CA2037415C - Plant activation display apparatus - Google Patents

Plant activation display apparatus Download PDF

Info

Publication number
CA2037415C
CA2037415C CA 2037415 CA2037415A CA2037415C CA 2037415 C CA2037415 C CA 2037415C CA 2037415 CA2037415 CA 2037415 CA 2037415 A CA2037415 A CA 2037415A CA 2037415 C CA2037415 C CA 2037415C
Authority
CA
Canada
Prior art keywords
plant
fluid
node
nodes
display apparatus
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA 2037415
Other languages
French (fr)
Other versions
CA2037415A1 (en
Inventor
Hiroshi Takiyama
Yuji Naka
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Technosystems KK
Original Assignee
Technosystems KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Technosystems KK filed Critical Technosystems KK
Priority to CA 2037415 priority Critical patent/CA2037415C/en
Publication of CA2037415A1 publication Critical patent/CA2037415A1/en
Application granted granted Critical
Publication of CA2037415C publication Critical patent/CA2037415C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Abstract

there is provided a plant activation display apparatus for use in a plant in which various points of plant components are represented by nodes including at least one system input node axed at least one system output node, the adjacent nodes being connected to one another by means of fluid passages, with a pump unit and/or valve unit for creating a fluid flow in a specified direction being provided in the middle of each of the fluid passages in desired positions. An output device successively tracks each of the categorised fluids with a specified phase from the system input node to the system output node, and sequentially displaying the array of the tracked nodes in one direction. A control device successively determines whether or not the operating conditions for the pump unit and/or valve unit are fulfilled, starting from the one located on the system input node side, and causes the output device to make an emphatic indication to the effect that the pump un it and/or valve unit concerned should be operated when the corresponding operating condition is fulfilled, and an emphatic indication of only the fluid passages between those nodes through which flows are caused by the operation of the pump unit and/or valve unit.

Description

TITLE OF THE INVENTION
PLANT ACTIVATION DISPLAY APPARATUS
BACKGROUND OF THE INVENTION
Field of the Invention The present invention relates to a plant activation display apparatus which is suited for use in a plant which is expected to smoothly, securely perform plant operations, such as start-up, shutdown, and emergency shutdown operations of a chemical plant, or for plant activation evaluation through simulated plant operations.
Description of the Related Art Many chemical plants comprise a very large number of plant components, including columns and vessels such as a reactors, distillation columns, heat exchangers, etc., and transportation apparatuses such as pumps, sophisticated piping, valves, and the like.
The plant operations at the site of a chemical plant, which are examined to very fine details, are described in an operation standard or the like. The general plant operation is usually reviewed in accordance with the following three kinds of informations. The first information relates to the structure of thE> chemical plant. This information .includes the types of units constituting the plant, the height and local;.ion of each unit, the states of connection between the units, equipment necessary- to perform non-steads state operation such as start-up operation, the .initial and final states in the plant, etc. The second kind of information relates to the steps of the procedure for operating the units, and the third kind of information relates to the execution timing for executing each step of the procedure.
Conventionally, in designing a plant, the plant operation procedure for the start-up operation starts to be examined when the basic flowsheet is completed.
This will be described below with reference to Fig. 29.
First, a designer, having the operation procedure in mind, decides the necessary piping location and the arrangement of pumps, main valves, etc. Then, the designer investigates the steps of the start-up operation procedure. The relationship between the designer's intention to operate the plant and the plant structure is often difficult for another designer to understand.
Usually, a plant designer is not an operator, so that the operator often cannot fully understand the designer's intention of the operation procedure, or the designer cannot understand what the operator expects the operation procedure to be.
These problems are attributable to the fact that there are no specific methods to definitely connect the process design, its operation procedure, and the timing for the execution thereof, despite the intimate relationships between them. It is to be desired, in particular, th at the execution timing as well as the conventional control systems are registered in a distributed control system (DCS), and are sequentially displayed on the display screen of an operation support apparatus. Various problems are caused by an indefinite representation of the relationships between the four elemenl~s shown in rig. 29, including the plant design, operation procedure, execution timing, and operation support apparatus.
For instance, even when PFD (Process Flowsheet Diagram) and P & ID (Piping and Instrumentation Diagram) are completed at the design phase, describing the start-up procedure, shutdown procedure, etc. in the manuals requires much time. The preparation of manuals has not been systematized yet, and each designer in charge confirms his or her planned steps of the procedure on the completed flowsheets one after another, which requires much time. Since errors are likely to be m:~de and the procedure is likely to be described in various expressions, moreover, the procedure would be very difficult for users (particularl,y, operators) to understand. The operation for converting the description of the procedure into the computer-a:Lded operation support screen is believed to be an independent work project, which also requires much time and labor.
Chemical plants are often modified or revamped, in which case the operation procedure and execution timing should be modified at the same time. Conventionally, however, modified sections of the plant and the associated modification of the operation procedure are not clearly described, so that accurate modification requires much time and labor. In this case, the operation support screen should be also modified, which also requires much time.
Since the relationship between the operation procedure and the elecution timing is not clear ly illustrated at the design phase, it is likely that the valves, etc. are positioned at the wrong places. Such plant thus designed will need great efforts to operate the valves, etc. as well as complicated operations.

-In shortening the start-up time, furthermore, it is very hard to be acquainted with the necessary preliminary apparatuses or equipment, or to know how to modify the operation procedure and execution timing.
If a chemical plant involves a combined unit which integrates several units , the di f ference between the operation procedure to operate the individual component units separately and those for operating the combined unit is not clear. It is often difficult, therefore, to determine whether the operation procedure to operate the individual units separately can be applied to the combined unit type.
Conventionally known are several studies on the representation of the plant operation procedure, although they are not satisfactory yet. These studies provide the following decision methods of operation procedures as follows: (1) A method based on the assumption that valve operation controls the operation procedure for a chemical plant if it is designed so as to form a targ et flow from the inlet of the plant to the outlet (J.R. Rivas and D.F. Radd, AIChE J., vol. 20 (2), 320-325 (1914); O'Shima, J. Chem. Eng. Japan, vol.
11 (5), 390-395 (1918)).
(2) A so-called automatic start-up procedure synthesis method in which the definitions of the functions of the constituent units are strictly-hierarchized, and the functions are connected in succession usinc; a knowledge engineering approach (Hwan,~ hue Suku, Shigeyuki Tomita, Ei,ji O'shima, Chem.
Eng. Reports vol.. 14 (6), 728-738 (1988)).
(3) A method for determining the plant operation procedure b5- handling steps of procedure structured ~'~:'::

with the plant operation as a knowledge base (R. Lakshamanan and G. Stephanopc>ulos, Comput. Chem. Engng., vol. 12 (9/10), 985-1002 (1988); R. Lakshamanan and G. Stephanopoulos, Comput.
Chem. Engng., vol.. 12 (9/10), 1003-1021 (1988); R. H. Fusillo and G. J. Powers, Comput. Chem. Engng., vol. 12 (9/10), 1023-1034 (1988)).
These methods of determining the plant operation procedure are all_ designed to determine the operation procedure based on a given plant structure, and basically involving description in text. There is therefore a difficulty in describing parall'_el operations. Since the plant structure is not clearly described in association with the operation procedure, when t:he plant structure is changed, it is difficult to understand the correlation between the modification of the structure and the. resulting, necessary modification of the operation procedure. In this case, the operation procedure should be recons_Ldered from the beginning.
SUMMARY OF THE INVENTION
The object of the present invention is to provide a plant activation tracking and display apparatus which can ensure clear illustration of the relation between the process design, the operations and the execution timing, as well as can permit the illustration to be used as a screen to support the plant operation.
According to the present invention, there is provided a plant activation tracking and display apparatus for use in a plant in which a plurality of points of plant components are represented by a plurality of nodes including at least one system input node through which an input fluid is externally supplied to the plant, and at least one system output node, through which an output fluid flows out from the plant, adjacent nodes of. said plurality of nodes being connected by means of fluid passages, at least some of said fluid passages having at least one transportation means and/or valve means for creating a fluid flow in a specified direction, the apparatus further comprising: an output device including:
means for categorizing all fluids flowing through said fluid passages, when the plant is in operation at a steady-state condition, in accordance with type and phase of said fluids, means for successively tracking categorized fluids with a specified phase over said plurality of nodes from said system input node to said system output node, and display means for sequentially disF~laying arrays of tracked nodes of said plurality of nodes in one direction; memory means for previous-ly storing data which correspond to operating conditions for each said transportation means and/or valve means; sensor means for sensing the operating conditions for each said transportation means and/or valve means to determine whether the operating conditions for each said transportation means and/or valve means are fulfilled; and output device control means for successively determining whether said operating conditions for each said transportation means and/or valve means are fulfilled, starting from the system input node side, and for causing t:he output device to make an emphatic indication that each said transportation means and/or valve means be operated when said conditions thereof are fulfilled, - 6a -and to make a further emphatic indication of only fluid passages between nodes through which fluid is caused to flow by the operation of each said transportation means and/or valve means.
The invention also provides a plant activation track-ing and display apparatus for evaluating plant activation through simulated operation of a plant in which a plurality of points of plant components are represented by a plurality of nodes including at least one system input node through which an input fluid is externally supplied to the plant, and at least one system output node, through which an output fluid flows out from the plant, adjacent nodes of said plurality of nodes being connected by means of fluid passages, at least some of said fluid passages having at least one transportation means and/or valve means for creating a fluid flow in a specified direction, the apparatus further comprising: an input device for producing a data signal through external input operation; an output device including means responsive to the data signal delivered from said input device, for categorizing all fluids flowing through said fluid passages when the plant is in operation at a steady-state condition, in accordance with a type and a phase of said fluids, for successively tracking categorized fluids with a specified phase over said plurality of nodes from said system input node to said system output node, and for sequentially displaying arrays of tracked nodes of said plurality of nodes in one direction; memory means for previously storing data correspond-ing to operating conditions for each said transportation means - 6b -and/or valve means in response to the data signal delivered from said input device; simulation signal output means for outputting a simulated signal for simulatively making said operating conditions for each said transport means and/or valve means fulfilled to desired operating conditions; and output device control means for successively determining whether said operating conditions for each said transportation means and/or valve means are fulfilled, starting from the system input node side, depending on the presence of the simulated signal output from said simulation signal output means, and for causing the output device to make an emphatic indication that each said transportation means and/or valve means be operated when said operating conditions thereof are fulfilled, and to make a further emphatic indication of only fluid passages between nodes through which fluid is caused to flow by the operation of each said transportation means and/or valve means.
If necessary, the plant components may include a heat exchanging component. In this case, at least one of the nodes is connected to a node of the heat _ 7 exchanging component through energy transfer, the heat exchanging compcanent being displayed on the output device, in the ~~icinity of the energy transferring nodes in parallel relation therewith. The fluids flowing through the fluid passages connected to that node which exchanges energy with the node of the heat exchanging component are regarded as identically categorized fluids if the fluids would change in phase state, around the node concerned. If necessary, the plant component: include a hold-up device to be displayed as one node.
Basically, plant operations such as start-up operation, are intended to create flows of a fluid in a desired state between the nodes of the plant components by effecting "f~.oca control" between the nodes and, if necessary, "holdup cont.rol." Thus, the present invention is based on an understanding that the plant operation procedure and execution timing can be displayed in as__=;ociation with the line c:onfiQurdtion of the plant by successively tracking each of the categorized fluids with a specified phase from the system input node to the system output node, and displaying the arra~~s of the tracked nodes in one direction. The plant operation procedure and execution timing' displayed on the output device in the aforesaid mannerĀ°, that is, sequence graphs of the plant are represented along the fluid flows or in association ~~-ith the line configuration.
Automatic operation may be enabled by providing the plant activation display apparatus of the present invention with drive means for driving the transportation means and/or valve means, so that the _8_ drive means is caused to drive the transportation and/or valve means when the operating conditions are fulfilled.
The plant activation display apparatus of the present invention may be used as a simulation support apparatus or a design support tool by replacing the sensor means with simulation signal output means for outputting a simulated signal for simulatively making the operating conditions on the transport means and/or valve means fulfilled. In this arrangement, it is successively determined whether or not the operating conditions for the transportation means and/or valve means are fulfilled, starting from the one located on the system input node side, depending on the presence of the simulation signal from the simulation signal output means, and the output device is caused to make an emphatic indication to the effect that the transportation means and/or valve means concerned should be operated when the corresponding operating condition is fulfilled, and an emphatic indication of only the fluid passages between those nodes through which flows are considered to have been caused by the operation of th<~ transportation means and/or valve means.
BRIEF DESCRIPTION OF THE DRAWINGS
Fig. 1 is a schematic diagram showing a configuration oi" a distillation column system according to a first embodiment to which a plant activation tracking and display app<~ratus of the present invention is applied;
Fig. 2 is a schematic diagram showing a configuration of the plant activation display apparatus 2p37415 _ g -applied to a distillation column system;
Fig. 3 is <~, flowsheet diagram showing a line configuration o:E a distillation column in a steady state operating condition;
Fig. 4 is a flowsheet diagram distinctively showing fluid transportation means;
Fig. 5 is a diagram showing necessary pumps and valves added to the flowsheet of Fig. 4;
Fig. 6 is a diagram showing an arrangement for the hold-up;
Fig. r is a flowsheet diagram showing a line configuration necessary for a steady-state transition operation with Ei total reflux at the time of a start-up operation;
Fig. 8 is a flowsheet diagram showing a line configuration ne~cessar,y for a steady-state transition operation with a circulation at the time of the start-up operation;
Fig. 9 is a diagram showing a node configuration of the distillation column system of the first embodiment;
Fig. 10 is a sequence graph displayed on a display device 44 shown in Fig. 2;
Fig. 11 is a flowchart illustrating steps of procedure of the start-up operation executed by means of an electronic: control device 40 shown in Fig. 2;
Fig. 12 is a block diagram showing a configuration of a heat pump connected to a distillation column system according to a second embodiment to which the plant activation. tracking and display apparatus of the present invention is applied;
Fig. 13 is a diagram showing a node configuration on the distillation column side according to the second embodiment;
Fig. 14 is a diagram showing a node configuration on the heat pump side according to the second embodiment;
Fig. 15 i~, a sequence graph illustrating a case in which only the distillation column side of the second embodiment is activated;
Fig. 16 is a sequence graph illustrating a case in which only the heat pump side of the second embodiment is activated;
Fig. 16A is a sequence graph illustrating a preliminary operation for the injection of a working fluid in the heat pump;
Fig. 16B is a sequence graph illustrating a preliminary operation for the circulation of a heat exchanger working fluid in the heat pump;
Fig. 16C is a sequence graph illustrating a preliminary operation for a circulation line of a compressor of t:he heat pump;
Fig. 16D is a sequence graph illustrating a preliminary operation for a drain line of the heat pump;
Fig. 16E is a sequence graph illustrating a preliminary operation for the ventilation of the heat pump;
Fig. 16F is a sequence graph illustrating a preliminary opei~ation for a superheating protection line of the compressor of the heat pump;
Fig. li is a diagram showing a node configuration for connecting t:he distillation column and the heat pump;

a Fig. 18 i;> a sequence graph illustrating the distillation column system according to the second embodiment;
Fig. 19 i~> a timing chart illustrating operation times for the valves and the like used when the distillation column system is started up in accordance with the sequence graph of Fig. 18;
Fig. 20 is. a timing chart illustrating operation times for the valves and the like used when the start-up time is shortened;
Fig. 21 is a diagram showing a configuration of an evaporator;
Fig. 22 is a diagram illustrating the way of representing a sequence graph for the evaporator;
Fig. 23 is a diagram showing a configuration of a self-heat exchanging reactor;
Fig. 24 is a diagram illustrating the way of representing a .sequence graph for the reactor of Fig.
23;
Fig. 25 is a block diagram showing a line configuration for supplying two types of fluids A and B
to a tank 110;
Fig. 26 is a diagram illustrating the way of representing a sequence graph used when the supply of the fluid B is :started after a set amount of the fluid A is introduced into the tank;
Fig. 27 is a diagram illustrating the way of representing a ,sequence graph used when the fluids A
and B are simultaneously supplied to the tank;
Fig. 28 is a diagram illustrating the way of representing a =_~equence graph equivalent to the one shown in Fig. 26, used when the fluids A and B are simultaneously ~>upplied to the tank; and Fig. 29 is a block diagram for i.Llustrating the basic concept of the present invention.
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS
The following is a description of a plant activation display apparatus according to a first embodiment of the present invention, as applied to a distillation co"_umn system. Since this display apparatus functions as a process design support tool for a plant, the' plant design procedure will be described first, Line Conf.igurat~on for Steady State Operation Let it be supposed that a pipeline configuration for the steady ~~tate operation and internal states of the plant are previously determined at the stage of the basic process design. Principally, a distillation column comprise~~ a column section, a reboiler, and a condenser, the -last two serving as heat exchanging elements. Fig. 3 shows the line configuration and elevation for these elements. In Fig. 3, the arrows indicate the directions of flows; the regular full line represents a flow of a liquid, the thick full line a flow of a gas-liquid mixture, the broken line a flow of a gas, and the double line a flow of heat. A circle (Q) indicates the point, of an inlet, outlet, or junction of the fluid. In this case, the internal states of the p_Lant, including the flow rate, composition, pr<~ssure, temperature, and the phase of the fluid, are previously determined as simulation data for the steady :Mate operation. Also suppose that the premises for the selection of the individual components, worl~;ing conditions, preliminary conditions, etc. are previously determined, and that the properties or reaction conditions of the fluid, such as the reactivity (polymerizability in particular), explosiveness, combustibility, toxicity, and corrosiveness, and other conditions, including the liability to cr5rstallization, solidification, scale, slurry, etc., are given.
(Layout of Pump;, Valves, etc.) Based on the above premises, the layout of valves, pumps and so forth necessary for the plant operation is determined. In making this decision, the concept of "flow control," which is essential to the realization of the present invention, is used.
The concept: of "flow control" includes two meanings: The first one is related to the control of the fluid state or creation of a fluid flow, and the second one is related to timing control main ly for the valve operation to create the flow, which will be described in detail later. For the former mode of control, it is necessary to study how to create the flow of the fluid at a steady state as shown in the plot plan of Fi~;. 3, and to investigate a device which causes a change in phase of the fluid, if any, to result in heat eexchange or a large pressure change (flash or the like).
The schematic plot plan of Fig. 3 is therefore prepared at the stage of PFD design. Since the types and the locations of a material tank, condenser, reflux tank, reboiler, bottom tank, etc. have already been determined as known information, the locations of the inlet point, outlet point and ,junction point (each indicated b,y Q;I shown in the flowsheet in Fig. 3 are rewritten, and at the same time, elements such as ejectors, which utilize external force to create a fluid flow,are distinguished from those which do not create such flow. Fig. 4 presents a flowsheet which distinguishes fluid transportation means. In this embodiment, those fluid transportation means which can create a fluid flow without using external force are indicated by labels "G," "S," and "PR." The label "G"
represents the fluid transportation means capable of carrying the fluid through gravity, "S" the or.e capable _ of conveying th~= fluid utilizing the siphon effect, and "PR" the one capable of transporting the fluid by means of pressure drop originating from condensation.
As shown in Fig. 4, those fluids except vapor and the fluids affi~ced with the above symbols and classified accordingly need transportation means involving external force. This transportation means may be means for applying high pressure to the fluid to carry it, such as a compressor, a pump, an ejector, and a device for causing a throttle valve to cooperate with the heating operation, or means for decompressing the fluid to car ry- it, such as a decompressing pump, an ejector, and a device for causing a throttle valve to cooperate with an operation to condense gas. Any one of means can be properly selected in accordance with the fluid type, physical properties, etc.
According to this embodiment, as shown in Fig. 5, it is necessary to provide a pump P1 between the inlet point for material supply and the material supply stage of the distillation column, a pump P2 in an intermediate portion of a fluid passage between the reflux tank of the condenser and the top of the distillation column, a pump P3 between this reflux tank and the outlet for a distillate, and a pump P4 between the bottom tank and the outlet for a distillate (bottom product) at the' column bottom. Though not illustrated in Fig. 5, preliminary devices or protection lines have only to be added when needed by proper ly selecting such external-force using transportation means.
In the ca~~e of the distillation column system of this embodiment, the valves should only be arranged according to th.e following rules. For example:
Rule 1: Dispose a valve on the discharge side of -a pump in line for maintenance of the pump. It is to be noted that a valve may be omitted for a pump that pumps up a constant amount of the fluid.
Rule 2: Dispose a valve on the inlet side of heating steam for the reboiler, and a drain valve on the outlet side.
Rule 3: Dispose a valve at the inlet or outlet of cooling water for the condenser.
Rule 4: Dispose a valve in the outgoing line from the tank.
Rule 5: At least one control valve (CV) is required when multiple lines from the tank are connected.
Fig. 5 illustrates the arrangement of valves according to they above rules. It is to be understood that the types of valves depend on their usage and the type of the fluid.
(Location of Hold-up) When the p)Lant is operatinc at a steady state, the hold-up does not; appear necessary. In view of a unsteady state process, such as start-up or shutdown operation, the hold-up is important in determining the execution timing of the plant operation procedure. In other words, the aforementioned "flow control" is executed by disposing the hold-up where necessary and controlling its quantity. In particular, it is necessary to provide the hold-up on the upstream side of a pump in order to ensure stable transportation of the fluid. Strictly speaking, the change in fluid phase normally does not occur at uniform speed, and is subject to fluctuation. In this respect, the hold-up is disposed at the location before the phase change takes place to thereby provide residence time for the flow and absorb fluid fluctuation. It is to be understood that the hold-up is provided to reserve the material liquid, the distillate (bottom product) at the column bottom, and the distillate (top product) at the column top.
Fig. 6 shows the hold-ups arranged from the above view points. A material supply tank Hl is disposed at the point from 'which a raw material is supplied, a bottom tank H5 at the bottom of the distillation column, and a r~eflu:c tank H8 on the distillate outlet side of the condenser. A top product tank H9 is located on the downstream side of the top distillate outlet, and a bottom product tank H10 is disposed on the downstream aide of the bottom distillate outlet.
In Fig. 6, these tanks are indicated by "Q".
Line Configuration for Start-Up Operation Then, a line configuration for the start-up operation is in~festigated, and necessary lines are added. The so-called total reflux operation, circulation operation, and effluent operation are known as start-up operation strategies. From the economical point of view, as well as in light of shortening the start-up operation time, it is necessary only to examines the former two operations, i.e., the total reflux operation and the circulation operation, as the line configuration for the start-up operation.
(Line Configuration for Total Reflux Operation) For the total reflux operation, the material supply line, top distillate line, and bottom distillate line are cut off so that all the fluids flow back and the distillates from the reflux tank H8 and bottom tank H5 respective ly have target compositions. Valves VI, V4 and V6 are provided on the respective lines to cut them off. As illustrated in Fig. r, this operation strategy requires no additional equipment but simply the open/close operation of the valves for the reflux purpose.
(Line Configuration for Circulation Operation) The circulation operation is an operation strategy wherein the top and bottom distillates are returned to the material supply tank H1 and kept within the operation.
For this operation, it is desirable to move to the total reflux operation when the top and bottom distillates reach a predetermined composition (temperature). However, start-up operation may be effected in the circulation operation until the distillates reach the desired composition (temperature). Recycle lines S20 and S21 which run from a top distillate line S12 and a bottom distillate line S14 back to the tank H1 are required as preliminary lines.
As the material supply tank HI, top product tank H9 and bottom :product tank H10 are all located on the ground, pumps :ire needed to return the distillates from these tanks H9 and H10 to the tank Hl. If the switching vale<~s SV1 and SV2 are disposed on the downstream side of the valves V4 and V6,of the distillate lines S12 and Sl4,and the recycle lines S20 and S21 are branched from the valves SV1 and SV2 shown in Fig. 8, the distillates would be circulated back to the tank HI by means of the pumps P3 and P4.
Through the above procedure, the basic plant design has been completed. It is preferable to investigate a changing line or by-pass line for inert gas for the start-up operation and, moreover, to examine a line configuration for emergency shutdown operation.
Fig. 9 is the flowsheet of the thus designed distillation column system shown in Fig. 8 with reference numerals given to the nodes, processing fluid and valves. The nodes representing the individual nodes of the plant components include pipe junction point, part of a unit, a unit such as a heat exchanger which has no point to connect to other pipes, a unit such as a pump which utilizes external force, an internal node such as a hold-up, a system input node through which the process fluid or working fluid is externally supplied to this plant, and a system output node from which the fluid flows out of the plant. The process fluid is indicated by reference numeral "Sl" or the like in contrast with the fluid flowing between the adjacent nodes. This reference numeral may be also regarded as an .indication of the fluid passage through which the fluid flows between the nodes. In some cases r, ~ 20374 15 the "fluid pasaage" means not only a pipe but also a column unit. 'thus, a feature of the present invention lies in that the process fluid is associated with the fluid passage.
A supply :Line SO to the material supply tank Hl is added. Here, "HO" denotes the system input node, that is a material reserving tank, and "PO" and "VO"
respective ly indicate a pump and a valve disposed on the supply line S0. The material reserving tank HO
includes a mobile tank unit such as a tank truck.
Fig. 1 is a schematic block diagram illustrating the distillation column system designed in the aforesaid manner. This system comprises a distillation column D, a reboiler RB, a condenser CD, reserving tanks, pumps and valves. Since like reference numerals are used to designate the components corresponding to the ones shown in the flowsheet of Fig. 9, a detailed description of those components will be omitted.
The distillation column system according to the first embodiment is equipped with the plant activation display apparatus shown in Fig. 2. The display apparatus displays the plant operation procedure and the execution taming, so that operators execute the plant operations, such as the start-up operation, while monitoring what is on the display.
Configuration of Plant Activation Display Apparatus The plant activation display apparatus comprises an electronic control unit (ECU) 40 for controlling the activation of the entire apparatus, an input device 42, a displa,v device 44, a printer 46, an external memory device 48, an I/O interface 50, a drive device 52, and sensor means 54. The input device 42 serves to input the plant configuration and a plant activation command signal when its keys or switches are operated. The display device tE4 displays the result of computation done by the electronic control unit 40 or the like on the screen. Lil~;ewise, the printer 46 prints out the computation result from the control unit 40. The external memory device 48 stores computing processes (program) or the like, which are to be executed by the control unit 40, The I/O interface 50 controls the input/output of the control unit 40. The drive device 52 opens or cloy>es valves and drive pumps in response to a drive signal sent via the I/O interface 50 from the control unit, 40. The sensor means 54 detects the hold-up level, column temperature, pressure, line flow rate, etc., and supplies them to the control unit 40 through the I/O interface 50.
The following is a description of the action of the plant activation display apparatus.
Preparation of :>eguence Graph Before describing the action of the plant activation display apparatus, a description will be given of how to prepare a sequence graph to be displayed on the screen of the display device 44 in the plant activation display apparatus, which is the fundamental technical concept of the present invention.
(Representation of Fluid Connection and Conditions for Flow Control) It is believed that the procedure of the operations of the chemical plant, especially the start-up operation procedure, is basically determined by performing "flow control" and "hold-up control," while conforming to the conditions for safety and product quality. In other words, the fundamental technical concept of the present invention is based on the ideas of "flow contrc>1" and "hold-up control."
When the ~~tart-up operation is executed to set the chemical plant from an initial state to a target state or steady state, the "flow control" is to control the state of the fluid in each line or fluid passage between the adjacent nodes, starting with the system input node to the system output node, to thereby establish the target flow state from the initial state.
According to the present invention, how ~o express the flow of the fluid in the plant is based on the knowledge that attention being paid to the phase state of the fluid, the operation procedure can naturally be represented if the fluid of the same phase is sequentially tracked from the nodes on the system input side to those on the system output side.
If the fluid in the same state is tracked from the nodes on the syatem input side, a change in phase of the fluid midway inhibits further tracking of the fluid from that point. This phase change results from heat exchange with the fluid or a Large change in pressure on the fluid. If such heat exchange or a substantial pressure change occurs, the phase-changed f=Luid is considered to be continuous at the point of change. In this respect, the phase-changed fluid i;s tracked forward to the nodes on the system output side.
with hold-ups provided wherever required in the plant, the "holo!-up control" is necessary to control the hold-up quantity for stable plant operations, particularly for ensuring stable operation timing. The - 2z - 20 374 1 5 "hold-up contro~L" is applied to start and stop conditions of the valve operation, such as the valve operation start~~ng when the hold-up quantity of the fluid flowing into the hold-up reaches a preset discrimination ~Talue. This discrimination value may vary according i:o the plant state, taking several proper values accordingly. For example, a discrimination value for drive a pump can be set different from i:he one after the steady state is reached. In other words, the discrimination value of the hold-up is considered to be a variable associated with the necessf~,ry start-up operation time and the quality control,.
Based on the idea described above, all possible phase states of the process fluid that flows between the adjacent nodes in the flowsheet shown in Fig. 9, are categorized so that all possible fluid connections a.nd conditions for flow control are given in the table 1 below.
Table SO (0-H -~1-H . L . . PO . V0 ) Sl (1-H ~ 3 . L . . P1 . V1 ) S2 (2 ~ 3 . L . . . ) S 3 ( -~4 . L . . . ) S4 (4 ~ 5-H . L . . . ) S5 ( ->6 . L . . . ) S6 (6 ~ 4 . V+L . +E2 . . ) S7 (4 ~ 3 . V . . . ) S 8 ( -~2 . V . . . ) S9 (2 ~ 7 . v . . . ) S 10 ( -~8-H . L . -E 1 . . ) S11(8-H -~2 . . . P2 . V2 ) L

S12(8-H -~18 . . . P3 . V4 ) L

S13i18 -~9 . . . . SVl(2)) L

SI4(5-H ~ 17 . . . P4 . V6 ) L

S15(17 ~ 10-H . . . . SV2(2)) L

S16(11 ~ 12 . . . . V3 ) L

S17(12 -~13 . . +El . . ) L

S18(14 ~ 15 . . -E2 . . V5 ) V

S19(15 -~16 . . . . ) L

S20(18 -~1-H . . . . SV1(1)) L

S21(17 -~1-H . . . . SV2(1)) L

The follow~~ng is a description of some of what are indicated by the' above representation of fluid connections the conditions for and flow control shown in Table 1.
The process fluid Sl is a liquid L which flows to the node 3 (feed plate of the distillation column) from the node 1-H (mf~,terial supply tank H1). The pump P1 is driven to make i:he liquid flow, which starts only when the valve V1 is opened.
The proces~~ fluid S3, a liquid L flowing from the node 3 to the node 4, runs without any external force.
The proces:~ fluid S6 is a mixture of gas and liquid (L+V) flowing from the node 6 to node 4. Since the phase of the' fluid S6 changes from the liquid phase L to the mixed phase (L+V) before or after the node 6, an external hearing energy +E2 is necessary at the node 6.
The process fluid S10 is a liquid L running from the node 7 to node 8-H (reflux tank H-8). Since the fluid S10 changes its phase from the vapor phase V to 2~3~4 15 the liquid phasE~ L around the node 8-H, an external cooling energy --E1 needs to be provided at the node 8-H.
The process fluid S15 is a liquid L which runs from the node 1'? to the node 10-H (bottom product tank H-10). The fluid S15 starts flowing when the switching valve SV2 of the node li is set to the state i2).
Table 2 ON conditions SO [ON <;1-HS] PO VO
.

S1 [ON > 1-HS] P1 V1 .

ss (oN]

s4 [oN]

S5 [ON]

S14[ON ;>5-H$] P4 V6 .

S21[ON SV2(1) .

S6 [ON > 5-HS] E2 .

S7 [ON]

S8 [ON]

S9 [ON]

S10[ON ] E1 .

S11(ON ;~8-HS] P2 V2 .

S12[ON > 8-HS] P3 V4 .

S20[ON ] SV1(1) .

S2 (ON]

SO [OFF > 1-HS, > 5-HS, > 8-HS]

Table 2 shows preset conditions under which the process fluid can be produced, or operating conditions for valves and pumps. These conditions should be determined beforehand.

20374 ~5 The condit~_on to permit the process fluid SO to flow iON condit:~on) is that the hold-up quantity of the hold-up H1 is smaller than a set value (1-HS). At this time the pump PO is activated and the valve VO is opened. When the hold-up quantity of the hold-up H1 becomes greater than the set value (1-HS), and when the hold-up quantities of the hold-ups H5 and H8 respectively become greater than set values (5-HS) and (8-H5), the pump PO is stopped to set the process fluid SO in an OFF stt~te. If it takes much time to prepare the pumps, the rump FO should be kept operating in an idling state.
The ON condition for the process fluid S1 is the hold-up quantity of the hold-up H1 greater than a set value (1-HS). When the ON condition is satisfied, the pump P1 is activated and the valve V1 is opened.
The proces:> fluid S3 is always in an ON state, which means that: when it is supplied to the node 3, the fluid S3 drops by the force of gravity, thus creating a fluid flow.
With regard to the process fluid S6, when the hold-up quantity of the hold-up H5 becomes greater than a set value (5-fIs), steam is caused to flow to the reboiler to create the flow of the fluid S6. The reboiler should be warmed up so that the steam is supplied to the reboiler on starting the start-up operation.
Table 3 S15 (ON . '.7 -~ 10 . . SV2I2) . #1]
S13 [ON . l.8 -j. 9 . . SV1(2) . #2]

Table 3 shows operating conditions for switching from the start-up operation to the steady-state operation. When the condition for the transition to the steady-state operation indicated by "#1" is fulfilled, the switching valve SV2 is set to the state (2) so that the process fluid S15 flowing from the node 17 to node 10 is rendered ON. When the condition for the transition i~o the steady-state operation indicated by "#2" is fulfp_Iled, the switching valve SV1 is set to the state (2) so that the process fluid S13 flowing from the node lei to node 9 is rendered ON. For the _ transition-to-steady-state conditions ~1 and 2, each composition (temperature) of the bottom and top distillates should be at a set value (target value).
When the aforesaid fluid connections and conditions for flow control are prepared, these pieces of information a.re inputted into the electronic control unit 40 through the key operation of the input device 42. When a computation start command signal is inputted to the control unit 40 through the input device 42 upon completion of the information input, the control unit 40 prepares a sequence graph based on the information shown in Tables 1 to 3, In accordance with the stored computation procedure, a graph is displayed on the screen of the display device 4=~. Fig. 20 illustrates a sequence graph for the start-up operation, which is the result of computation done b,y-the control unit 40 and displayed on the display device 44.
Sequence Graph The following is a description of the way the control unit 40 prepares this sequence graph on the _ 2037415 - 2r -basis of the computation result shown in Fig. I0.
It is easy for one skilled in the art to prepare a program so that= the control unit 40 runs to obtain the sequence graph of Fig. 10 on the basis of the aforementioned fluid connections and conditions for flow control shown in Tables I to 3, and there are various ways to prepare the program, so that no particular discussion will be given to the details of the program preparation. The feature of the present invention lies in displaying a sequence graph which expresses the designed plant configuration, operation procedure and execution timing in a single flowsheet, not in how to prepare the computer software.
The sequence graph of the present invention indicates the individual points of the plant components by nodes, and shows their layout along the flow of the fluid in one direction on the screen or downward from the top of the acreen in this embodiment, successively tracking the nodes from the system input node to the system output node on the basis of the phase state of the fluid. In i~he sequence graph shown in Fig. 10, at the input node of the body of the distillation column, there is a singJ_e node 0-H, which corresponds to the material reserving tank H0. At the output nodes, there are two nodes 9--H and 10-H, which correspond to the top product tank H9 and bottom product tank H10. There are input nodes I=1 a.nd lI as well as output nodes 16 and I3 respective ly in the reboiler and condenser, which constitute a heat exchanger.
This sequence graph is the contents of Tables 1 to 3 converted into a flowsheet according to the procedure presented below. First, the control unit 40 tracks the fluid of the same phase in order from the system input node to the sysl-,em output node, on the basis of the input information given in Table 1. More specifically, with regard to i~he process fluid SO of a liquid phase, this fluid of a liquid phase L flows from the node f)-H
(the input nodes and reaches the hold-up node 5-H
passing through the nodes 1-H, 3 and 4 in the named order. The fluud is branched to two directions at the node 5-H; one pt~.rt becomes the process fluid S14 and reaches the nodE~ li. At the node 17 or the switching valve SV2, this fluid becomes either the process fluid S15 or S21 in ac:cordanee with the switching state of the valve SV2, reaching the node 10-H or returning to the input node .l-H accordingly.
The other i'luid branched at the hold-up node 5-H
becomes the process fluid S5 which reaches the node 6.
At the node 6 the fluid S5 changes its phase due to heating energy I+E2) from the reboiler to have a mixed phase of the vapor phase V and liquid phase L. When there occurs he~~t exchange, the process fluid is considered to be continuous according to the aforementioned rules. The fluid S6 of the mixed phase moves from the node 6 to the node 4. At the node 4, the fluid S6 is divided into two phases. A liquid portion becomes the aforementioned process fluid S~, which reaches tree hold-up node 5-H again, a gaseous portion becomes the process fluid S7, which rises up by the force of gravity (density difference) and reaches the node 7 of the condenser passing through the nodes 3 and 2 in the named order. During this period, the fluid S7 keeps i:he vapor phase, and the flow is indicated by the broken line in the flowsheet.

At the node 7 the heat (-El)of the fluid is removed by the cooling water, causing the phase transition from the vapor to liquid. In this case the process fluid i:~ also considered to be continuous because of the heat exchange, so that it becomes the process fluid SLO, reaching to the hold-up node 8-H or the reflux tank H8. The fluid is divided into two portions at the node 8-H. One becomes the process fluid S11 of a =Liquid phase L, which .returns to the node 3 through i:,he node 2, and the other becomes the process fluid 512, which reaches the node 18. The fluid S12 becomes either the process fluid S13 or S20 in accordance with the switching state of the switching valve SV1, the i_'ormer reaching the output node 9-H and the latter returning to the input node 1-H.
The steam i'luid S18 of a vapor phase comes from the input node :'~~4 of the reboiler and reaches the node 15 via the valve V5. This fluid changes its phase here and reaches the output node 16. The cooling water S16 of a liquid phase from the input node 11 of the condenser reaches the node 12 via the valve V3. After heat exchange there, the resultant fluid reaches the output node 13.
Various synnbols in the sequence graph will now be explained. The structural nodes are denoted by circles including ellipses. What is included in the structural nodes is as described before (see Fig. 9?.
The conditions for hold-up control and various decision conditions are contained in brackets '' [ ] " . The decision conditions may additionally include various conditions, such as the ones for the transition from the start-up opeeration to the steady-state operation, besides the hold-up quantity and the liquid level. It is to be under:atood that all the possible decision conditions according to this embodiment are taken into consideration at the stage of the preparation of Tables 1 to 3, as des<:ribed before.
Although t:he valves are normally closed in the initial state, the operation sequence may go close open -~ close ..., depending on the situation.
Therefore, the word or symbol "CLOSE" is added to indicate the closure of each valve. This symbol can be displayed with varying brightness on the screen; it may be dark when the valve is closed, and bright when the valve is open, for example.
The directions of flow are indicated by the arrows in Fig. 10, and the broken lines drawn perpendicular to the flow as if to shield the flow indicate the activation of valves, heating or cooling, pumps, and compressors. If every node having a flow which directly enters this activation and the decision conditions are marked, the activation can start. For instance, the first activation appearing as viewed from the top of the -flow in Fig. 10 indicates the activation of the valve VO., and the decision condition for opening this valve is the hold-up quantity equal to or smaller than a set value 1-HS. If this condition is fulfilled with the pump FO prepared, every flow directly entering this activation is marked, allowin~ the valve VO to be opened. Particularly, when the time-involved valve operation, such as the opening speed, is important, the activation may be indicated b.y the double broken line, with a time condition affixed between the two broken lines.

' 20 3 74 1 5 The aforementioned flow includes the flow of heat (indicated by the double real line as described before) and the flow of information in addition to the flow of a material such as a fluid of a mixed phase. As the information inc_Ludes information representing that the decision condition for hold-up control, the decision condition concerning the process flow, etc., the flow of information _is indicated by the broken line connecting the decision condition given in the brackets "[ ]" and the activation, the arrowhead showing the direction. Although the material flow and the heat flow are indicai~ed by the same types of lines as described before (see Fig. 3), they may be colored differently or expressed b,y- different lines for distinction.
The aforementioned marking is made in a manner such that when t;he decision conditions concerning a node having a f~~'.ow, the hold-up control, and the process flow are fulfilled, this node and the decision conditions are ~_ndicated with an increased brightness on the screen a~~ aforesaid. Instead of changing the brightness, color may be changed. Normally, when a valve is closed, the material flow (heat flow) through this valve is inhibited. In other words, the mark on the node, which is associated with the material flow (heat flow) and is joined to the flow created by the activation of tH~at valve, disappears. When there is a recycle loop of a material flow on the downstream side of the activation associated with the closed valve, the material flow in the loop may continue in some cases.
In this case, th,e mark on the node in the loop will not disappear.

The aforementioned sensor means 54 always monitors and checks whether or not the decision condition concerning the mold-up control and the state of the process flow is fulfilled. More specifically, the sensor means 54 always detects the liquid level of a hold-up or the hold-up quantity, the temperature or pressure at each position in the distillation column, the composition of a distillate, etc., and sends a detection signal_ through the I/O interface 50 to the control unit, 40,. From this detection signal, the control unit 40 determines whether or not the decision conditions associated with the hold-up control and the process flow are fulfilled.
The following is a description of how to perform the start-up operation of the plant activation display apparatus and how to determine the execution timing while monitorin~; the sequence graph. As the initial condition, a mai:erial is reserved in the material reserving tank HO and the hold-up quantity of the other hold-ups is zero. In addition, the preliminar,y-operation for the start-up of the pumps and reboiler RB
have already been completed, and the switching valves SVl and SV2 have been set to the state fll. Also, the pumps and valves can all be remote ly operated in response to an ON drive command signal sent to the drive device 52 from the control unit ~0 through the switching or ke~r operation of the input device ~2 of the plant activation display apparatus. It is to be understood, however, that the pumps and valves may be also manually operated as needed by operators, or may-be manually operated for the ON operation and automatically disabled by the control unit ~0 at the time of the OFF' operation or emergency shutdown operation.
Further, when the activation switch of the distillation column system is set ON, the hold-up 0-H
and the control condition [< 1-HS] are marked in the sequence graph on the screen of the display device 44.
The nodes 14 and 11 are also marked and emphatically indicated. An operator sets the operation switch of the pump PO ON after confirming the mark indication in the sequence graph. The valve V5 of the reboiler RB is opened when the hold-up quantity of the bottom tank H5 reaches a set value. Then, when the valve V3 is opened, the nodes 11 to 13 of the condenser CD are all marked. These valves V3 and V5 ma,y be activated at a preliminary openĀ°ation stage if such an operation is safe and entail: no problems on the apparatus.
Activating the pump PC also marks the pump node P C . A s a r a s a 1 t; , a v a r y f 1 o w g o i n g through activation to the valve VC ha.. been marked, satisfying all the decision conditions for the valve V0, so that the valve VO can be opened:. The control unit 40 sends the ON
drive signal through the drive device ~2 to the valve VO and opens the valve. Consequently, a material fluid flows from the reserving tank HO to the material supply tank H1, the hold-up node is emphasized or marked on the display screen.
The activation concerning the valve VI is held until a predetermined amount of the material fluid is supplied to the supply tank HI. At this time, the pump P1 is idling and is thus marked. tvhen the hold-up quantity of the tank H1 reaches a set value, the decision condition is marked and every flow going through - 3~ -activation has been marked. Consequently, the control unit ~0 sends the ON drive signal through the drive device 52 to the valve V1 and opens the valve. As a result, a flow t.o the next activation is formed, and every node up to each activation associated with the valves V6, V4 and V2 is marked. Actually, because no flow of the process fluid. S6 by the reboiler RB
substantially occurs unless the hold-up quantity of" the bottom tank H5 reaches the vicinity of a set value, the fluid dropping in the bottom tank H5 of the distillation column is reserved there.
When the hold-up quantity of the bottom tank H5 reaches the set value, the decision condition is marked. Confirming this mark, the operator activates the pump P4, marking every- flow going to each activation assoe:iated with the valve V2, and opening the valve V6. When the valve V6 is opened, the switching valve SV2 remains at the state (1) since the distillation co7_umn system has not reached the steady state yet. The fluid from the bottom tank H5 therefore returns to the ~>upply tank H1 through the reflex line 521.
When the hold-up quantity of the bottom H5 reaches the set value, the valve V6 of the reboiler RB is opened and heating of the process fluid by steam starts. The di~~tillate component then reaches the node 7 passing throe~;h the nodes 4, 3 and 2 in the named order, and is cooled and condensed there by cooling water. The resulting f.Luid flows in the reflex tank H8.
The activai:ion associated with the valves V~ and V2 is held unti7_ the hold-up quantity of the tank 118 - J ~ -reaches a set value [8-HS]. When the hold-up quantity reaches this set value, the pump P3 is activated and the valve V4 is opened. As a result, part of the distillate in the reflux tank H8 returns the supply tank Hl via the switching valve SV1, which is rendered in the state (1). The pump P2 is activated and the valve V2 is opened, permitting part of the distillate of the tank H8 t o return to the top. when the hold-up quantity of the tank H8 reaches the set value and all t h a d a c i s i o n c o n d i t i o n s indicate that the hold-up quantities and 1-H are equal to or greater than their respective s a t va 1 ue s , then the valve VO is closed and the apparatus is ready to shift t;o the steady-state operation in the circulation system.
The sensor means 5=~ always monitors the compositions, temperature, etc. of the bottom and top distillates. When the compositions (temperature or the like) of the distillates reach target values and the conditions #1 ar.:d #2 for the steady-state operation are fulfilled (YES), the associated switching valves SV1 and SV2 are switched to the state (2). As a result, the top and bottom distillates circulating to the hold-up node 1-H start being retained in the respective tank H9 and H10, and the mode shifts to the steady-state operation.
At the initial stage of the start-up operation, the process fluid is circulated by the circulation operation strategy until the compositions of the bottom and top distillates of the hold-up nodes 5-H and 8-H
reach the target values (temperature), thus shortening the start-up operation time.
To further ;shorten the start-up operation time, the valves VI, V4 and V6 may be disabled when the sensor means 59': detects that the compositions (temperature, etc.) of the bottom and top distillates have reached the set values, thus ensuring recycling of the distillate; of the bottom and top hold-ups H5 and H8 with the total reflux operation strategy. Also in this case, when the compositions (temperature, etc.) of the bottom and top distillates reach the target values, the valves V1, V4 and V6 are reopened, and the switching valves SVl and SV2 are set to the state (2), thus ensuring the transition to the steady-state operation.
Further, if products are put into the top and bottom hold-ups H8 and H5 before the start of the start-up operation, and if the start-up operation is started according to the total reflux system, the start-up operation time can be further shortened.
The start-up operation procedure can be described in brief with r~=ference to the flowchart of Fig. 11.
Various preparation jobs and the initialization of the control unit 40 are performed (step I). Then, it is determined whether or not the first decision condition Gi of the sequence graph is satisfied, and the process holds until the condition is fulfilled (step 2). When the decision condition Ci is fulfilled in step 2, the activation Ai is e:~ecuted (step 3).
The e:~ecution of the activation Ai creates a flow to the newt activation Ai+1, and the individual nodes up to the activation Ai+1 in the sequence graph are marked and emphasized. Then, the control variable _i is incremented by "1" in step 4. It is then determined whether or not i_ has reached a predetermined value Ni (step ~1, and the operation returns to step 2 to determine whether or not the decision condition for the next activation is fulfilled. 'The individual activations are sequentially executed in this manner.
When execution of the (?~i - 1)-th activation is completed, the c>peration advances to step 6 to trait for the transition-t,o-steady-state conditions #1 and ~2 to be fulfilled. 4~hen these conditions ~1 and n2 are fulfilled, the operation for the transition to the steady state is executed (step 7i, completing the start-up operation.
Sequence Graph for Shutdown Operation When the shutdown operation of the distillation column s,vstem i~~ performed after the steady-state operation, the aforementioned sequence graph for the start,-up operation can be used as it is. What should be considered For the shutdown operation are safety and the quality of i;he fluid remaining as a hold-up. 'the shutdocan operation is to inhibit part of the flow conditions for i~he steady-state operation included in the sequence graph for the start-up operation. Since the equipment required for the start-up operation can be used directl.~-, it may be unnecessary to provide a particular equipment for the shutdown operation, i.e., the structure of the equipment for the shutdown operation is t~hfy same as the one required for the start-up operat.p_on.
Thus, the shutdown operation procedure should only be sequentially executed according to the execution timing displayed on the screen of the display device ~4, using the sequence graph used for the start-up operation. In many cases, the shutdown operation procedure, unlike the start-up operation procedure, does not create the flow "from material supply to product."
In the case of the distillation column system of this embodiment, the valve V1 is closed and the pump P1 is activated to stop the supply of the raw material, then the valve V5 is closed to cutoff steam which has been supplied to the reboiler RB. At the same time, the switching valves SV1 and SV2 are set to the state (1) to suppress the top and bottom products and increase the amount of reflux. When the process fluid is sufficiently cooled down, the valve V3 for supplying cooling water is closed, thus completing the shutdown operation.
The operation procedure and e~cecution timing can be indicated on~~ after another to the operator if the subsequent activations are sequentially blinked using the same sequence graph as used for the start-up operation.
Seguence Graph :Por Emergency Shutdown Operation In general., since safety has the highest priority in the emergency shutdown operation procedure, equipment designed for emergency shutdown is often added to the plant for safety's sake, and the operation sequence graph is prepared in accordance with the added line configuration. The additional equipment may be one for dischar~;in~' the fluid from the main plant component or one' for supplying sealing gas for prevention of explosion. Although the emergency shutdown operation procedure, in contrast with the case of the start-up operation, never creates the flow "from material supply to product," it may be represented by the same method for the shutdown operation. Although a line for fluid transportation should be added to the main process line to supply an additional fluid or eliminate the process fluid, the additional line basically can be expressed by the same way as used for the start-up operation, facilitating the preparation of the sequence graph. To permit the additional equipment to forcibly discharge the process fluid, it is preferable to give particular consideration to the distinction bet~.~een the node at where the main process line is ,joined to the discharging equipment, and other nodes by means of affixing special symbols, coloring or the like.
The aforementioned plant activation display apparatus can ensure fully automatic start-up and shutdown operations if all the pumps and valves are driven under the control of the electronic control unit 40. That is, the plant activation display apparatus of the present invention can be used as an automatic operation apparEitus.
Lse as Simulation Support Apparatus The plant activation display apparatus according to the above-de=scribed embodiment of the present invent.i.on, as applied to a distillation column system, is effective not; only as an apparatus to inform an operator of the start-up, shutdown, or emergency-shutdown operation procedure and execution timing of a real model, but also as a design support tool to design a plant in the 7.ight of the operation procedure and the execution ti.min~;. This plant activation display apparatus is also effective as a simulation support apparatus for training operators to how to operate the real mode.
To use the plant activation display apparatus as a simulation apparatus, the sensor means 54 of the plant activation display apparatus shown in Fig. 2 should only be replaced with a simulation signal generator, which generates pseudo signals indicative of status quantities, such as the flow rate, pressure, temperature, composition, etc. of the process fluid at various points in the distillation column, the reboiler RB and the condenser CD, or in the hold-ups, the generator being connected to the control unit ~0 through the I/O interface 50. When the pumps and valves are oper<~.ted, changes in the status quantities of the process fluid caused by the operation are estimated and supplied to the control unit 44 in succession.
Also when the plant activation display- apparatus is used as the simulation apparatus, as in the aforesaid case where it is applied to the real model, the evaluation of the activation performance, such as the operating ei.-'ficiency of the designed plant, and the study or learning of the plant operation can be facilitated by displaying the sequence graphs on the screen of the display device 44, and operating the apparatus accorclin.~ to the instructions of the emphasized activations.
Second Embodiment The sequence graph displayed on the screen of the plant activation display apparatus of the present invention can be also applied to a combined unit which is formed of a plurality of units. If the basic units are of high modularity, in particular, the graph can be - 2~ 374 1 5 applied more easily. Since the structure of the plant corresponds to the procedure of operation, changed portions of the operation procedure can be cleared up correspondingly by detecting modified structure portions necess.&ry for the connection of two units.
The following is a description of a distillation column system with a heat pump according to a second embodiment, as an e:cample of the aforesaid arrangement.
In Fig. 12, like reference numerals used to denote the lines (fluid paasages) of the first embodiment refer to corresponding fluids.
Line Configuration of Heat Pump The distillation column system of the second embodiment is a combined system obtained by connecting a heat pump HP, which uses water as a working fluid (heat transfer medium), to the distillation column system of the first embodiment. Fig. 12 shows a line configuration~o:E a heat pump unit applied to this distillation co:Lumn system.
The heat pump HP includes two heat e~cchangers (side cooler and side heater) SC and SH which are falling film-type heat e:cchangers. The side cooler SC
removes condensation heat from a process fluid, and gives the heat i:o the water for use as a working fluid, thereby vaporizing the water. The side heater SH gives condensation heat from the working fluid to the process fluid, thereby evaporating part of the process fluid.
Hold-ups H5~ and H54 for collecting the cast working fluid are attached to the bottom portions of the side cooler SC and the side heater SH, respectively. The heat pump HP is provided with compressors C1 and C2 for boosting the temperature of the vaporized working fluid and a decompre;>sor V51, besides the heat exchangers.
To increa=~e the wet area of their heat transfer surfaces, the ~;ide heater SH and the side cooler SC are provided with a~ process fluid circulation line S44 and working fluid circulation lines S52 and S53, respectively. Each combination of circulation pump and valve P41, V41, and P50, V52, and V53 is arranged in the individual circulation line.
A line for introducing the working fluid (water) is required as preliminary equipment for the operation of the heat pump HP. For example, a fluid injection pipe S51 is attached to the side cooler SC. The working fluid is heated to be evaporated by means of the process fluid in the side cooler SC, and is then delivered to th~= side heater SH through the compressors C1 and C2. In the side heater SH, the working fluid is condensed and collected in the hold-up H54. A pipe S60 for reducing starting load is required for smooth activation of the compressors C1 and C2. The pipe S60 is provided with a valve V54 which closes the pipe S60 during the steady-state operation. Drain lines S65, S66 and S67 are provided to be used to remove the working fluid condensed around the compressors C1 and C2. Further provided are exhaust lines S61, S62 and S63 for removing air introduced into the heat pump HP
and a working fluid sprayer (S64, V53? for prevention of superheating.
Modification of Line Configurations of Distillation Column & Heat Pump The heat pump HP is disposed in an intermediate stage between the condenser CD and distillation column D of the first embodiment so that the two heat 20 37 ~+ 1 5 - ~3 -exchangers SC and SH are individually in contact with the column-side process fluid across their respective heat transfer surfaces. 'Therefore, the distillation column D and the heat pump HP require a structural mod:ificati.on for the connection between them. 'table 4 collectively shows the details of ,junctions between the distil_lat;ion column D and the heat pump HP.
Table 4 Distillation Column Side HP side (phase of fluid) (phase of fluid) 1) Column top output (Gi ~ SC input (G) Reflux tank input (L) E- SC output (L) Condenser input (G) ~ SC output (G) 2) Intermediate stage of recovery section Output (L) ~ SH input (L) Input (L) E SH output (L) Input (G) E SH output (G) In consideration of the relationships between the respective height positions of the two opposite ends of each connecting line, it is necessary only that a pump P42 and a valve V43 be arranged in a line S~7 on the output side of the side cooler SC, a pump P40 and a valve V40 be arranged in a line S41 on the process-flu:id input side of the side heater SH, and pipelines for associated utilities be added, fol.~ use as necessary transportation apparatuses.
Line Configuration for Start-Up Operation The following is a description of a necessary line configuration for the start-up operation of the distillation column system with the heat pump. First, the circulation system described in connection with the first embodiment is used, and in this case, piping is required to return the products from t;he top and bottom of the column to a material supply tank Hl.
A hold-up 33-H is provided between the top of the column and the node 7 in addition to the hold-up of the distillation column system according to the first embodiment. The hold-up 33-H is used to receive the process fluid flowing down from the top side of the distillation column, and deliver it to the side of the heat pump HP.
Based on this situation, Fig. 13 shows a structural representation of a distil7_ation column system modified for the connection of the heat pump HP, and Fig. 14 shows a structural representation of the heat pump HP. In these drawings, like reference numerals used to denote the components of the distillation column system according to the first embodiment refer to like or corresponding components.
Preparation of ~~eguence Graph (Representation of Fluid Connections and Conditions for Flow Control in Distillation Columnl Table 5 shows fluid connections and conditions for and flow control during the start-up operation on the distillation column side, similar to the ones shown in Table l, arranged by the same method as the one described in connection with the first embodiment.

m ~~ c SO ( 0-H - 1-H . L . FO . VO ) .

S1 ( 1-H -~3 . L . . P1 . V1 ) S ( 2 - 3 . L . . ) 2 .

S3 ( 3 ->30 . L . . ) .

S3' ( 32 -~~ . L . . ) .

S4 i 4 - 5-H . L . . ) .

S5 ( 5-H -~6 . L . . ) .

S ( 6 - 4 . L&V . . ) 6 .

S7' ( 4 -~32 . V . . ) .

S7" ( 32 - 31 . V . . ) .

S7"'( 31 -~30 . V . . ) .

S7 ( 30 - 3 . V . . ) .

S ( 3 -~2 . V . . ) 8 .

S9 ( 2 -~33-H . V . . ) .

S9' ( 33-H-~i . V . . ) .

S10 (7 -~8-H . L . . ) .

S ( 8-H -~2 . L . P2 . V2 ) 11 .

S12 (8-H -~18 . L . P3 . V4 ) .

S13 (18 -~9-H . L . . SV1(21) .

S14 (5-H -~17 . L . P4 . V6 ) .

S15 (17 -j10-H . L . . SV2(2)) .

S16 (11 -~12 . L . . V3 ) .

S17 (12 -~13 . L . +E1 . . ) S18 (14 -~15 . V . . V5 ) .

S19 (15 -~16 . L . -E2 . . ) S20 (18 -~1-H . L . P4 . SV1(1)) .

S21 (17 -~1-H . L . . . SV2(1)) Table 5 differs from Table 1 only in that fluids S?', S'7" , Si"', S3', S9, and S9' are added or modified.

2037~1~
- ~6 -(Transition to Steady-State Operation) Switching from the start-up operation to the steady-state operation on the distillation column side is achieved i.n the following manner.
When all the hold-ups fulfill their set values during the start-up operation, the valve V1 is closed to stop the material supply, and at the same time, the valves V4 and V6 are closed so that the transition-to-steady-state conditions #1 and #2 are fulfilled in accordance with the full reflux system. When the conditions #1 and #2 are fulfilled, the operation shown in Table 6 is executed.
m.,,-., ~ c S13 (18 -~ ~a-H . L . . . SVl(2)) S15 (17 -~ l'.0-H . L . . . SV2(2)?
More specifically, the lines S13 and S15 are opened, while the lines S20 and S21 are closed. The transition-to-steady-state conditions #1 and #2 may alternatively be set so that excesses of the column bottom and top temperatures over their respective set values (T1i > Tlis, T18 > T18S) can be discriminated thereby.
(Representation of Fluid Connections and Conditions for Flow Control in Heat Pump) The following is a description of preliminary operations for the operation of the heat pump HP.
Preliminary Operation 1 (in.jection of working fluid):
In this operation, a valve V50 of a line S51 i_s opened, and the working fluid is injected into a hold-- 4r -up H55. When the working fluid is collected to a required amount, the valve V50 is closed (see Fig.
16A).
Preliminary Operation 2 (heat exchanger circulation):
In this operation, the pump P50 is actuated, and the valve V52 is opened to allow the working fluid in the hold-up H55 of the side cooler SC to circulate.
Also, the pump P41 is actuated, and the valve V41 is opened t.o allow the working fluid in the hold-up H54 of the side heater SH to circulate. As t;he working fluid ci.rcu7_ates in this manner, its wettability on the heat transfer surfaces increases, so that the heat transfer efficiency of the system is improved (se<> Fig. 16B).
Preliminary Operation 3 (construction of compressor circulation line):
This operation should be performed before the activation of the compressors. The valve V54 is opened, the discharge side of the compressor C2 is communicated to the intake-side of the compressor C1, and the load for starting the compressors is reduced (see Fig. 16C).
Preliminary Operation 4 (construction of drain Line):
This operation should be also performed before the activation of the compressors. A valve V56 on the discharge side of the first compressor C1 and a valve V55 on the discharge side of the second compressor C2 are opened to discharge the working fluid (water) from the compressors into the hold-up H55 (see Fig. 6D) Preliminary Operation 5 (ventilation):
This operation should be also performed before the -4g-activation of the compressors. Valves V57 and 1'58 a:re opened, and air in the heat pump HP is discharged by means of an ejector EJ (see Fig. 16E).
Preliminary Operation 6 (construction of superheating protection line):
This operation is executed when t:he outlet temperature of the compressor C2 exceeds a specified temperature. A valve V53 is opened, and the working fluid (L) in the hold-up H55 is sprayed into the line between the compressors C1 and C2 through the aforesaid circulation line of the side cooler SC',. Thus, the working fluid is prevented from being superheated (see Fig. 16F).
These preliminary operation sequence graphs, as well as the one shown in Fig. 16 (mentioned later), can be displayed on the screen of the display device 44, and if necessary, these preliminary operations can be introduced as decision conditions for the activation into the sequence graphs. Generally, it is advisable to complete many of these preliminary operations before the first activation associated with the heat pump H-P
appears, as shown in the sequence graph of Fig. 16.
Table i shows fluid connections and conditions for flow control during the start-up operation in the heat pump and auxiliary lines, arranged in the same manner as in Table 1.
Table ~ (Process fluid in heat pump HP and flow conditions in auxiliary lines) S40 ( 30 -~ 40-H . L . . . ) S41 (40-H =~ 41 . L . . P40 . V40) S42 ( 41 -> 42-H . L . . . ) r 2037415 S43 (42-H -~43 . L . . P41. ) S44 ( 43 -~41 . L . . . V41 ) S45 f 43 -~32 . V . . . V42 ) S46 f42-H -~43 . L . +E50 . ) .

Table Workin~; fluid inheat pump HP and flow i ( conditions auxiliary lines) in S50 (54-H -~55-H L . -E50 . v51) . .

S51 f58 -~55-H L . . . V50) .

S52 (55-H -~56 . L . . P50. V52) S53 (56 -~55-H L . . . ) .

S54 (55-H -~5i . V . +E51 . ) .

S55 ( 57 -~50 . V . . . ) S56 (50 -~51 . V . . Cl . ) S5 i ( 51 -~52 . V . . . ) S58 (52 -~53 . V . . C2 . ) S59 (53 -~54-H V . . . ) .

S60 (53 -~57 . V . . . V54) S61 ( 53 -~60 . V . . . V57 ) S62 (59 -j60 . V . . . V58) S63 ( 60 -~61 . V . . . ) S65 (50 -~63 . L . . . V56) S66 ( 52 -~.63 . L . . . V55 ) S67 (63 -~55-H . . . . ) L

(Conditions for Transition to Steady-State Operation of Heat Pump) The operation mode of the heat pump HP is switched from the start-up operation to the steady-state operation as th<~ valve V54 of the circulation line S60 is gradually closed when the working fluid temperatures in the hold-ups H54 and H55 exceed set values T54S and _ ~0 _ T555, respectively (T54 > T54S, T55 > TSbs).
When supplied with the fluid connections and conditions for flow control shown in Tables 4 to 7, the electronic control unit 40 creates sequence graphs for the distillation column and the heat pump in the same manner as aforesaid. Figs. 15 and 16 show the sequence graphs for the distillation column D and the heat pump HP, respectively.
Fig. 17 shows a line configuration of the combined system obtained by superposing two junctions of the heat exchangers shown in Figs. 13 and 14. Fig. 18 is a sequence graph for this combined system, which can be represented by superposing the .junctions, as in the case of the sup.=rposition of the line configurations.
This sequence g:caph, which incorporates the sequence graphs of Figs. 16A to I6F for the preliminary operation of the heat pump HP, represents the procedure and execution timing for the start-up operation of the whole system.
Thus, the sequence graphs of the plant activation display apparatus according to the present invention correspond to the line configurations in the operation procedure and execution timing. Accordingly, modifying the line configurations and combining the units can be effected very easily.
In the start-up operation of the combined system, as described before with reference to Fig. 11, it is necessary only that activations be successively executed from the inlet node side, in the same manner of the first embodiment. The start-up operation of the heat pump HP is finished by closing the circulation line 560. In this case, heat exchange between the -~1_ X037415 working fluid ar,~d the process fluid starts before the line S60 is closed. Thus, the target function or compressing effect of the heat pump unit can be fulfilled by cutting off the circulation line S60 ,Then the working fluid is preheated to a certain temperature. The sequence graph of Fig. 18 represents the steps of operation procedure before the transit;ion to the steady-state operation of the heat pump HP and the timings therefor, as well as the order of the operation timings on the heat pump side and on the distillation column side. In the sequence graphs of Figs. 15, 16, 16A to 16F, and 18, the display of the specific decision conditions for the execution of activation .is omitted. Actually, however, all the necessary decision conditions are to be described i.n the brackets ( J.
In the sequence graphs of the plant activation apparatus according to the present invention, the flow directions correspond to the time axis. The speed of the process fluid flowing between the nodes and the time elapsed before the hold-up quantities attain the set values can be estimated from simple operational expressions or empirical values. Shortening time elapsed for the start-up operation can be facilitated by arranging the steps of procedure and execution timing for the start-up operation in a time series based on the sequence graphs. If the operation times for the valves and the pumps in the sequence graphs are fetched and rearranged on the time series basis, for example, time elapsed for individual steps of the start-up operation can be more clearly indicated.
Fig. 19 shows the operation times of the valves - ~ 2037415 after the starting time for the start-up operation of a positive pilot plant based on the sequence graph of Fig. I8, that is, the times for the start of individual activations and transitions to the steady-state operation, arranged on the time series basis.
The configuration and operating conditions of this positive pilot plant are as follows:
The distillation column D is a packed column (column section? with a diameter of 200 mm and height of 5,000 mm, and a 1-inch mini-cascade ring is used as a packing, whose packing height is 4,000 mm. The process fluid to be separated in the column is a mixture of ethanol and water. As a result of an experiment, it is ascertained that the theoretical number of stager corresponding to a plate-column of the target packed column, including the reboiler RB, is 11.
The material is supplied to a seventh stage counted from the' column top as a first stage. A side-cut plate for fe>eding the process fluid to the side heater SH of the> heat pump HP corresponds to the eighth plate of the di~~tillation column D. The reboiler RB of the column D ha,. a heat transfer area of 2.0 m2, and steam of 2.0 kgfG/cmz is used as a heating utility. In the reboiler RB, heat exchanges of about 40 kW and 16 kW are made during the start-up operation and steady-state operation, respectively.
The condenser CD of the distillation column D, whose heat transfer area is 4 m2, uses water as a cooling utility. Table 8 shows the principal specifications of the distillation column of the pilot plant.

2034 ~5 T .. 1. , _ U
Type : Packed co7_umn Diameter: 200 mm Height of packed zone: 4,000 mm Theoretical number of plates: 11 Reboiler hold-up: 70 liter Reflux tank hold-up: 40 Liter The heat pump HP, which is of an indirect compression t,ype~, uses water as a working fluid. The compressors C1 and C2 are rotary compressors, which are used in series with each other, enjoying a great difference in compression temperature. Further, each compressor is provided with an inverter for load adjustment.
The two heat exchangers, that is, the side heater SH and the side cooler SC, which constitute a section through which hE~at is delivered to or from the distillation column D, are of a falling-film type.
Thus, these heat, exchangers can satisfactorily exchange heat energy despite a relatively small temperature difference from the process fluid. Table 9 shows the principal specifications of the heat pump of the pilot plant.
Table 9 Type: Indirect compression type Working fluid: Water Compressor type: 2-stage rotary type compressors Heat exchanger type: falling film type Heat transfer area of SH: 3.43 m2 Heat transfer area of SC: 5.14 m2 SH:
Processing fluid hold-up: 20 liter Working fluid: 7 liter SC:
Processing fluid hold-up: ? liter Working fluid: 20 liter This pilot plant was brought to a stand-by state for the transition to the steady-state operation of the distillation co:Lumn when the heat pump HP was switched to the steady-sl=ate operation, that is, in 246 minutes after the start of the start-up operation. The whole system entered t:he steady-state operation in 376 minutes after the start of the start-up operation.
Thus, by operating the plant in accordance with the sequence graphs displayed by means of the plant activation display apparatus according to the present invention, the plant was able to be activated stably and securely to a target state.
In the first and second embodiment described above, the start-up operation procedure is composed of the ideas of "flow control" and "hold-up control," as the basic concepts, plus "operation mode modification conditions" and "transition-to-steady-state conditions"
as required. In many cases, it is preferable that the execution timing is adjusted by using variables, such as the temperature, pressure, and composition of the process fluid in a suitable position, instead of depending solely on the hold-up state. Further, an operating condition for avoiding risky operating conditions may- be additionally used. In any cage, the plant operation can be made flexible by adding these conditions to the decision conditions for the activation.
According t.o the second embodiment, it was verified that the use of the pilot plant enables a securer plant ox>eration. Since the completion of the start-up operation took 376 minutes, however, there is yet room for improvement in this arrangement.
Thereupon, the operation procedure was improved. Table shows time elapsed for accumulating desired hold-up quantities after the valve operation times shown in Fig. 19.
m~t,n ._ i n Hl Material supply tank: 5 min.
.

H5 Bottom tank: 20 min.
.

H8 Reflux tanlt: 70 min.
.

H65: Side cooler hold-up: 2 min.

H54: Side heater hold-up: 15 min.

Heat pump preheating time: 80 mi_n.

Stand-by time for transition to 130 min.
steady-state operation:

The time elapsed for fluid supply to the bottom tank H7 at the column bottom can be shortened by preliminarily supplying the tank Ho caith the bottom product before the start of the start-up operation. In this case, it is necessary to additionally use a line for supplying the bottom tank H5 with the bottom product.
The time elasped for preheating the heat pump HP
can be shortened if the pump HP is preheated while the working fluid is being introduced into the side cooler SC' as a preliminary operation for the pump. In this case, the side c:ool.er SC should be additionally provided with a steam supply line.
The time elasped for fluid supply to the reflux tank H8 at the column top can be shortened by preliminarily s~:~pplying the tank H8 with the top product before the start of the start-up operation.
Also in this ca~~e, it is necessary to additionally use a line for supplying the reflux tank H8 with the top product.
When the aforementioned positive pilot plant was started up after these improvements in lane configuration and operation procedure, the start-up operation time required before the start of the steady-state operation was able to be reduced to 168 minutes.
Fig. 20 clearly shows the operation timing for each valve. If' the valves are operatE~d not by remote control but by operators at the ,job site, the stationing of the operators, valve arrangement, etc.
can be easily achieved in consideration of the efficiency of tree valve operations at the site. More specifically, the timing chart of Fig. 20 and the 7_ine configuration are collated with each other for the allotment of the individual valve operations to the operators, or for optimum location of the valves in the case of a one-man operation. These operations can be performed with ease because the plant design definitely corresponds to the plant operation and the timing therefor, based on the sequence graphs of the plant activation display apparatus of the present invention.
(Sequence Graph for Shutdo~.rn Operation) The shutdown operation procedure for the - 5i -distillation column system with the heat pump HP can be also decided on the basis of the sequence graph of Fig.
18.
In performing the shutdown operation, the material-supply and the =_~upply of steam to the reboiler RB are first stopped. As the steam supply is stopped in this manner, vapor ceases to be generated from the reboiler RB. If the heat; pump HP is operating, however, the process fluid c~~n also circulate, so that the pump HP
is finally stopped.
The shutdo~~rn operation procedure and timing (operation sequence? can be set in the same manner as in the case of the first embodiment. Alternatively, however, these factors may be represented by gradually lowering the brightness of the activation displayed on the screen of tl-,e display device 44, using the sequence graph for the start-up operation.
(Sequence Graph for Emergency Shutdown Operation) Also in the second embodiment, equipment designed for emergency shutdown, such as a seal gas supply system, emergency removal line for the process fluid, etc., may be added as required to the plant for safety's sake, in the manner described in connection with the first embodiment. It is necessary only that an operation sequence be set in consideration of the added equipment, as in the first embodiment. Also in this case, the ~~etivation can be displayed on the screen of the display device 44 in the same manner as in the shutdown operation. If the emergenc,v shutdown equipment is adc'.ed, its operation only requires emergency shutdown conditions and its operation sequence to the activation decision conditions.

Otherwise, the operation is performed in the same manner as the shutdown operation.
It is to be understood that the plant activation display apparatus according to the present invention is not limited to the distillation column systems of the first and second embodiments described herein, and that the invention ma.,y be also applied to various other chemical plants. There are several methods for representing sequence graphs for other plant components as follows.
Fig. 21 shows an evaporator, in which a process fluid is heated to be evaporated by means of a heat exchanger' H.EX1 which uses steam as a utility. The evaporated process fluid flows from the evaporator to a line S80, while a liquid collected in the evaporator flows out into a, line 581. Fig. 22 shows its sequence graph for the evaporator.
Fig. 23 shows a configuration of a self-heat exchanging reactor, in which a reactive mixed process fluid reacts and. generates reaction heat. The reactor R comprises two heat exchangers HEX2 and HEX3. The heat exchanger H:EX2 uses steam as a heat transfer medium to preheat the process fluid which reacts in the reactor R. In the heat exchanger HEX3, the process fluid heated to high temperature by the reaction heat generated in the reactor R heats the process fluid itself flowing into the reactor R. Fig. 2~ shows a sequence graph for the self-heat exchanging reactor.
The following is an illustration of the wa,y of representing fluid connections and conditions for flow control obtained when phase changes are caused at nodes by crystallization, flash, liquefaction under pressure, or sedimentation, separation.
Crystallization Table 11 S90 (N1 ~ P~t2 . L . . . ) S91 ( N2 -~~ PJ3 . L+S . -E . . ) Table 11 ir..dicates that a process fluid S90 in the liquid phase L is cooled to be partial_Iy crystallized at a node N2, thus forming a process fluid S91 containing portions in the solid phase S and the liquid phase L.
Flash Table 12 S92 ( N5 ~ PJ6 . L . . . ) S93 ( N6 -> t~'7 . L . -P . . ) S94 (N6 ~ N8 . V . -P . . ) Table 12 indicates that a process fluid S92 in the liquid phase L is decompressed to be partially vaporized at a node N6, thus forming a process fluid S9~ in the gas ~~hase V and a process fluid S93 in the Liquid phase L.
Liquefaction under Pressure Table 13 S96 (N10 -~ N11 . V . . . y S97 (N11 -~ N12 . L . +P . . ) Table 13 indicates that a process f_Luid S96 in the gas phase V is pressurized to be condensed at a node 2~37415 N11, thus forming a process fluid S9i in the liquid phase L.
Sedimentation Separation Table 1~
S88 (N14 ~ N15 . L+S . . . ) S 8 9 ( N 15 -~ '~i 16 . L . . . ) S90 (N15 -~ N17 . L+S . . . ) Table 14 indicates that a fluid S88 enters a node N15 in the form of a slurry, whereupon it is divided into two phases, the liquid phase L and the slurry phase (L + S). These two divisions emerge from the node N15 in the form of a fluid S89 and a fluid 590.
Supply of Proce~,s Fluids ~ & B
a chemical plant may be operated in different wars without changing; its configuration. When process fluids A and B a.re supplied to a tank 100, as shown in Fig. 25, the following different methods may have to be used depending an the processes to be executed.
According to the first supply method, the process fluid A is first supplied to the tank 100. When the resulting hold-u.p quantity attains a set value [> 100-HS], the process fluid B is then supplied to the tank 100. Fig. 26 shows a sequence graph for this case, in which a hold-up quantity condition [> 100-HS] is added to an activation condition for a valve V102.
.According to a second supply method, the process fluids A and B are simultaneously supplied to the tank 100. Fig. 2r shows a sequence graph for this ease, in which the condition that both of preliminary operations for the fluids A and B are finished is added to activation conditions for valves VI01 and V102. Thus, the moment the preliminary operations for the process fluids A and B 2.re both finished, the valves 101 and VI02 are simultaneously opened. The sequence graph of Fig. 2i can be rewritten into the one shown in Fig. 2$
according to a conventional method of sequence graph representation. This sequence graph also indicates that the valves V101 and V102 are opened in synchronism with each other.
Although the sequence graphs are displayed on the screen of the display device ~4 in the embodiments described above, they may be printed out by means of the printer ~6. Alternatively, as shown in Fig. 2, the activation display apparatus may be distributively connected to a distributed control system (DCS1 49 for each plant so that the aforementioned sequence graphs are delivered as required from the central electronic control unit 40 to the display apparatus in the plant, thus constituting part of the control system.

Claims (23)

1. A plant activation tracking and display apparatus for use in a plant in which a plurality of points of plant components are represented by a plurality of nodes including at least one system input node through which an input fluid is externally supplied to the plant, and at least one system output node, through which an output fluid flows out from the plant, adjacent nodes of said plurality of nodes being connected by means of fluid passages, at least some of said fluid passages having at least one transportation means and/or valve means for creating a fluid flow in a specified direction, the apparatus further comprising:
an output device including:
means for categorizing all fluids flowing through said fluid passages, when the plant is in operation at a steady-state condition, in accordance with type and phase of said fluids, means for successively tracking categorized fluids with a specified phase over said plurality of nodes from said system input node to said system output node, and display means for sequentially displaying arrays of tracked nodes of said plurality of nodes in one direction;
memory means for previously storing data which correspond to operating conditions for each said transportation means and/or valve means;
sensor means for sensing the operating conditions for each said transportation means and/or valve means to determine whether the operating conditions for each said transportation means and/or valve means are fulfilled; and output device control means for successively determining whether said operating conditions for each said transportation means and/or valve means are fulfilled, starting from the system input node side, and for causing the output device to make an emphatic indication that each said transportation means and/or valve means be operated when said conditions thereof are fulfilled, and to make a further emphatic indication of only fluid passages between nodes through which fluid is caused to flow by the operation of each said transportation means and/or valve means.
2. The plant activation tracking and display apparatus according to claim 1, wherein said plant components include a heat exchanging component, and at least one of said plurality of nodes is connected to a node of said heat exchanging component through energy transfer, said heat exchanging component being displayed on the output device adjacent to a display of energy transferring nodes in parallel relation therewith.
3. The plant activation tracking and display apparatus according to claim 2, wherein the fluids flowing through the fluid passages connected to a node which exchanges energy with the node of said heat exchanging component are identically categorized fluids if said fluids change in phase around the node which exchanges energy with the node of said heat exchanging component.
4. The plant activation tracking and display apparatus according to claim 1, wherein said plant components include a hold-up device to be displayed as one node.
5. The plant activation tracking and display apparatus according to claim 1, wherein said output device comprises an image display device.
6. The plant activation tracking and display apparatus according to claim 1, wherein said output device comprises a printer.
7. The plant activation tracking and display apparatus according to claim 1, wherein said plant comprises a plurality of plant units.
8. An automatic plant operation apparatus comprising the plant activation tracking and display apparatus according to claim 1, and drive means for driving said transportation means and/or valve means when the operating conditions thereof are fulfilled.
9. A plant activation tracking and display apparatus for evaluating plant activation through simulated operation of a plant in which a plurality of points of plant components are represented by a plurality of nodes including at least one system input node through which an input fluid is externally supplied to the plant, and at least one system output node through which an output fluid flows out from the plant, adjacent nodes of said plurality of nodes being connected by means of fluid passages, at least some of said fluid passages having at least one transportation means and/or valve means for creating a fluid flow in a specified direction, the apparatus further comprising:
an input device for producing a data signal through external input operation;
an output device including means responsive to the data signal delivered from said input device, for categorizing all fluids flowing through said fluid passages when the plant is in operation at a steady-stage condition, in accordance with a type and a phase of said fluids, for successively tracking categorized fluids with a specified phase over said plurality of nodes from said system input node to said system output node, and for sequentially displaying arrays of tracked nodes of said plurality of nodes in one direction;
memory means for previously storing data corresponding to operating conditions for each said transportation means and/or valve means in response to the data signal delivered from said input device;
simulation signal output means for outputting a simulated signal for simulatively making said operating conditions for each said transport means and/or valve means fulfilled to desired operating conditions; and output device control means for successively determining whether said operating conditions for each said transportation means and/or valve means are fulfilled, starting from the system input node side, depending on the presence of the simulated signal output from said simulation signal output means, and for causing the output device to make an emphatic indication that each said transportation means and/or valve means be operated when said operating conditions thereof are fulfilled, and to make a further emphatic indication of only fluid passages between nodes through which fluid is caused to flow by the operation of each said transportation means and/or valve means.
10. The plant activation tracking and display apparatus according to claim 9, wherein said plant components include a heat exchanging component, and one of said plurality of nodes is connected to a node of said heat exchanging component through energy transfer, said heat exchanging component being displayed on the output device, adjacent to a display of energy transferring nodes in parallel relation therewith.
11. The plant activation tracking and display apparatus according to claim 10, wherein the fluids flowing through the fluid passages connected to a node which exchanges energy with the node of said heat exchanging component identically categorized fluids if said fluids change in phase around said node which exchanges energy with the node of said heat exchanging component.
12. The plant activation tracking and display apparatus according to claim 9, further comprising command means for outputting a pseudo command signal for manually controlling a specified transportation means and/or valve means through human manipulation, said manually controlling including one of activating and stopping, and wherein said output device control means causes the output device to make an emphatic indication of only fluid passages between nodes through which new fluid is caused to flow when said specified transporation means and/or valve means is manually controlled, in response to the pseudo command signal from said command means, and to make a further emphatic indication that each said transportation means and/or valve means be operated when the operating conditions thereof are changed due to new fluid flows.
13. The plant activation tracking and display apparatus according to claim 9, wherein said plant components include a hold-up device to be displayed as one node.
14. The plant activation tracking and display apparatus according to claim 9, wherein said output device comprises an image display device.
15. The plant activation tracking and display apparatus according to claim 9, wherein said output device comprises a printer.
16. The plant activation tracking and display apparatus according to claim 9, wherein said plant comprises a plurality of plant units.
17. The plant activation tracking and display apparatus according to claim 2, wherein said plant comprises a plurality of plant units.
18. The plant activation tracking and display apparatus according to claim 3, wherein said plant comprises a plurality of plant units.
19. The plant activation tracking and display apparatus according to claim 10, wherein said plant comprises a plurality of plant units.
20. The plant activation tracking and display apparatus according to claim 11, wherein said plant comprises a plurality of plant units.
21. The plant activation tracking and display apparatus according to claim 1, wherein at least one of said nodes has a fluid flowing out from said at least one of said nodes, said fluid returning along a flowing direction which is identical in phase through at least one fluid passage to said at least one of said nodes.
22. The plant activation tracking and display apparatus according to claim 1, wherein said transportation means and/or valve means is provided in an intermediate portion of each of said fluid passages.
23. The plant activation tracking and display apparatus according to claim 9, wherein said transportation means and/or valve means is provided in an intermediate portion of each of said fluid passages.
CA 2037415 1991-03-01 1991-03-01 Plant activation display apparatus Expired - Fee Related CA2037415C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CA 2037415 CA2037415C (en) 1991-03-01 1991-03-01 Plant activation display apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CA 2037415 CA2037415C (en) 1991-03-01 1991-03-01 Plant activation display apparatus

Publications (2)

Publication Number Publication Date
CA2037415A1 CA2037415A1 (en) 1992-09-02
CA2037415C true CA2037415C (en) 2000-10-31

Family

ID=4147104

Family Applications (1)

Application Number Title Priority Date Filing Date
CA 2037415 Expired - Fee Related CA2037415C (en) 1991-03-01 1991-03-01 Plant activation display apparatus

Country Status (1)

Country Link
CA (1) CA2037415C (en)

Also Published As

Publication number Publication date
CA2037415A1 (en) 1992-09-02

Similar Documents

Publication Publication Date Title
US5241296A (en) Plant activation tracking and display apparatus
Wolff et al. Operation of integrated three-product (Petlyuk) distillation columns
CN102405389A (en) Method and apparatus for cooling down a cryogenic heat exchanger and method of liquefying a hydrocarbon stream
Floudast Synthesis of heat integrated nonsharp distillation sequences
Dimian et al. Pinch point analysis
Caxiano et al. Eco-efficiency analysis and intensification of the acetic acid purification process
CA2037415C (en) Plant activation display apparatus
CN101600517A (en) Regenerating unit and renovation process
SE434989B (en) PROCEDURE FOR IMPROVING THE ENERGY TRANSMISSION AND THE PREPARATION OF THE PROCEDURE IN A PRESSURE STEP EXCHANGER
Eden et al. Dynamics and control during startup of heat integrated distillation column
Patle et al. Plantwide control and process safety of formic acid process having a reactive dividing-wall column and three material recycles
Manenti Natural gas operations: Considerations on process transients, design, and control
CN1211606C (en) All-range water supply control system for boosting steam generator of water reactor
Hunt et al. The propagation of faults in process plants: 6, overview of, and modelling for, fault tree synthesis
JP3058435B2 (en) Plant operation display
US5784538A (en) Process and apparatus for predicting and controlling flood and carryover conditions in a separation column
Luyben Dynamic simulation of flooded condensers
AU772839B2 (en) Method for continuously monitoring and controlling the monomer conversion during emulsion polymerisation
Paules IV et al. Synthesis of flexible distillation sequences for multiperiod operation
FI75681C (en) Structural design of product plants and decentralized control.
JP3834501B2 (en) Distillation tower and start-up method of distillation tower
Jantzen Fuzzy supervisory control
Naka et al. Computer-Aided Process Design System for Plant Operation
JPH01265301A (en) System control method
Yang Dynamic simulation and optimization for flare minimization and safety operation

Legal Events

Date Code Title Description
EEER Examination request
MKLA Lapsed