CA2359337C - Procede de separation de sucres - Google Patents

Procede de separation de sucres Download PDF

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Publication number
CA2359337C
CA2359337C CA002359337A CA2359337A CA2359337C CA 2359337 C CA2359337 C CA 2359337C CA 002359337 A CA002359337 A CA 002359337A CA 2359337 A CA2359337 A CA 2359337A CA 2359337 C CA2359337 C CA 2359337C
Authority
CA
Canada
Prior art keywords
liquor
carbohydrate
hydrogenated
hydrolysate
resin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA002359337A
Other languages
English (en)
Other versions
CA2359337A1 (fr
Inventor
Michael Saska
Feng Chen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Louisiana State University and Agricultural and Mechanical College
Original Assignee
Louisiana State University and Agricultural and Mechanical College
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Louisiana State University and Agricultural and Mechanical College filed Critical Louisiana State University and Agricultural and Mechanical College
Publication of CA2359337A1 publication Critical patent/CA2359337A1/fr
Application granted granted Critical
Publication of CA2359337C publication Critical patent/CA2359337C/fr
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/14—Purification of sugar juices using ion-exchange materials
    • C13B20/146—Purification of sugar juices using ion-exchange materials using only anionic ion-exchange material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterized by the components to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04—Processes using organic exchangers
    • B01J41/05—Processes using organic exchangers in the strongly basic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/20—Anion exchangers for chromatographic processes
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K13/00—Sugars not otherwise provided for in this class
    • C13K13/002—Xylose
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2215/00—Separating processes involving the treatment of liquids with adsorbents
    • B01D2215/02—Separating processes involving the treatment of liquids with adsorbents with moving adsorbents
    • B01D2215/023—Simulated moving beds
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/8813—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample biological materials
    • G01N2030/8836—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample biological materials involving saccharides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Sustainable Development (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

L'invention concerne des séparations améliorées de xylose, mannose, galactose, arabinose, glucose, xylitol, arabitol, sorbitol, galactitol, ou mannitol (ainsi que d'autres monosaccharides et alcools de sucre) d'autres sucres et alcools de sucres. Lesdites séparations peuvent être réalisées par chromatographie sur des surfaces échangeuses d'anions sous forme hydroxyle préparées à partir de résines échangeuses anioniques à des teneurs hydroxyle relativement faibles. Lorsqu'une résine échangeuse anionique à forte base, telle qu'une résine échangeuse anionique à forte base sous forme de chlorure, est conditionnée avec une faible teneur en hydroxyle (par exemple une solution NaOH avec une teneur se situant entre 0,1 et 1000 mM, de préférence entre 1 et 10 mM), ladite résine permet de séparer, les uns des autres, un certain nombre de sucres et d'alcools de sucres, avec désorption rapide à partir de la résine.
CA002359337A 1999-01-14 1999-12-22 Procede de separation de sucres Expired - Fee Related CA2359337C (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US23119399A 1999-01-14 1999-01-14
US09/231,193 1999-01-14
PCT/US1999/030877 WO2000042225A1 (fr) 1999-01-14 1999-12-22 Procede de separation de sucres

Publications (2)

Publication Number Publication Date
CA2359337A1 CA2359337A1 (fr) 2000-07-20
CA2359337C true CA2359337C (fr) 2005-09-13

Family

ID=22868132

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002359337A Expired - Fee Related CA2359337C (fr) 1999-01-14 1999-12-22 Procede de separation de sucres

Country Status (3)

Country Link
AU (1) AU2387200A (fr)
CA (1) CA2359337C (fr)
WO (1) WO2000042225A1 (fr)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040173533A1 (en) * 2001-07-24 2004-09-09 Farone William A. Separation of xylose and glucose
US6773512B2 (en) 2001-12-31 2004-08-10 Danisco Sweeteners Oy Method for the recovery of sugars
FI20020592A (fi) 2002-03-27 2003-09-28 Danisco Sweeteners Oy Menetelmä sokereiden, sokerialkoholien, hiilihydraattien ja niiden seosten erottamiseksi niitä sisältävistä liuoksista
FI20030963A0 (fi) 2003-06-27 2003-06-27 Danisco Sweeteners Oy Erotusmenetelmä
US20050033045A1 (en) 2003-06-27 2005-02-10 Danisco Sweeteners Oy Separation method
BR112014021163A2 (pt) 2012-02-27 2020-10-27 Del Mar Pharmaceuticals métodos analíticos aprimorados para analisar e determinar impurezas em dianidrogalactitol
US20140275518A1 (en) * 2013-03-14 2014-09-18 Orochem Technologies, Inc. L-glucose production from l-glusose/l-mannose mixtures using simulated moving bed separation
AU2014348232A1 (en) * 2013-11-18 2016-06-30 Del Mar Pharmaceuticals HPLC analysis of impurities in dianhydrogalactitol
JP6732017B2 (ja) 2015-07-24 2020-07-29 アニッキ ゲーエムベーハーＡｎｎｉｋｋｉ Ｇｍｂｈ 糖混合物から酸化生成物および還元生成物を得るための方法
EP3416740B1 (fr) 2016-02-19 2021-01-06 Intercontinental Great Brands LLC Procédé de création de flux de valeurs multiples à partir de sources de biomasse
FR3097855B1 (fr) * 2019-06-28 2021-07-23 Ifp Energies Now Séparation en phase liquide des sucres de deuxième génération par adsorption sur zéolithe de type FAU de ratio atomique Si/Al inférieur à 1,5

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5420578B1 (fr) * 1970-12-09 1979-07-24
US5084104A (en) * 1989-12-05 1992-01-28 Cultor, Ltd. Method for recovering xylose
EP0481603A1 (fr) * 1990-10-15 1992-04-22 The Dow Chemical Company Séparation d'acides organiques faibles de mélanges de liquides
US5482631A (en) * 1994-10-06 1996-01-09 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Separation of inositols from sugars and sugar alcohols

Also Published As

Publication number Publication date
WO2000042225A9 (fr) 2001-09-13
WO2000042225A1 (fr) 2000-07-20
CA2359337A1 (fr) 2000-07-20
AU2387200A (en) 2000-08-01

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Effective date: 20101222