CA2424226A1 - An improved optical device having continuous and disperse phases - Google Patents
An improved optical device having continuous and disperse phases Download PDFInfo
- Publication number
- CA2424226A1 CA2424226A1 CA002424226A CA2424226A CA2424226A1 CA 2424226 A1 CA2424226 A1 CA 2424226A1 CA 002424226 A CA002424226 A CA 002424226A CA 2424226 A CA2424226 A CA 2424226A CA 2424226 A1 CA2424226 A1 CA 2424226A1
- Authority
- CA
- Canada
- Prior art keywords
- optical body
- copolymer
- degree
- randomness
- homopolymers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 230000003287 optical effect Effects 0.000 title claims description 96
- 239000000203 mixture Substances 0.000 claims abstract description 37
- 229920001519 homopolymer Polymers 0.000 claims abstract description 33
- 229920005604 random copolymer Polymers 0.000 claims abstract description 24
- 238000005809 transesterification reaction Methods 0.000 claims abstract description 16
- 229920001577 copolymer Polymers 0.000 claims description 58
- 239000000178 monomer Substances 0.000 claims description 40
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 31
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 30
- 238000006243 chemical reaction Methods 0.000 claims description 20
- 229920000642 polymer Polymers 0.000 claims description 18
- -1 polyethylene terephthalate Polymers 0.000 claims description 10
- 239000011112 polyethylene naphthalate Substances 0.000 claims description 8
- 229920003207 poly(ethylene-2,6-naphthalate) Polymers 0.000 claims description 6
- 230000001747 exhibiting effect Effects 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 47
- 239000010408 film Substances 0.000 abstract description 45
- 239000012788 optical film Substances 0.000 abstract description 10
- 239000000463 material Substances 0.000 description 28
- 229920001400 block copolymer Polymers 0.000 description 18
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 17
- 230000008569 process Effects 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 14
- 238000005482 strain hardening Methods 0.000 description 14
- 230000001965 increasing effect Effects 0.000 description 13
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 9
- 229920000728 polyester Polymers 0.000 description 9
- 239000007787 solid Substances 0.000 description 9
- 238000006116 polymerization reaction Methods 0.000 description 8
- 238000002844 melting Methods 0.000 description 6
- 230000008018 melting Effects 0.000 description 6
- 230000000704 physical effect Effects 0.000 description 6
- 238000001125 extrusion Methods 0.000 description 4
- 239000000155 melt Substances 0.000 description 4
- 125000005487 naphthalate group Chemical group 0.000 description 4
- KYTZHLUVELPASH-UHFFFAOYSA-N naphthalene-1,2-dicarboxylic acid Chemical compound C1=CC=CC2=C(C(O)=O)C(C(=O)O)=CC=C21 KYTZHLUVELPASH-UHFFFAOYSA-N 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 230000010287 polarization Effects 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920010524 Syndiotactic polystyrene Polymers 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 230000009477 glass transition Effects 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000008188 pellet Substances 0.000 description 3
- 229920001225 polyester resin Polymers 0.000 description 3
- 239000004645 polyester resin Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000005481 NMR spectroscopy Methods 0.000 description 2
- 229920001283 Polyalkylene terephthalate Polymers 0.000 description 2
- 239000004952 Polyamide Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000000113 differential scanning calorimetry Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000004927 fusion Effects 0.000 description 2
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- RXOHFPCZGPKIRD-UHFFFAOYSA-L naphthalene-2,6-dicarboxylate Chemical compound C1=C(C([O-])=O)C=CC2=CC(C(=O)[O-])=CC=C21 RXOHFPCZGPKIRD-UHFFFAOYSA-L 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
- 229920001281 polyalkylene Polymers 0.000 description 2
- 229920002647 polyamide Polymers 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000000135 prohibitive effect Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 1
- 229920001634 Copolyester Polymers 0.000 description 1
- 239000004705 High-molecular-weight polyethylene Substances 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 239000004983 Polymer Dispersed Liquid Crystal Substances 0.000 description 1
- 238000012300 Sequence Analysis Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 229920000359 diblock copolymer Polymers 0.000 description 1
- 229940117389 dichlorobenzene Drugs 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- BTVWZWFKMIUSGS-UHFFFAOYSA-N dimethylethyleneglycol Natural products CC(C)(O)CO BTVWZWFKMIUSGS-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000009998 heat setting Methods 0.000 description 1
- 229920006158 high molecular weight polymer Polymers 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000010128 melt processing Methods 0.000 description 1
- 125000001434 methanylylidene group Chemical group [H]C#[*] 0.000 description 1
- RXOHFPCZGPKIRD-UHFFFAOYSA-N naphthalene-2,6-dicarboxylic acid Chemical compound C1=C(C(O)=O)C=CC2=CC(C(=O)O)=CC=C21 RXOHFPCZGPKIRD-UHFFFAOYSA-N 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 description 1
- 239000004038 photonic crystal Substances 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000001338 self-assembly Methods 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/30—Polarising elements
- G02B5/3025—Polarisers, i.e. arrangements capable of producing a definite output polarisation state from an unpolarised input state
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Polarising Elements (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Polyesters Or Polycarbonates (AREA)
- Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/686,460 US6654170B1 (en) | 1999-10-12 | 2000-10-11 | Optical device having continuous and disperse phases |
| US09/686,460 | 2000-10-11 | ||
| PCT/US2001/021355 WO2002031539A2 (en) | 2000-10-11 | 2001-07-02 | An improved optical device having continuous and disperse phases |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2424226A1 true CA2424226A1 (en) | 2002-04-18 |
Family
ID=24756380
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002424226A Abandoned CA2424226A1 (en) | 2000-10-11 | 2001-07-02 | An improved optical device having continuous and disperse phases |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6654170B1 (enExample) |
| EP (1) | EP1327164A2 (enExample) |
| JP (1) | JP2004518991A (enExample) |
| KR (1) | KR100808704B1 (enExample) |
| CN (1) | CN100350276C (enExample) |
| AU (1) | AU2001278869A1 (enExample) |
| CA (1) | CA2424226A1 (enExample) |
| MX (1) | MXPA03003100A (enExample) |
| WO (1) | WO2002031539A2 (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6939499B2 (en) * | 2001-05-31 | 2005-09-06 | 3M Innovative Properties Company | Processes and apparatus for making transversely drawn films with substantially uniaxial character |
| US7329465B2 (en) | 2004-10-29 | 2008-02-12 | 3M Innovative Properties Company | Optical films incorporating cyclic olefin copolymers |
| US9709700B2 (en) | 2005-04-06 | 2017-07-18 | 3M Innovative Properties Company | Optical bodies including rough strippable boundary layers |
| WO2006107970A2 (en) * | 2005-04-06 | 2006-10-12 | 3M Innovative Properties Company | Diffuse reflective polariziing films with orientable polymer blends |
| WO2006107969A1 (en) | 2005-04-06 | 2006-10-12 | 3M Innovative Properties Company | Optical bodies including rough strippable boundary layers and asymmetric surface structures |
| US20060227421A1 (en) | 2005-04-06 | 2006-10-12 | Stover Carl A | Optical bodies including strippable boundary layers |
| KR101287740B1 (ko) | 2005-04-08 | 2013-07-18 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 광학 필름의 열 경화법 |
| US7583440B2 (en) * | 2006-06-05 | 2009-09-01 | Skc Haas Display Films Co., Ltd. | Diffusely-reflecting polarizer having nearly isotropic continuous phase |
| KR100809849B1 (ko) * | 2006-11-10 | 2008-03-04 | 엘지.필립스 엘시디 주식회사 | 광학 필름 및 이의 제조 방법, 그리고 액정 표시 장치 |
| KR101361866B1 (ko) * | 2006-11-10 | 2014-02-12 | 엘지디스플레이 주식회사 | 광학 필름 및 이의 제조 방법, 그리고 액정 표시 장치 |
| KR101279303B1 (ko) * | 2006-11-10 | 2013-07-05 | 엘지디스플레이 주식회사 | 광학 필름 및 이의 제조 방법, 그리고 액정 표시 장치 |
| KR200453893Y1 (ko) * | 2009-04-28 | 2011-06-01 | (주)상문 | 슬림형 슬라이딩 화장품 용기 |
Family Cites Families (65)
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| US3124639A (en) | 1964-03-10 | figure | ||
| US540768A (en) | 1895-06-11 | Richard walsingham western | ||
| US2604817A (en) | 1948-10-14 | 1952-07-29 | Du Pont | Light polarizing composition |
| US3213753A (en) | 1962-01-24 | 1965-10-26 | Polaroid Corp | Multilayer lenticular light polarizing device |
| US3546320A (en) | 1968-03-25 | 1970-12-08 | Sun Oil Co | Polyalkylene terephthalate molding composition |
| US3610729A (en) | 1969-06-18 | 1971-10-05 | Polaroid Corp | Multilayered light polarizer |
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| JPS5414320B2 (enExample) | 1972-07-25 | 1979-06-06 | ||
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| US4525413A (en) | 1981-03-02 | 1985-06-25 | Polaroid Corporation | Optical device including birefringent polymer |
| US4521588A (en) | 1981-03-02 | 1985-06-04 | Polaroid Corporation | Optical device including birefringent polyhydrazide polymer |
| US4520189A (en) | 1981-03-02 | 1985-05-28 | Polaroid Corporation | Optical device including birefringent aromatic amino carboxylic acid polymer |
| US4617373A (en) | 1985-02-15 | 1986-10-14 | Eastman Kodak Company | Condensation polymers and products therefrom |
| US4720426A (en) | 1986-06-30 | 1988-01-19 | General Electric Company | Reflective coating for solid-state scintillator bar |
| US5211878A (en) | 1988-03-10 | 1993-05-18 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Difluorobenzonitrile derivatives |
| US5486949A (en) | 1989-06-20 | 1996-01-23 | The Dow Chemical Company | Birefringent interference polarizer |
| US5235443A (en) | 1989-07-10 | 1993-08-10 | Hoffmann-La Roche Inc. | Polarizer device |
| WO1991006889A1 (de) | 1989-11-01 | 1991-05-16 | F.Hoffmann-La Roche Ag | Lichtsteuereinrichtungen mit flüssigkristallen |
| NL9000808A (nl) | 1990-04-06 | 1991-11-01 | Koninkl Philips Electronics Nv | Vloeibaar kristallijn materiaal en beeldweergeefcel die dit materiaal bevat. |
| ES2091333T3 (es) | 1990-07-30 | 1996-11-01 | Eastman Chem Co | Mezclas de poli(tereftalato de etileno) y poli(naftalenodicarboxilato de etileno) que contienen un estabilizante que contiene fosforo. |
| US5217794A (en) | 1991-01-22 | 1993-06-08 | The Dow Chemical Company | Lamellar polymeric body |
| US5294657A (en) | 1992-05-15 | 1994-03-15 | Melendy Peter S | Adhesive composition with decorative glitter |
| DE4326521B4 (de) | 1992-08-10 | 2005-12-22 | Bridgestone Corp. | Lichtstreuendes Material und Verfahren zu seiner Herstellung |
| US5269995A (en) | 1992-10-02 | 1993-12-14 | The Dow Chemical Company | Coextrusion of multilayer articles using protective boundary layers and apparatus therefor |
| AU5322594A (en) | 1992-10-29 | 1994-05-24 | Dow Chemical Company, The | Formable reflective multilayer body |
| EP0606939B1 (en) | 1993-01-11 | 1998-05-06 | Koninklijke Philips Electronics N.V. | Illumination system and display device including such a system |
| TW289095B (enExample) | 1993-01-11 | 1996-10-21 | ||
| US5389324A (en) | 1993-06-07 | 1995-02-14 | The Dow Chemical Company | Layer thickness gradient control in multilayer polymeric bodies |
| US5486935A (en) | 1993-06-29 | 1996-01-23 | Kaiser Aerospace And Electronics Corporation | High efficiency chiral nematic liquid crystal rear polarizer for liquid crystal displays having a notch polarization bandwidth of 100 nm to 250 nm |
| JP3358850B2 (ja) | 1993-08-17 | 2002-12-24 | 住友化学工業株式会社 | 長繊維強化熱可塑性樹脂組成物の製造装置、その製造方法及びその製造用被覆ダイ |
| CA2179625C (en) | 1993-12-21 | 2004-10-26 | Andrew J. Ouderkirk | Optical polarizer |
| EP0962806B1 (en) | 1993-12-21 | 2008-12-03 | Minnesota Mining And Manufacturing Company | Multilayered optical film |
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| AU1434795A (en) | 1993-12-21 | 1995-07-10 | Minnesota Mining And Manufacturing Company | Reflective polarizer display |
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| US5686979A (en) | 1995-06-26 | 1997-11-11 | Minnesota Mining And Manufacturing Company | Optical panel capable of switching between reflective and transmissive states |
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| US5767935A (en) | 1995-08-31 | 1998-06-16 | Sumitomo Chemical Company, Limited | Light control sheet and liquid crystal display device comprising the same |
| US5783120A (en) | 1996-02-29 | 1998-07-21 | Minnesota Mining And Manufacturing Company | Method for making an optical film |
| US5825543A (en) * | 1996-02-29 | 1998-10-20 | Minnesota Mining And Manufacturing Company | Diffusely reflecting polarizing element including a first birefringent phase and a second phase |
| US5867316A (en) | 1996-02-29 | 1999-02-02 | Minnesota Mining And Manufacturing Company | Multilayer film having a continuous and disperse phase |
| EP0835476B1 (en) | 1996-04-26 | 2004-11-03 | Koninklijke Philips Electronics N.V. | Optical system |
| US5808794A (en) | 1996-07-31 | 1998-09-15 | Weber; Michael F. | Reflective polarizers having extended red band edge for controlled off axis color |
| US5976424A (en) | 1996-07-31 | 1999-11-02 | Minnesota Mining And Manufacturing Company | Method for making multilayer optical films having thin optical layers |
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| KR100601228B1 (ko) | 1998-01-13 | 2006-07-19 | 미네소타 마이닝 앤드 매뉴팩춰링 캄파니 | 다층 광학 필름의 제조 방법 |
| US6256146B1 (en) | 1998-07-31 | 2001-07-03 | 3M Innovative Properties | Post-forming continuous/disperse phase optical bodies |
| US6005713A (en) | 1998-08-21 | 1999-12-21 | 3M Innovative Properties Company | Multilayer polarizer having a continuous and disperse phase |
| AU2515200A (en) | 1999-09-20 | 2001-04-24 | 3M Innovative Properties Company | Optical films having at least one particle-containing layer |
-
2000
- 2000-10-11 US US09/686,460 patent/US6654170B1/en not_active Expired - Lifetime
-
2001
- 2001-07-02 JP JP2002534871A patent/JP2004518991A/ja active Pending
- 2001-07-02 EP EP01957093A patent/EP1327164A2/en not_active Withdrawn
- 2001-07-02 CA CA002424226A patent/CA2424226A1/en not_active Abandoned
- 2001-07-02 WO PCT/US2001/021355 patent/WO2002031539A2/en not_active Ceased
- 2001-07-02 MX MXPA03003100A patent/MXPA03003100A/es active IP Right Grant
- 2001-07-02 AU AU2001278869A patent/AU2001278869A1/en not_active Abandoned
- 2001-07-02 KR KR1020037005053A patent/KR100808704B1/ko not_active Expired - Fee Related
- 2001-07-02 CN CNB01817132XA patent/CN100350276C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| WO2002031539A2 (en) | 2002-04-18 |
| KR100808704B1 (ko) | 2008-02-29 |
| KR20030038810A (ko) | 2003-05-16 |
| WO2002031539A3 (en) | 2002-10-31 |
| AU2001278869A1 (en) | 2002-04-22 |
| JP2004518991A (ja) | 2004-06-24 |
| MXPA03003100A (es) | 2004-05-04 |
| EP1327164A2 (en) | 2003-07-16 |
| CN1468381A (zh) | 2004-01-14 |
| CN100350276C (zh) | 2007-11-21 |
| US6654170B1 (en) | 2003-11-25 |
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