CA2451534A1 - Poudre d'adsorption a base de carbone contenant du chlorure cuivrique - Google Patents

Poudre d'adsorption a base de carbone contenant du chlorure cuivrique Download PDF

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Publication number
CA2451534A1
CA2451534A1 CA002451534A CA2451534A CA2451534A1 CA 2451534 A1 CA2451534 A1 CA 2451534A1 CA 002451534 A CA002451534 A CA 002451534A CA 2451534 A CA2451534 A CA 2451534A CA 2451534 A1 CA2451534 A1 CA 2451534A1
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CA
Canada
Prior art keywords
weight percent
carbon
powder
carbons
cupric chloride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002451534A
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English (en)
Inventor
Youssef El-Shoubary
Rudy Maes
Subash C. Seth
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Merck and Co Inc
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US09/408,361 external-priority patent/US6589318B2/en
Priority claimed from US09/902,293 external-priority patent/US6524371B2/en
Priority claimed from US09/902,285 external-priority patent/US6638347B2/en
Application filed by Individual filed Critical Individual
Publication of CA2451534A1 publication Critical patent/CA2451534A1/fr
Abandoned legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/64—Heavy metals or compounds thereof, e.g. mercury
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/68—Halogens or halogen compounds
    • B01D53/70—Organic halogen compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0222—Compounds of Mn, Re
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0233—Compounds of Cu, Ag, Au
    • B01J20/0237—Compounds of Cu
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0262—Compounds of O, S, Se, Te
    • B01J20/0266—Compounds of S
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0274—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04 characterised by the type of anion
    • B01J20/0288—Halides of compounds other than those provided for in B01J20/046
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/041—Oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/046—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing halogens, e.g. halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/102—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/20—Halogens or halogen compounds
    • B01D2257/206—Organic halogen compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/60—Heavy metals or heavy metal compounds
    • B01D2257/602—Mercury or mercury compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/42—Materials comprising a mixture of inorganic materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48—Sorbents characterised by the starting material used for their preparation
    • B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
    • B01J2220/4825—Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48—Sorbents characterised by the starting material used for their preparation
    • B01J2220/4875—Sorbents characterised by the starting material used for their preparation the starting material being a waste, residue or of undefined composition
    • B01J2220/4881—Residues from shells, e.g. eggshells, mollusk shells

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Treating Waste Gases (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

L'invention concerne une poudre d'adsorption à base de carbone contenant une quantité efficace de chlorure cuivrique. Cette poudre peut être utilisée pour éliminer du mercure d'un flux gazeux à haute humidité et à haute température, la quantité efficace de chlorure cuivrique étant comprise entre environ 1 et environ 45 % en poids. Des additifs supplémentaires, tels que le permanganate de potassium, l'hydroxyde de calcium, l'iodure de potassium et le soufre, peuvent être ajoutés à cette poudre pour améliorer l'élimination du mercure du flux gazeux.
CA002451534A 1999-09-29 2002-07-05 Poudre d'adsorption a base de carbone contenant du chlorure cuivrique Abandoned CA2451534A1 (fr)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US09/408,361 US6589318B2 (en) 1999-09-29 1999-09-29 Adsorption powder for removing mercury from high temperature, high moisture gas streams
US09/902,293 2001-07-10
US09/902,293 US6524371B2 (en) 1999-09-29 2001-07-10 Process for adsorption of mercury from gaseous streams
US09/902,285 US6638347B2 (en) 1999-09-29 2001-07-10 Carbon-based adsorption powder containing cupric chloride
US09/902,285 2001-07-10
PCT/US2002/021120 WO2003006140A1 (fr) 1999-09-29 2002-07-05 Poudre d'adsorption a base de carbone contenant du chlorure cuivrique

Publications (1)

Publication Number Publication Date
CA2451534A1 true CA2451534A1 (fr) 2003-01-23

Family

ID=40427833

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002451534A Abandoned CA2451534A1 (fr) 1999-09-29 2002-07-05 Poudre d'adsorption a base de carbone contenant du chlorure cuivrique

Country Status (4)

Country Link
EP (1) EP1406718A4 (fr)
JP (1) JP2004534641A (fr)
CA (1) CA2451534A1 (fr)
WO (1) WO2003006140A1 (fr)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6841513B2 (en) * 2001-03-29 2005-01-11 Merck & Co., Inc. Adsorption powder containing cupric chloride
US20080127631A1 (en) * 2006-11-30 2008-06-05 General Electric Company Method for removal of mercury from the emissions stream of a power plant and an apparatus for achieving the same
US20110137266A1 (en) * 2009-12-07 2011-06-09 Michael Schlitt Catheter
EP2697329A4 (fr) 2011-04-15 2015-05-27 Biogenic Reagents LLC Réactifs biogéniques à haute teneur en carbone et utilisations correspondantes
CN103958030B (zh) * 2011-11-28 2016-04-20 Ada碳解决方案有限责任公司 用于从烟道气中快速除汞的多官能组合物
CA3225246A1 (fr) * 2012-05-07 2013-11-14 Carbon Technology Holdings, LLC Charbon actif biogene et ses procedes de fabrication et d'utilisation
CN103056157A (zh) * 2013-01-25 2013-04-24 贵州省环境科学研究设计院 汞污染土壤的低温热解处理修复方法及装置
CN105467040B (zh) * 2015-12-30 2017-09-05 乌鲁木齐谱尼测试科技有限公司 土壤中对氨基苯甲醚和对硝基苯甲醚残留量的检测方法
CN107737581A (zh) * 2017-11-09 2018-02-27 东南大学 一种制备改性石油焦基脱汞吸附剂的方法
EP4217519A4 (fr) 2020-09-25 2024-09-11 Carbon Tech Holdings Llc Bioréduction de minerais métalliques intégrés à la pyrolyse de biomasse
US11851723B2 (en) 2021-02-18 2023-12-26 Carbon Technology Holdings, LLC Carbon-negative metallurgical products
EP4329955A1 (fr) 2021-04-27 2024-03-06 Carbon Technology Holdings, LLC Compositions de biocarbone à carbone fixe optimisé et leurs procédés de production
US20230020752A1 (en) 2021-07-09 2023-01-19 Carbon Technology Holdings, LLC Producing biocarbon pellets with high fixed-carbon content and optimized reactivity, and biocarbon pellets obtained therefrom

Family Cites Families (16)

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Publication number Priority date Publication date Assignee Title
US1984164A (en) * 1931-06-30 1934-12-11 Degea Ag Process and apparatus for purifying air vitiated with mercury vapors
US3193987A (en) * 1962-02-23 1965-07-13 Pittsburgh Activated Carbon Co Mercury vapor removal
US3194629A (en) * 1962-02-23 1965-07-13 Pittsburgh Activated Carbon Co Method of removing mercury vapor from gases
US3956458A (en) * 1973-11-16 1976-05-11 Paul Brent Anderson Method and apparatus for air purification
DE2656803C2 (de) * 1975-12-18 1986-12-18 Institut Français du Pétrole, Rueil-Malmaison, Hauts-de-Seine Verfahren zur Entfernung von in einem Gas oder in einer Flüssigkeit vorhandenem Quecksilber
DK158376C (da) * 1986-07-16 1990-10-08 Niro Atomizer As Fremgangsmaade til nedbringelse af indholdet af kviksoelvdamp og/eller dampe af skadelige organiske forbindelser og/eller nitrogenoxider i roeggas fra forbraendingsanlaeg
US5344626A (en) * 1992-06-26 1994-09-06 Minnesota Mining And Manufacturing Company Dual impregnated activated carbon
CA2114331C (fr) * 1993-06-10 2000-03-28 Bernard J. Lerner Elimination du mercure, du cadmium et de leurs composes presents dans les gaz de combustion
US5482915A (en) * 1993-09-20 1996-01-09 Air Products And Chemicals, Inc. Transition metal salt impregnated carbon
DE4344113A1 (de) * 1993-12-23 1995-06-29 Metallgesellschaft Ag Verfahren zur Reinigung von Abgasen der Abfallverbrennung
DE4403244A1 (de) * 1994-02-03 1995-08-10 Metallgesellschaft Ag Verfahren zur Reinigung von Verbrennungsabgasen
US6033461A (en) * 1998-01-02 2000-03-07 Gas Research Institute Selective nitrogen oxides adsorption from hot gas mixtures and thermal release by adsorbent
WO2001023072A1 (fr) * 1999-09-29 2001-04-05 Merck & Co., Inc. Poudre d'adsorption servant a extraire du mercure de flux gazeux possedant une temperature elevee et une teneur importante en humidite
US6533842B1 (en) * 2000-02-24 2003-03-18 Merck & Co., Inc. Adsorption powder for removing mercury from high temperature, high moisture gas streams
US6558642B2 (en) * 2001-03-29 2003-05-06 Merck & Co., Inc. Method of adsorbing metals and organic compounds from vaporous streams
US6841513B2 (en) * 2001-03-29 2005-01-11 Merck & Co., Inc. Adsorption powder containing cupric chloride

Also Published As

Publication number Publication date
EP1406718A4 (fr) 2005-10-19
JP2004534641A (ja) 2004-11-18
WO2003006140A1 (fr) 2003-01-23
EP1406718A1 (fr) 2004-04-14

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FZDE Discontinued