis method for semiconductor device
JP2007214399A (en) Alignment mark and its manufacturing method
DE19746642C2 (en) Method for producing a semiconductor component and its use in a chip card
DE102018124940B4 (en) CMOS sensors and methods for forming the same

Legal Events

Date Code Title Description
EEER Examination request
MKLA Lapsed

Effective date: 20220329

MKLA Lapsed

Effective date: 20200929