CA1206432A - Treating beer to prevent chill haze while preventing metal contamination - Google Patents
Treating beer to prevent chill haze while preventing metal contaminationInfo
- Publication number
- CA1206432A CA1206432A CA000446765A CA446765A CA1206432A CA 1206432 A CA1206432 A CA 1206432A CA 000446765 A CA000446765 A CA 000446765A CA 446765 A CA446765 A CA 446765A CA 1206432 A CA1206432 A CA 1206432A
- Authority
- CA
- Canada
- Prior art keywords
- pbw
- beer
- magnesium silicate
- chill
- hydrogel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 235000013405 beer Nutrition 0.000 title claims abstract description 39
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 24
- 239000002184 metal Substances 0.000 title claims abstract description 24
- 238000011109 contamination Methods 0.000 title claims abstract description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000000391 magnesium silicate Substances 0.000 claims abstract description 41
- 235000019792 magnesium silicate Nutrition 0.000 claims abstract description 38
- 229910052919 magnesium silicate Inorganic materials 0.000 claims abstract description 38
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 28
- 239000000017 hydrogel Substances 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 19
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 18
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 claims abstract 18
- 239000000741 silica gel Substances 0.000 claims description 13
- 229910002027 silica gel Inorganic materials 0.000 claims description 13
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 6
- 239000011148 porous material Substances 0.000 claims description 6
- 239000000499 gel Substances 0.000 claims description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 54
- 229910052742 iron Inorganic materials 0.000 abstract description 27
- 150000002739 metals Chemical class 0.000 abstract description 15
- 235000013361 beverage Nutrition 0.000 abstract description 5
- 239000010949 copper Substances 0.000 abstract description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract description 4
- 229910052802 copper Inorganic materials 0.000 abstract description 4
- ZADYMNAVLSWLEQ-UHFFFAOYSA-N magnesium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[Mg+2].[Si+4] ZADYMNAVLSWLEQ-UHFFFAOYSA-N 0.000 description 26
- 229960002366 magnesium silicate Drugs 0.000 description 20
- 239000000463 material Substances 0.000 description 10
- 239000011777 magnesium Substances 0.000 description 6
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 5
- 229920001429 chelating resin Polymers 0.000 description 5
- 229910052749 magnesium Inorganic materials 0.000 description 5
- 235000001055 magnesium Nutrition 0.000 description 5
- 229940091250 magnesium supplement Drugs 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 239000003463 adsorbent Substances 0.000 description 4
- 238000005342 ion exchange Methods 0.000 description 4
- 239000000395 magnesium oxide Substances 0.000 description 4
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 239000008367 deionised water Substances 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 235000012243 magnesium silicates Nutrition 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 150000004760 silicates Chemical class 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 229910021536 Zeolite Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 229910052681 coesite Inorganic materials 0.000 description 2
- 229910052906 cristobalite Inorganic materials 0.000 description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 2
- 239000003456 ion exchange resin Substances 0.000 description 2
- 229920003303 ion-exchange polymer Polymers 0.000 description 2
- 159000000003 magnesium salts Chemical class 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 229910052682 stishovite Inorganic materials 0.000 description 2
- 229910052905 tridymite Inorganic materials 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000010457 zeolite Substances 0.000 description 2
- DPEYHNFHDIXMNV-UHFFFAOYSA-N (9-amino-3-bicyclo[3.3.1]nonanyl)-(4-benzyl-5-methyl-1,4-diazepan-1-yl)methanone dihydrochloride Chemical compound Cl.Cl.CC1CCN(CCN1Cc1ccccc1)C(=O)C1CC2CCCC(C1)C2N DPEYHNFHDIXMNV-UHFFFAOYSA-N 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 description 1
- 241000212342 Sium Species 0.000 description 1
- ULGYAEQHFNJYML-UHFFFAOYSA-N [AlH3].[Ca] Chemical compound [AlH3].[Ca] ULGYAEQHFNJYML-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 235000015107 ale Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000019985 fermented beverage Nutrition 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- -1 iron Chemical class 0.000 description 1
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 1
- 229910001425 magnesium ion Inorganic materials 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 235000021577 malt beverage Nutrition 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 235000020004 porter Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000015106 stout Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
- C12H1/04—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
- C12H1/0408—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of inorganic added material
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Genetics & Genomics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Food Science & Technology (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Silicon Compounds (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/492,314 US4508742A (en) | 1983-05-06 | 1983-05-06 | Treating beer to prevent chill haze and metal contamination |
| US492,314 | 1983-05-06 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1206432A true CA1206432A (en) | 1986-06-24 |
Family
ID=23955790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000446765A Expired CA1206432A (en) | 1983-05-06 | 1984-02-03 | Treating beer to prevent chill haze while preventing metal contamination |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4508742A (https=) |
| EP (1) | EP0124685B1 (https=) |
| JP (1) | JPS6016584A (https=) |
| KR (1) | KR910008623B1 (https=) |
| AU (1) | AU562324B2 (https=) |
| BR (1) | BR8401044A (https=) |
| CA (1) | CA1206432A (https=) |
| DE (2) | DE3485645D1 (https=) |
| MX (2) | MX161308A (https=) |
| PH (1) | PH20945A (https=) |
| ZA (1) | ZA84997B (https=) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4636394A (en) * | 1984-04-16 | 1987-01-13 | J. E. Siebel Sons' Company, Inc. | Method and compositions for chillproofing beverages |
| US4766000A (en) * | 1985-07-16 | 1988-08-23 | Pq Corporation | Prevention of chill haze in beer |
| US4681768A (en) * | 1985-08-14 | 1987-07-21 | Reagent Chemical & Research Company | Treatment of cooking oils and fats |
| US4684530A (en) * | 1985-10-04 | 1987-08-04 | W. R. Grace & Co. | Adsorption of proteins from fluids |
| US4758440A (en) * | 1986-02-03 | 1988-07-19 | Heem Peter V D | Process for chillproofing a malt beverage and silica product for chillproofing |
| JPS62207712A (ja) * | 1986-03-05 | 1987-09-12 | Fuji Debuison Kagaku Kk | ビ−ルの安定化処理用含水シリカゲル |
| US4746439A (en) * | 1987-05-15 | 1988-05-24 | Manville Corporation | Process for removal of heavy metal contamination in waste water |
| US4797294A (en) * | 1987-06-29 | 1989-01-10 | Pq Corporation | Chillproofing with magnesium silicate/silica gel agents |
| US5232724A (en) * | 1988-12-22 | 1993-08-03 | Unilever Patent Holdings B.V. | Method for stabilizing alcoholic beverages using an aqueous suspension containing amorphous silica |
| CA2006146A1 (en) * | 1988-12-22 | 1990-06-22 | Derek Aldcroft | Stable suspensions |
| ATE145667T1 (de) * | 1989-10-12 | 1996-12-15 | Pq Corp | Verbesserte bierbehandlung und -zusammenstellung |
| US5149553A (en) * | 1989-10-12 | 1992-09-22 | Pq Corporation | Beer processing and composition |
| US5006356A (en) * | 1990-04-19 | 1991-04-09 | The Dallas Group Of America, Inc. | Treatment of fruit-based or vegetable-based beverages with precipitated magnesium silicate |
| US5009906A (en) * | 1990-06-19 | 1991-04-23 | Manville Corporation | Method and composition for filtering beer, ale or malt liquor to reduce multivalent metal cations |
| US5550264A (en) * | 1994-07-13 | 1996-08-27 | Henkel Corporation | Process for the removal of dissolved metallic catalyst from ester products |
| US5856429A (en) * | 1996-06-28 | 1999-01-05 | W. R. Grace & Co.-Conn. | Polyamide compositions for removal of polyphenols from liquids |
| US5628910A (en) * | 1996-06-28 | 1997-05-13 | W. R. Grace & Co.-Conn. | Polyamide compositions for removal of polyphenols from liquids |
| US6555151B2 (en) * | 2001-01-12 | 2003-04-29 | Pq Corporation | Process for making and using a low beverage soluble iron content adsorbent and composition made thereby |
| US20090261041A1 (en) | 2006-07-14 | 2009-10-22 | World Minerals Inc. | Composition for Filtering and Removing Particles and/or Constituents from a Fluid |
| WO2008024952A2 (en) * | 2006-08-25 | 2008-02-28 | World Minerals, Inc. | Processes for reducing beer soluble iron in diatomaceous earth products, diatomaceous earth products and compositions thereof, and methods of use |
| US20090114569A1 (en) * | 2007-11-02 | 2009-05-07 | General Electric Company | Methods for removing metallic and non-metallic impurities from hydrocarbon oils |
| CA2934794C (en) * | 2013-12-25 | 2020-02-18 | Kenji Hosoi | Device and method for removing unwanted component included in beverage |
| IT201800004721A1 (it) * | 2018-04-19 | 2019-10-19 | Dispositivo per la stabilizzazione del vino ed altre bevande vegetali e relativo procedimento di stabilizzazione. | |
| CN116116318A (zh) * | 2023-01-15 | 2023-05-16 | 国投盛世承德科技股份有限公司 | 一种沸石醇化醒酒珠的制备方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB586996A (en) * | 1943-09-27 | 1947-04-10 | Richard Gibson Shaler | Method of clarifying and stabilizing beer and like beverages |
| BE647680A (https=) * | 1963-05-10 | |||
| DE1442334B2 (de) * | 1963-08-02 | 1980-04-24 | Wilz-Pauls Geb. Pauls, Rosemarie, Basel (Schweiz) | Verfahren zur Behandlung von Bier |
| GB1215928A (en) * | 1967-04-28 | 1970-12-16 | Unilever Ltd | A process for reducing haze in beer |
| DE2020294C3 (de) * | 1970-04-25 | 1974-12-05 | Gebr. Herrmann, 5000 Koeln | Verfahren zur Herstellung eines hochkieselsäurehaltigen Materials zur Adsorption von Eiweiß-Stoffen aus flüssiger Phase |
| DE2257336C2 (de) * | 1972-11-22 | 1982-09-23 | Wilz-Pauls, geb. Pauls, Rosemarie, Basel | Verfahren zur Herstellung eines Kieselsäuregel-Adsorptionsmittels zur Stabilisierung und Klärung von Getränken |
| US3940498A (en) * | 1974-09-03 | 1976-02-24 | Johns-Manville Corporation | Chill-proofing with synthetic magnesium silicates |
| US4202910A (en) * | 1977-02-07 | 1980-05-13 | Johns-Manville Corporation | Filtration of vegetable based matter |
-
1983
- 1983-05-06 US US06/492,314 patent/US4508742A/en not_active Expired - Lifetime
-
1984
- 1984-02-03 CA CA000446765A patent/CA1206432A/en not_active Expired
- 1984-02-06 DE DE8484101186T patent/DE3485645D1/de not_active Expired - Lifetime
- 1984-02-06 EP EP84101186A patent/EP0124685B1/en not_active Expired - Lifetime
- 1984-02-06 DE DE198484101186T patent/DE124685T1/de active Pending
- 1984-02-10 ZA ZA84997A patent/ZA84997B/xx unknown
- 1984-02-17 PH PH30262A patent/PH20945A/en unknown
- 1984-03-08 BR BR8401044A patent/BR8401044A/pt unknown
- 1984-03-09 AU AU25496/84A patent/AU562324B2/en not_active Ceased
- 1984-03-19 JP JP59051245A patent/JPS6016584A/ja active Granted
- 1984-03-26 KR KR1019840001591A patent/KR910008623B1/ko not_active Expired
- 1984-05-04 MX MX201240A patent/MX161308A/es unknown
-
1988
- 1988-10-07 MX MX1334488A patent/MX165212B/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ZA84997B (en) | 1984-09-26 |
| AU562324B2 (en) | 1987-06-04 |
| JPS6016584A (ja) | 1985-01-28 |
| DE124685T1 (de) | 1985-05-09 |
| KR910008623B1 (ko) | 1991-10-19 |
| MX161308A (es) | 1990-09-06 |
| KR840008813A (ko) | 1984-12-19 |
| DE3485645D1 (de) | 1992-05-21 |
| MX165212B (es) | 1992-10-30 |
| EP0124685A3 (en) | 1986-06-04 |
| EP0124685A2 (en) | 1984-11-14 |
| AU2549684A (en) | 1984-11-08 |
| JPH0523739B2 (https=) | 1993-04-05 |
| EP0124685B1 (en) | 1992-04-15 |
| BR8401044A (pt) | 1985-02-26 |
| PH20945A (en) | 1987-06-10 |
| US4508742A (en) | 1985-04-02 |
Similar Documents
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| CA1206432A (en) | Treating beer to prevent chill haze while preventing metal contamination | |
| US4684530A (en) | Adsorption of proteins from fluids | |
| US8263153B2 (en) | Method of preventing or reducing haze in a beverage using silane-treated silica filter media | |
| US4965084A (en) | Method of reducing the iron content in beverages utilizing a particulate filteraid with a polydentate ligand | |
| CA2040069C (en) | Treatment of fruit-based or vegetable-based beverages with precipitated magnesium silicate | |
| US4797294A (en) | Chillproofing with magnesium silicate/silica gel agents | |
| AU612632B2 (en) | Amorphous silicas | |
| EP0683222B1 (en) | Stabilizing agent for beer | |
| US4766000A (en) | Prevention of chill haze in beer | |
| US6555151B2 (en) | Process for making and using a low beverage soluble iron content adsorbent and composition made thereby | |
| US4631193A (en) | Treating beer to prevent chill haze | |
| US4563441A (en) | Composition for treating beer to prevent chill haze and metal contamination | |
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| KR0169299B1 (ko) | 개량된 맥주 제법 및 조성물 | |
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| US20240150686A1 (en) | Product and method for stabilization/chill proofing of fermented liquids | |
| RU2132305C1 (ru) | Способ умягчения и очистки питьевой воды | |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |