CA2215748A1 - Freeze-drying process and apparatus - Google Patents
Freeze-drying process and apparatusInfo
- Publication number
- CA2215748A1 CA2215748A1 CA002215748A CA2215748A CA2215748A1 CA 2215748 A1 CA2215748 A1 CA 2215748A1 CA 002215748 A CA002215748 A CA 002215748A CA 2215748 A CA2215748 A CA 2215748A CA 2215748 A1 CA2215748 A1 CA 2215748A1
- Authority
- CA
- Canada
- Prior art keywords
- freeze
- shell
- drying process
- vial
- frozen material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004108 freeze drying Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 238000007710 freezing Methods 0.000 abstract 2
- 230000008014 freezing Effects 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
- F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
- F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
Landscapes
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Drying Of Solid Materials (AREA)
Abstract
A freeze-drying process includes a freezing step of rotating the vial (1) about its longitudinal axis at a speed not less than that required to maintain by centrifugal force the aqueous material to be freeze-dried in the form of a shell (7) on the inner walls of the vial (1) and then subjecting the material to freezing conditions to freeze it in the form of said shell (7). In another aspect of the invention, the freeze-drying process also includes the step of drying the shell frozen material (7), by directing heat radially inwards from a heating block (14) to the shell frozen material (7) and increasing the temperature over a time period to dry the shell frozen material (7).
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB9505523.2A GB9505523D0 (en) | 1995-03-18 | 1995-03-18 | Lyophilization process |
GB9505523.2 | 1995-03-18 | ||
PCT/GB1996/000597 WO1996029556A1 (en) | 1995-03-18 | 1996-03-14 | Freeze-drying process and apparatus |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2215748A1 true CA2215748A1 (en) | 1996-09-26 |
CA2215748C CA2215748C (en) | 2007-08-14 |
Family
ID=38434449
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002215748A Expired - Fee Related CA2215748C (en) | 1995-03-18 | 1996-03-14 | Freeze-drying process and apparatus |
Country Status (1)
Country | Link |
---|---|
CA (1) | CA2215748C (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3714226A4 (en) * | 2017-11-22 | 2021-03-03 | IMA Life North America Inc. | Spray freeze drying on a substrate |
-
1996
- 1996-03-14 CA CA002215748A patent/CA2215748C/en not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3714226A4 (en) * | 2017-11-22 | 2021-03-03 | IMA Life North America Inc. | Spray freeze drying on a substrate |
Also Published As
Publication number | Publication date |
---|---|
CA2215748C (en) | 2007-08-14 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request | ||
MKLA | Lapsed |
Effective date: 20150316 |