CA2095351A1 - Shaped solid made with a rigid, interlocking mesh of neutralized carboxylic acid - Google Patents

Shaped solid made with a rigid, interlocking mesh of neutralized carboxylic acid

Info

Publication number
CA2095351A1
CA2095351A1 CA2095351A CA2095351A CA2095351A1 CA 2095351 A1 CA2095351 A1 CA 2095351A1 CA 2095351 A CA2095351 A CA 2095351A CA 2095351 A CA2095351 A CA 2095351A CA 2095351 A1 CA2095351 A1 CA 2095351A1
Authority
CA
Canada
Prior art keywords
carboxylic acid
rigid
interlocking mesh
shaped solid
neutralized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2095351A
Other languages
French (fr)
Other versions
CA2095351C (en
Inventor
Mark L. Kacher
James E. Taneri
James B. Camden
Paul E. Vest
Sylvia J. Bowles
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US07/782,956 external-priority patent/US5340492A/en
Application filed by Individual filed Critical Individual
Publication of CA2095351A1 publication Critical patent/CA2095351A1/en
Application granted granted Critical
Publication of CA2095351C publication Critical patent/CA2095351C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00—Compositions of detergents, not provided for by one single preceding group
    • C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/04—Carboxylic acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/04—Carboxylic acids or salts thereof
    • C11D1/08—Polycarboxylic acids containing no nitrogen or sulfur
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00—Compositions of detergents, not provided for by one single preceding group
    • C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00—Compositions of detergents, not provided for by one single preceding group
    • C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/006—Detergents in the form of bars or tablets containing mainly surfactants, but no builders, e.g. syndet bar
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0069—Laundry bars
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/04—Carboxylic acids or salts thereof
    • C11D1/10—Amino carboxylic acids; Imino carboxylic acids; Fatty acid condensates thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/123—Sulfonic acids or sulfuric acid esters; Salts thereof derived from carboxylic acids, e.g. sulfosuccinates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/126—Acylisethionates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/16—Sulfonic acids or sulfuric acid esters; Salts thereof derived from divalent or polyvalent alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29—Sulfates of polyoxyalkylene ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/32—Protein hydrolysates; Fatty acid condensates thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/34—Derivatives of acids of phosphorus
    • C11D1/345—Phosphates or phosphites
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/662—Carbohydrates or derivatives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/75—Amino oxides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/90—Betaines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/92—Sulfobetaines ; Sulfitobetaines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Materials For Medical Uses (AREA)
  • Catalysts (AREA)

Abstract

The invention provides a shaped solid, three-dimensional skeleton structure comprising: a relatively rigid, interlocking mesh of neutralized crystalline carboxylic acid. In another respect, the present invention provides an improved cleansing bar which is comprised of the rigid, interlocking mesh of neutralized carboxylic acid, preferably sodium soap fibers. Such preferred cleansing bars can be formulated to have essentially no bar smear. Some cleansing bars comprise surprisingly large amounts of water and another liquids while maintaining their rigidity and excellent smear properties; even when allowed to soak overnight in water.
CA002095351A 1990-11-26 1991-11-20 Shaped solid made with a rigid, interlocking mesh of neutralized carboxylic acid Expired - Fee Related CA2095351C (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US61782790A 1990-11-26 1990-11-26
US617,827 1990-11-26
US07/782,956 US5340492A (en) 1990-11-26 1991-11-01 Shaped solid made with a rigid, interlocking mesh of neutralized carboxylic acid
US782,956 1991-11-01

Publications (2)

Publication Number Publication Date
CA2095351A1 true CA2095351A1 (en) 1992-05-27
CA2095351C CA2095351C (en) 1998-12-15

Family

ID=27088104

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002095351A Expired - Fee Related CA2095351C (en) 1990-11-26 1991-11-20 Shaped solid made with a rigid, interlocking mesh of neutralized carboxylic acid

Country Status (27)

Country Link
EP (1) EP0559837B1 (en)
JP (1) JPH06503122A (en)
KR (1) KR100226393B1 (en)
CN (1) CN1036529C (en)
AR (1) AR247426A1 (en)
AT (1) ATE129522T1 (en)
AU (1) AU657295B2 (en)
BR (1) BR9107125A (en)
CA (1) CA2095351C (en)
CZ (1) CZ283495B6 (en)
DE (1) DE69114143T2 (en)
DK (1) DK0559837T3 (en)
EG (1) EG19580A (en)
ES (1) ES2079180T3 (en)
FI (1) FI932366L (en)
GR (1) GR3017892T3 (en)
HU (1) HU215484B (en)
IE (1) IE72087B1 (en)
MA (1) MA22349A1 (en)
MX (1) MX9102229A (en)
NO (1) NO931848L (en)
NZ (1) NZ240709A (en)
PT (1) PT99606A (en)
RU (1) RU2080365C1 (en)
SG (1) SG59939A1 (en)
SK (1) SK52693A3 (en)
WO (1) WO1992009679A1 (en)

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US5262079A (en) * 1992-03-20 1993-11-16 The Procter & Gamble Company Framed neutral pH cleansing bar
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CA2147674C (en) * 1994-05-16 1999-03-30 David Robert Zint Shaped semi-solid or solid dishwashing detergent
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WO1998027193A1 (en) * 1996-12-16 1998-06-25 The Procter & Gamble Company Personal cleansing bar composition containing sodium lauroyl lactylate
US6680285B2 (en) * 2000-12-21 2004-01-20 Unilever Home & Personal Care Usa A Division Of Conopco, Inc. Skin cleansing bar with high levels of liquid emollient
US6630432B2 (en) * 2001-04-18 2003-10-07 Unilever Home & Personal Care Usa, Division Of Conopco Processable soap based bars comprising soaps of α hydroxy acid and minimum amount of free fatty acid and/or monoglyceride
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AU2003227048A1 (en) * 2002-04-02 2003-10-13 Unilever N.V. Detergent bar compositions
US6664217B1 (en) * 2002-07-18 2003-12-16 Unilever Home & Personal Care, Usa Division Of Conopco, Inc. Toilet bar having simultaneous exfoliating and moisturizing properties
WO2004029058A1 (en) * 2002-09-25 2004-04-08 Sankyo Company, Limited Medicinal composition for inhibiting increase in blood gastrin concentration
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US7045491B2 (en) * 2003-10-28 2006-05-16 Colgate-Palmolive Company Bar soap composition with reduced bar wear properties
JP5367494B2 (en) * 2009-08-06 2013-12-11 花王株式会社 Manufacturing method of frame kneaded soap
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CN107245391A (en) * 2016-12-25 2017-10-13 池州市建东生物科技有限公司 A kind of special soap of skin disease
JP7485605B2 (en) 2018-01-26 2024-05-16 エコラボ ユーエスエー インコーポレイティド Solidification of liquid amine oxide, betaine, and/or sultaine surfactants with a carrier
CN111655830A (en) 2018-01-26 2020-09-11 埃科莱布美国股份有限公司 Curing Liquid Anionic Surfactants
CN111655829A (en) 2018-01-26 2020-09-11 埃科莱布美国股份有限公司 Curing Liquid Amine Oxide, Betaine and/or Sultaine Surfactants with Binder and Optional Carrier
CN115297819A (en) 2020-04-10 2022-11-04 宝洁公司 Rheological solid composition
US12122979B2 (en) 2020-04-10 2024-10-22 The Procter & Gamble Company Cleaning article with preferential rheological solid composition
WO2021207439A1 (en) 2020-04-10 2021-10-14 The Procter & Gamble Company Rheological solid composition
WO2021216288A1 (en) 2020-04-10 2021-10-28 The Procter & Gamble Company Cleaning implement with a rheological solid composition
WO2021207442A1 (en) 2020-04-10 2021-10-14 The Procter & Gamble Company Rheological solid oral composition
WO2021207438A1 (en) * 2020-04-10 2021-10-14 The Procter & Gamble Company Oral care product comprising a rheological solid composition
US11833237B2 (en) 2021-03-09 2023-12-05 The Procter & Gamble Company Method for enhancing scalp active deposition
EP4098243A1 (en) * 2021-05-31 2022-12-07 BIC Violex Single Member S.A. Solid shaving aid composition
CN118043442A (en) * 2022-08-12 2024-05-14 宝洁公司 Solid soluble compositions
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WO2024036123A1 (en) * 2022-08-12 2024-02-15 The Procter & Gamble Company Low-water compositions
WO2024036117A1 (en) * 2022-08-12 2024-02-15 The Procter & Gamble Company Low-water compositions
CA3235282A1 (en) * 2022-08-12 2024-02-15 Matthew Lawrence Lynch Solid dissolvable compositions
CA3236012A1 (en) * 2022-08-12 2024-02-15 Matthew Lawrence Lynch Solid dissolvable compositions

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US4758370A (en) * 1987-04-30 1988-07-19 Neutrogena Corp. Compositions and processes for the continuous production of transparent soap
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Also Published As

Publication number Publication date
HUT76489A (en) 1997-09-29
DK0559837T3 (en) 1996-03-04
SG59939A1 (en) 1999-02-22
RU2080365C1 (en) 1997-05-27
AU657295B2 (en) 1995-03-09
MX9102229A (en) 1992-07-08
CN1062759A (en) 1992-07-15
NZ240709A (en) 1995-04-27
FI932366A7 (en) 1993-05-25
HU215484B (en) 1999-01-28
FI932366A0 (en) 1993-05-25
EG19580A (en) 1995-08-30
FI932366L (en) 1993-05-25
CA2095351C (en) 1998-12-15
CZ98793A3 (en) 1994-07-13
HU9301532D0 (en) 1993-09-28
WO1992009679A1 (en) 1992-06-11
NO931848D0 (en) 1993-05-21
HK1006179A1 (en) 1999-02-12
BR9107125A (en) 1993-11-09
EP0559837B1 (en) 1995-10-25
DE69114143D1 (en) 1995-11-30
NO931848L (en) 1993-07-23
GR3017892T3 (en) 1996-01-31
EP0559837A1 (en) 1993-09-15
AR247426A1 (en) 1994-12-29
CN1036529C (en) 1997-11-26
AU9176391A (en) 1992-06-25
JPH06503122A (en) 1994-04-07
CZ283495B6 (en) 1998-04-15
ATE129522T1 (en) 1995-11-15
IE72087B1 (en) 1997-03-12
DE69114143T2 (en) 1996-04-25
SK52693A3 (en) 1994-01-12
KR100226393B1 (en) 1999-10-15
ES2079180T3 (en) 1996-01-01
PT99606A (en) 1992-10-30
MA22349A1 (en) 1992-07-01
IE914094A1 (en) 1992-06-03

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