CA2074667A1 - Methode et appareil d'analyse de materiaux macromoleculaires - Google Patents
Methode et appareil d'analyse de materiaux macromoleculairesInfo
- Publication number
- CA2074667A1 CA2074667A1 CA 2074667 CA2074667A CA2074667A1 CA 2074667 A1 CA2074667 A1 CA 2074667A1 CA 2074667 CA2074667 CA 2074667 CA 2074667 A CA2074667 A CA 2074667A CA 2074667 A1 CA2074667 A1 CA 2074667A1
- Authority
- CA
- Canada
- Prior art keywords
- pyrolyzate
- trap
- traps
- outlet
- heating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000004458 analytical method Methods 0.000 title claims abstract description 52
- 239000000463 material Substances 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 title claims abstract description 23
- 238000000197 pyrolysis Methods 0.000 title abstract description 29
- 238000001816 cooling Methods 0.000 claims abstract description 63
- 229910052751 metal Inorganic materials 0.000 claims abstract description 15
- 239000002184 metal Substances 0.000 claims abstract description 15
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 239000011800 void material Substances 0.000 claims abstract 11
- 238000010438 heat treatment Methods 0.000 claims description 64
- 239000002826 coolant Substances 0.000 claims description 40
- 238000004891 communication Methods 0.000 claims description 27
- 239000012530 fluid Substances 0.000 claims description 27
- 238000012546 transfer Methods 0.000 claims description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 8
- 230000001105 regulatory effect Effects 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 7
- 230000001186 cumulative effect Effects 0.000 claims description 7
- 230000001276 controlling effect Effects 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 229910001220 stainless steel Inorganic materials 0.000 claims description 5
- 239000010935 stainless steel Substances 0.000 claims description 5
- 239000005350 fused silica glass Substances 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- 230000004044 response Effects 0.000 claims description 2
- 238000010926 purge Methods 0.000 claims 6
- 229910000619 316 stainless steel Inorganic materials 0.000 claims 1
- 230000000977 initiatory effect Effects 0.000 claims 1
- 239000011148 porous material Substances 0.000 claims 1
- 238000012882 sequential analysis Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 28
- 239000007789 gas Substances 0.000 description 23
- 150000002500 ions Chemical class 0.000 description 14
- 229930195733 hydrocarbon Natural products 0.000 description 11
- 150000002430 hydrocarbons Chemical class 0.000 description 11
- 239000012159 carrier gas Substances 0.000 description 10
- 239000004215 Carbon black (E152) Substances 0.000 description 8
- 239000011435 rock Substances 0.000 description 7
- 239000004020 conductor Substances 0.000 description 6
- 238000009413 insulation Methods 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 238000000045 pyrolysis gas chromatography Methods 0.000 description 4
- 239000010453 quartz Substances 0.000 description 4
- ZPEZUAAEBBHXBT-WCCKRBBISA-N (2s)-2-amino-3-methylbutanoic acid;2-amino-3-methylbutanoic acid Chemical compound CC(C)C(N)C(O)=O.CC(C)[C@H](N)C(O)=O ZPEZUAAEBBHXBT-WCCKRBBISA-N 0.000 description 3
- MGADZUXDNSDTHW-UHFFFAOYSA-N 2H-pyran Chemical compound C1OC=CC=C1 MGADZUXDNSDTHW-UHFFFAOYSA-N 0.000 description 3
- 150000001335 aliphatic alkanes Chemical class 0.000 description 3
- 230000004907 flux Effects 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 2
- 241000950638 Symphysodon discus Species 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 230000003466 anti-cipated effect Effects 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000000875 corresponding effect Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011152 fibreglass Substances 0.000 description 2
- 238000004817 gas chromatography Methods 0.000 description 2
- 239000011810 insulating material Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- 229920000136 polysorbate Polymers 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- -1 kerogen Substances 0.000 description 1
- WWYNJERNGUHSAO-XUDSTZEESA-N (+)-Norgestrel Chemical compound O=C1CC[C@@H]2[C@H]3CC[C@](CC)([C@](CC4)(O)C#C)[C@@H]4[C@@H]3CCC2=C1 WWYNJERNGUHSAO-XUDSTZEESA-N 0.000 description 1
- 241001593730 Acacia salicina Species 0.000 description 1
- 240000002791 Brassica napus Species 0.000 description 1
- 241001269524 Dura Species 0.000 description 1
- 241001364889 Helius Species 0.000 description 1
- 101000741788 Homo sapiens Peroxisome proliferator-activated receptor alpha Proteins 0.000 description 1
- 102100038831 Peroxisome proliferator-activated receptor alpha Human genes 0.000 description 1
- 108010085603 SFLLRNPND Proteins 0.000 description 1
- 101150098265 TDP2 gene Proteins 0.000 description 1
- 244000166490 Tetrameles nudiflora Species 0.000 description 1
- 230000035508 accumulation Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- VREFGVBLTWBCJP-UHFFFAOYSA-N alprazolam Chemical compound C12=CC(Cl)=CC=C2N2C(C)=NN=C2CN=C1C1=CC=CC=C1 VREFGVBLTWBCJP-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 238000013500 data storage Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000009428 plumbing Methods 0.000 description 1
- BALXUFOVQVENIU-KXNXZCPBSA-N pseudoephedrine hydrochloride Chemical compound [H+].[Cl-].CN[C@@H](C)[C@@H](O)C1=CC=CC=C1 BALXUFOVQVENIU-KXNXZCPBSA-N 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000012358 sourcing Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000002470 thermal conductor Substances 0.000 description 1
- 238000005382 thermal cycling Methods 0.000 description 1
- KUAZQDVKQLNFPE-UHFFFAOYSA-N thiram Chemical compound CN(C)C(=S)SSC(=S)N(C)C KUAZQDVKQLNFPE-UHFFFAOYSA-N 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/12—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using combustion
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0033—Other features
- B01D5/0036—Multiple-effect condensation; Fractional condensation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0033—Other features
- B01D5/0051—Regulation processes; Control systems, e.g. valves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0078—Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
- B01D5/0096—Cleaning
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/121—Preparation by evaporation cooling; cold traps
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/125—Preparation by evaporation pyrolising
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/126—Preparation by evaporation evaporating sample
- G01N2030/128—Thermal desorption analysis
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Immunology (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Molecular Biology (AREA)
- Automation & Control Theory (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US80033291A | 1991-11-27 | 1991-11-27 | |
| US800,332 | 1991-11-27 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2074667A1 true CA2074667A1 (fr) | 1993-05-28 |
Family
ID=25178128
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA 2074667 Abandoned CA2074667A1 (fr) | 1991-11-27 | 1992-07-27 | Methode et appareil d'analyse de materiaux macromoleculaires |
Country Status (4)
| Country | Link |
|---|---|
| CA (1) | CA2074667A1 (fr) |
| FR (1) | FR2684185B1 (fr) |
| GB (1) | GB2261827B (fr) |
| NO (1) | NO303512B1 (fr) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2488820C1 (ru) * | 2012-04-02 | 2013-07-27 | Общество с ограниченной ответственностью "Научно-производственная фирма "Мета-хром" | Устройство для определения содержания углеводородов в грунтах |
| CN105486764A (zh) * | 2014-09-19 | 2016-04-13 | 天士力制药集团股份有限公司 | 一种坤灵丸的气相指纹图谱的分析方法及其应用 |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5228514A (en) * | 1992-11-19 | 1993-07-20 | Ruska Laboratories, Inc. | Gas trap apparatus |
| US6190917B1 (en) | 1998-03-20 | 2001-02-20 | Cem Corporation | Microwave apparatus and method for analysis of asphalt-aggregate compositions |
| US6207462B1 (en) | 1998-03-20 | 2001-03-27 | Cem Corporation | Microwave apparatus and method for analysis of asphalt-aggregate compositions |
| DE102010022017A1 (de) | 2010-05-29 | 2011-12-01 | Gerstel Systemtechnik Gmbh & Co.Kg | Verfahren zur Probenvorbereitung bei chromatographischen Trennmethoden und Vorrichtungen zur Durchführung einer Probenvorbereitung |
| CN112326726B (zh) * | 2020-10-30 | 2023-12-29 | 北京临近空间飞行器系统工程研究所 | 一种树脂基复合材料热解引射因子测试装置及方法 |
| CN112666296B (zh) * | 2021-03-16 | 2021-06-29 | 常州磐宇仪器有限公司 | 一种用于色谱仪检测的双通道热解吸进样系统及方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4234315A (en) * | 1978-09-29 | 1980-11-18 | Phillips Petroleum Company | Gas chromatographic analysis method and apparatus |
| GB2161269B (en) * | 1984-07-02 | 1988-08-10 | Ruska Petroleum Lab Inc | Method and apparatus for analyzing hydrogen and carbon containing materials |
| US4842825A (en) * | 1986-06-19 | 1989-06-27 | Ruska Laboratories, Inc. | Apparatus for determining chemical structure |
| US5092219A (en) * | 1987-07-08 | 1992-03-03 | Thermedics Inc. | Selective decomposition of nitrite esters and nitramines |
| US4862932A (en) * | 1988-04-20 | 1989-09-05 | Bio-Rad Laboratories, Inc. | Fraction collector |
-
1992
- 1992-07-27 CA CA 2074667 patent/CA2074667A1/fr not_active Abandoned
- 1992-10-19 GB GB9221941A patent/GB2261827B/en not_active Expired - Fee Related
- 1992-11-26 FR FR9214240A patent/FR2684185B1/fr not_active Expired - Fee Related
- 1992-11-26 NO NO924567A patent/NO303512B1/no not_active IP Right Cessation
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2488820C1 (ru) * | 2012-04-02 | 2013-07-27 | Общество с ограниченной ответственностью "Научно-производственная фирма "Мета-хром" | Устройство для определения содержания углеводородов в грунтах |
| CN105486764A (zh) * | 2014-09-19 | 2016-04-13 | 天士力制药集团股份有限公司 | 一种坤灵丸的气相指纹图谱的分析方法及其应用 |
| CN105486764B (zh) * | 2014-09-19 | 2019-05-17 | 天士力医药集团股份有限公司 | 一种坤灵丸的气相指纹图谱的分析方法及其应用 |
Also Published As
| Publication number | Publication date |
|---|---|
| NO303512B1 (no) | 1998-07-20 |
| NO924567L (no) | 1993-05-28 |
| GB9221941D0 (en) | 1992-12-02 |
| GB2261827A (en) | 1993-06-02 |
| NO924567D0 (no) | 1992-11-26 |
| GB2261827B (en) | 1996-04-03 |
| FR2684185A1 (fr) | 1993-05-28 |
| FR2684185B1 (fr) | 1997-05-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Dead |