CA1205760A - Tubular object of thermoplastic material - Google Patents

Abstract

ABSTRACT OF THE DISCLOSURE

An object is produced from a tubular blank of thermo-plastic material of the type polyester or polyamide, preferably of polyethylene terephthalate by reducing the thickness of amorphous material in one or several areas of the blank by means of one single or several consecutive re-shaping operations. A mechanical shaping device moves a transitional zone situated between thicker and thinner material along the blank and elongates simul-taneously the blank in the moving direction of the tran-sitional zone. After the last re-shaping operation the thinner material has preferably an oriented state. During the re-shaping operation the temperature of the material in the transitional zone is controlled at a level which, immediately before the re-shaping operation, is within or close to the range of the glass transition temperature.
In one embodiment the reduction of the wall thickness of the material is begun in a track in the wall of the blank and continues symmetrically around the track.
Clamping devices are used to maintain the axial position of the blank. The blank is suitable for re-shaping for instance into a container in which the mouth too consists of oriented material. The invention offers possibilities for materials savings by comparison with previously used methods, at the same time as the thermal and mechanical characteristics of the container are improved.

Description

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~ he present invention relates to a tubular object of polyethylene terephthalate or a similar thermoplastic material made from a tubular blank of amorphous material. The object has one or more cylindrical areas of material in which the thickness of the material in the blank has, in the case of polyethylene terephthalate, been reduced by one or more shaping operations until it is approximately 1/3 of the original thickness of the material. In certain applications the thickness of the materiai is reduced along the entire length of the object.
In the areas with reduced wall thickness the material is axially oriented and has, in the case of polyethylene terephthalate, a crystallinity of less than approximately 30%, usually being of the order of 10 - 25 %. The initial temperature ~ the material during shaping is preferably below the glass transition temperature ~TG) and the shaping operation takes :: .

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place with the temperature of the material controlled in the area of shaping, where the material is in surface contact with an external draw xing and/or an internal shaping device.

Previously disclosed in Canadian patent application 352,909 filed May 28, 198G by K. M. Jakohsen et al, is an object in which the wall thickness preferably at a central point of said object has been reduced to approxima-tely 1/3 of the original thickness of the material. The reduction in thickness is produced by clamping each end of a tubular blank in which the material is at an initial temperature below the glass transition temperature (TG) in two ]aws which are then moved apart. By causing an annular area of the material to have a higher temperature than the surrounding material, the obtained material properties of the area will cause the reduction in thickness to commence in the area during the stretching operation. In certain applications the internal diameter of the blank is stabilized by the use of an internal mandrel. The process as disclosed will produce an object in which the material is axially oriented and has a crystallinity of less than approximately 3~/O, usually being of the order of 10-25%.

Already disclosed in Swedish Patent Application SE 7905045-6, laid open for public inspection on December 11, 1980 naming K. M. Jakobsen as inventor, is a method for causing the thickness of the material in a tubular blank to be reduced mechanically by the use of an external device. The device consists of one or more rollers which make contact with the external and/or internal surface of the blank with such force that the desired reduction in thickness will occur as the initial temperature of the material approaches the glass transition ternperature. The external device is moved around the periphery of the blank and along the axis of the blank simultaneouslyO This method will also produce an object in which the crystallinity in the areas of reduced material thickness will be less than approximately 30% and will be of the order~ lQ-25%;,~

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~owever, the material will not have been oriented axially to such a high degree as when the process described in the previous paragraph is used.
In accordance with the inventions described above, certain applications will produce oblects which differ in respect of the transitional zone between stretched and non-stretched material. This condition will arise, for instance, if a central section of a tubular blank is stretched whilst the material in the blank is at an initial temperature below the glass transition tempera-ture (TG) and if the blank i5 then separated into two parts so as to form two separate objects. The differ-ence is due to the fact that one of the objects con-tains the start zone for the yielding of material produced by the stretching operation, whilst the other object contains the stop zone for -the yielding of material.
When practising the invention in accordance with Canadian Patent application 352,909 an annular transi-tional zone between the thinner material which has beenstretched and the thicker material which has not been stretche~l will normally be produced. In the zone the surface of the material will form an angle of approxi-mately 45 with the surfaces of the stretched and non-stretched material respectively. Axially displaced tapering areas will occasionally be produced in the essentially annular transitional zone durin~ the drawin~
operation, the presence of said areas usually requiring the object to be scrapped~
A tubular object of thermoplastic material in accordance with the present invention formed from a tubular blank consists of material with a crystallinity of less than 10%, the object having a cylindrical part which consists of material which is oriented along the axis of the object only and has a maximum crystallinity ,~

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- 3a -of approximately 30%. The material of the cylindrical part is obtai.ned by reducing the thickness of the blank while substantially ma:intaining its diameter.
More specifically, the present invention relates to tubular objects with areas of the wal.l, which, in the case of polyethylene terephthalate, the original thickness has been reduced to approximately 1/3 of its initial value, in which areas the material is oriented mainly along the axis of the object only, .
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in which areas crystallinity is less than approximately 30 ~ and is preferably within the range of 10-25 %,. and in which areas the crystallinity produced in the material by the aforementioned orientatio:n will achieve a maximum value of 17 %. The material in these areas will also have been oriented mainly along the axis of the object.

The speed at which the thickness of the material is reduced is greater in accordance with the present f invention-than by previously disclosed methods.
Furthermore, the transitional zone between material with the original wall thickness and material with reduced wall thickness will always have a predetermined shape, at the same time as the length of the sections .
with reduced wall thickness will always be precisely : 15 defined due to the fact that the re-shaping of the blank in the transitional zone itself is mechanically controlled~ For example, when star~ing from a tubular blank in order to make an object to be used for two prefo.rms which face each other, the rate of production

2~ will additionally be doubled by starting the drawing operation at a central point and by then continuing it simultaneously towards-the two ends of the tube. The object which has thus been produced may be cut and the cut sections sealed to form two preforms for future processing, in which the transitional zone between material with the original wall thickness and material ! with reduced wall thickness will always have a pre~
` determined shape and will always contain material with characteristics which are idential from one preform to another.

In accordance wlth the present in~ention it is also po.ssible to produce an object in which the thickness of : the material is reduced along the entire length of the object or in one or more cylindrical sections of the ~:: 35 object. The object is in thé form of a tube which is .

open at both ends or, in certain applications, in the for~ of a tube which has been sealed at one end. The object is mainly intended to be moulded into containers, whereby each single object is formed into either a single container or a number of containers. In the latter case, the object is divided into a number of parts which are then moulded intc> containers.

The production of an object of polyethylene tereph-f thalate in accordance with the present invention starts with a tubular blank or a similar thermoplastic material.
The material in this blank will be in an amorphous state.
In one single operation or a number of consecutive operations the thickness of the material in the blank is reduced to approximately 1/3 of its original thick-ness. This reduction in thickness takes place either along the entire length of the blank or in one or more sec-tions of the blank. Use is made of a draw ring in certain applications, in which the relationship between the internal circumference of the draw ring and the external circumference of the blank is such that the thic~ness of the material will be reduced as the draw ring is moved a~ially along the blank. The temperature of the material immediately before the reduction in thickness takes place must be in the range o~ or lower than the glass-transition temperature (TG) of the material, which temperature will be abbreviated to TG
in the following/ and should deviate ~rom TG preferably by no more than 15 C. Although the technical effect of the present invention may be achieved at a much lower temperature, it is advantageous to use an initial temperature close to TG, for instance a temperature which is between 1 to 3 C below TG, since material at this initial temperature will permit the draw ring to be moved at high speed. In certain typical applications, the draw ring operates in conjunction with an internal shaping device located inside the .

blank, whereby the external dimension of -the shaping device fits the internal surface o~' the blank. In other applications only the internal 5haping device 19 used~ The thickness of the material in the blank i5 reduced by contact with the draw ring and/or the internal shaping device as said draw ring and/or shaping device is moved axially along the blank. During the re-shaping operation a transitional zone is formed between f material with the original thickness a~d material with reduced thickness, said transitional ~one gradually moving axially along the blank~ ~he ma-terial in the.
transitional zone is kept at a temperature close to ~G during the re-shaping operation by the transfer o~
heat to the draw ring and/or the shaping device located inside the tubular blank~ In certain applications the material in the transitional zone is, however, allo~Yed to assume a temperature ~hich exceeds ~G by no more than 30 C 9 and pre~erably by no more than 15~.
In certain applications -the material in the area adjacen~ to the transitional zone is cooled to a tempera~ure below TG immediately after it has been reduced in thickness.

:In accordance with the present invention the possibilit~
is offexed of producing an object with areas with mainly a monoaxial orientation and in which the material has been xeduced in thickness and of which the external : circumference has been reduced and/or the internal circumference has been increased compared to the circum-ference of the corresponding sections of material in the blank.

In the case of sections with reduced wall thickncss requiriny to be produced in areas situated between the ends of -the blank, the reduction in thickness is begun by forming one or more peripheral grooves in 76~

-- 7a -the wall of the blanX at the same time as external devices are used to subject the blank to tensile stress alon~
its axis. This stretching operation reduces the wall thickness in the grooves to about 1/3 of its original thickness at the same time as the blank is elongated axially. Further reduction of the thickness of the wall of the blank is produced by positioning the draw ring in the aforemelltioned groove or grooves and moving it axially along the blank. Certain applications use two rings, whereby the reduction in wall thickness takes place simultaneoùsly from a specific groove outwards towards the two ends of the blank.
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In the case of a blank which is sealed at one end and in which the wall thickness is to be reduced adjacent to the seal, the draw ring should preferably be moved from the seal towards the other end of the blank. In certain appli-cations the reduction in thickness is allowed to continue along the entire length of the blank.

In those applications in which the blank is in the form of a tube open at both ends, this may be sealed in certain cases after the reduction in thickness by heating the material at one end of the object and then by press moulding the material in a mould which may be cup-shaped, for instance.
Patent Specification DE PS 1 704 119 published January 17, 1974 in the name of Otto Rosenkranz et al contains examples of methods suitable for achieving sealing of this kind.
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7 b The reduction of the thickness of the material in several stages is used mainly in the event of the material being so thick that problems arise in transferring sufficient heat away from the transitional zone. By reducing the thickness of the material a number of times before the final reduction in:thickness is made, a thinner material will be produced which w-ill facilitate the transfer of heat away from the transitional zone to the adjacent draw ring and/or internal shaping device.

Two draw rings are included in one device for producing an object in accordance with the invention.
A mandrel around which a tubular blank is placed during the drawing operation is positioned axially to and inside the two draw rings. Separate clamping devices are also positioned near the end sections of the blank.
Each draw ring consists of -two draw ring halves which ~ . .
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are moved by the driving device between an operating pos,ition in which the hal~es of the draw ring are in contact with each other and an open position in which the halves of the draw ring are separated from each other. ~he open position is used when inserting the tubular blank or removing the made object from the device.

~ Driving devices are also positioned in such a way as to move the draw rings and clamping devices axiall~ along the blank,, At least whilst the draw rings are moving to~wards the ends of the tubular blank~, the movement of the draw rings is connected to the moveme~t of the clamping devices in such a way that the draw ring and clamping device which are adjacent to each other are moved in the same direction and in such a way that the correlation between the speed of the respecti~e draw ring and clamping device is determined by the reduction in -thickness which it is wished to produce in the material in the tubular b-lank~ ~or example, when reducing the wall thickness of the blank to 1/3 o~ its original-thickness,, the ratio between the speeds o~ the clamping device and the draw ring shall be 2/3 , with a ratio of 1/2 when reducing the thickness of the ma-terial to 1/2 of its original thickness, etcO
The clamping de~ices are fi-tted with axially movable sprung components against which the edges o~ the tubul,~r blank make contact~, Any longtitudinal tolerances which are present in the blank both before ,~nd during the drawing operation are absorbed by the sprung components.

In one embodiment of the invention each draw ring usually consists of three ring sections with a certain degree of thermal insulation between the sections.
Each~ring section is provided with channels for a fluid, .... . .

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said fluid either heating or c,ooling the ring section.
The aforementioned mandrel is also provided with liquid channels. The central riny section incl.udes that part of the draw ring against which the transitional zone be-tween material with its original thickness and material with reduced wall thickness is formed during the drawing of the tubular blank. Of the neighbouring ring sections, the one with the :Largest internal diameter is in contact with the material with its original thick-ness during the drawing operation, whilst the other ring section with the smallest internal diameter is in contact with the material with reduced-thickness.
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When dra~ing a tubular blank~ said blank is positioned on the mandrel in such a way that it is held securely by the clamping devicesO A central peripheral gro~ve in the base of which the wall thickness has been reduced to approximately 1/3 of its original thicknes~
is formed in the tubular blank in the manner described aboveO ~he draw ring halves are then moved to their operating position. ~he shape and the axial length cf those parts o~ the draw rings whic~ are introduced into the groove match the shape and the axial length of the grooveO The material ~f the blanX
in the area which is to be drawn should preferably be heated to a temperature close to but below ~G before the blank is positioned on the mandreln ~he material will be raised to the correct drawing temperature through the contact surfaces formed between the material of the blank and the draw rings and mandrel.

During the actual drawing operation the draw rings and the clamping devices are moved away from the track by the driving devices, when the aforementioned relative speed between the draw rings and the clamping devices is maintained. Thus the thickness of the material in the . blank will continue to be reduced by the draw rings for .

as long a~ movement continues At the sa~e time the blank is lengthened along its axis.

An essential factor relating to the device is the control of the tempera-ture of the material in the transitional zone between amorphous material with the original wall thickness and ~aterial which has been reduced in thicXness. The draw ring has an internal profile which matches -the change in the thickness of ( the material which occurs in the transitional zoneO
The profile has been selected in such a way that it will form contact surfaces with the internal surface of the draw ring not only in the transitional zone, but also ahead of and after it during the drawing operation.
The draw ring is able in this way to control the shape of the transitional surface in the transitional zone.
The temperature of the material in the blank is regulated during the entire drawing operation by the transfer of heat between the material in the blank and the draw rings and/or the mandrel It is particularly important that the section of the draw ring which is in contact with the ~ateriaI in the transitional ~one should maintain the material in the blank at a temperature close to ~G ~
A simplified embodiment of the present in~ention makes use of ~ single draw rin~ which is moved ~rom a start track preferably all the way to the edge at one of the - ends of the blank. In this way an obiect is produced in which the wall thickness is reduced at one end only.
This embodiment preferably makes use of an internal 3C mandre~ as a dolly which will take up the axial forces which arise as the wall thickness is reduced. The movement of the draw ring is interrupted in certain applications before it passes over the edge of the tubular blan~. ~he edge will thus be bordered by a rim in which the wall thickness has not been reduced after the drawing operation is complete. The object which is produced in this way is suitable for use as a prerorm, possibly after a certain amount of re-shaping of the rim, i.e. what will become the edge of the mouth, for a container intended to be closed by means of a "crown cork", for instance. sefore the object is moulded into a container, the area which will become the mouth is stabilized by heating and by thermal crystallization, with crystalli~ation usually being allowed to continue until the material in the afore-mentioned rim becomes opaque.

- In a preferred embodiment of the present invention the - blank is provided with a start track of such axial length that space is provided in the track for a clamping device together with the draw rin~ or draw rings. At least during the initial stage of the movement of the draw ring or draw rings, the clamping device holds sections of the wall of the material in the base of the track pressed against the mandrel. In this way the position of the blank relative to the mandrel is fixed. In the embodiment of the present invention in which two draw rings are moved away from each other, the clamping device is designed to hold the wall of the blank in an area situated between the draw rings. By holding the blank securely against the mandrel, this will prevent any axial movement of the blank in relation to the mandrel which might arise depending on the axial forces - which occur at the contact surfaces between the respective draw ring and the material in the transitional zone between the wall of the blank with reduced thickness and the wall of the blank with non-reduced thickness. Any movement could, for instance, lead to the disadvantage that in the variant of the inven~ion in which an area surrounding the track has the thickness of its wall reduced, the area with reduced wall thickness may be positioned unsymmetrically in relation to the start trac~.
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The use of a clampiny device i~ accordance with the previous paragraph offers the possibility of producing any desired axial length in the area in which the wall thickness of the material has been reduced. In certain applica-tions this involves producing such a reduction in the thickness of the wall of the material along the entire lenyth of the blank, whereas in other applications the reduction in thickness is interrupted before the draw ring or draw rings reach and pass beyond the end ~~ 10 or ends of the blank. By leaving an area of amorphous material at the very end or ends of the blank~ a section of material will be produced which is highly suitable, for example, for sealing to produce the base of a pre-form by the use of a method which is described in Patent Specification DE PS 1 704 119 or, after having been subjected to thermal crystallization, for fcrming a rim for use with the "crown cork" type of closure.

In an alternative embodiment the draw ring is used to reduce the wall thickness of the material in a tubular blank with a sealed bottom, the mouth of which is already provided with a means-of closure, for example screw threads. The blank in which the material is intended to be subjected to a reduction in thickness is produced by so~e previously disclosed method, for example by injection moulding or by e~trusion followed by ~sealing and moulding the bottom and mouth. In certain applications the start track is formed in the manner described above, whilst in other applications a starting point or the start track in whole or partly is produced during the injection moulding of the preform.

When using an external draw ring to reduce the thickness of the material in the wall of the blank, a certain reduction in the internal diameter of the blank will also be produced, as has already been mentioned~ The mandrel inside the blank thus acts as a shaping device which will determine the extent of the reduction in diameter.
Surprisinyly, it has been found that, for material with-in the r~nge of temperatures indicated above during the re-shaping operation, the c~ntact between the wall of the materi~l and the mandrel and produced by the contraction, generates relatively little contact pressure between the internal surface of the wall of - the blank and the e~ternal surface of the manArel, for which reason no problems are encountered in removing ~ 10 the finished blank from the mandrel af-ter the shaping - (drawing) of the blank is complete.

No internal mandrel is called for in certain types of applicatio~ for the device, in which the object is allowed to assume an internal circumference which is smaller than its original circumference. By selecting an internal mandrèl with an external circum~erence which is smaller than the internal circumference of the blank, it is possible in other typical applications to control the xeduction in t~e internal circumference of the blank during the drawing operation to a value which is suitable for the envisaged specific application.
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~he pr~sent invention is described in greater detail with reference to a number of ~igures3 in which .~
~ig. 1 shows a perspective view of a drawing device;
~ig. 2 shows a long~ltudinal section through the drawing device in accordance with ~ig~ 1 in which the draw rings of the drawing device are in the initial position before drawing;
~ig. 3 -shows part of a long~itudinal section - corresponding to ~ig. 2, in which the draw ` rings have been separa-ted from each other, - ~ig, 4 shows a support plate fitted with a draw ring ~ in its operating position;

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Fig. 5 shows a longitudinal section through a tubular blank with a draw ring in its initial position;
Fig. 6 shows a longitudinal seetion through a tubular blank during drawing in the direction away from its sealed part;
Fig. 7 shows a section through a tubular blank with a draw ring in the initial position prior to drawing the blank in a short section at one end;
Fig. 8 shows a section of the -tubular blank in accordance with Fig. 7 with the draw ring in its final position;
Fig. 9 shows a longitudinal section through a drawing deviee with a central clamping device and with the draw rings or the clarnping device in the initial position before drawing;
Fig. 10 shows part of a longitudinal seetion eorre-sponding to Fig. 9 with the draw rings moved - apart;
Fig. 11 shows the eentral area in accordanee with Fig. 9 in detail;
Fig. 12 shows the central area in aceordance with - Fig. 10 in detail;

Flg- 13 show objects of alternative embodiments.
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: : -; Fig~ 1, which shows an overall perspective view of a drawing deviee in aecordance with the present invention, portrays a base 30 from which a nurnber of guide pins 31 project vertieally, as shown in the Figure. The rest ~2~

. of the description which follows will relate t~ the device in this position, although the idea of invention is in no way restricted to a special p~sition of this kind.- The designations "upper" or "l~wer" ~r other similar designations are occasionally used below in connection with a variety of components, said designations being used only for the purpose of clarification.

. ~he base is fitted with driving devices with gearing (not shown in the ~igure) for a number of drive screw~
32 which lie parallel with the guide pins~ ~our support plates 50,60~70,80 are positioned at right angles to the guide pîns and the drive screws. ~ach support plate is fitted with bearings which fit the guide pins 31 and threaded holes 52,62772,82 which operate in conjunction wi-th a mImber of the drive screws 32 ~ The plates are also provided with openings 58~68j78,88 for those drive screws which are not in threaded contact with the actual support plate. The : 20 top and bottom support plates: 50 and 60 are arranged to operate in conjunction with the two drive screws 32 a and c , whereas the two-interjacent support plates 70 and 80 are arranged to operate in conjunction with the two remaining drive screws 32 b and d . Purthermore~ the upper parts of the drive screws which operate in conjunction with the support plates 50 and 70 are threaded in opposite directions to the lower parts o~ the drive screws which operate 1n conjunction with the support plates 60 and 80 . This means that as the drive screws are rotated the two upper support plates will move in the same direction, although this will be opposite to the direction in which the two lower support plates will move.

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Sin~e -the top and bo-ttom support plates are driven by the screws 32 a and c a~d ~he two middle support plates are driven by the screws 32 b and d , the spe~d at which the respective support plates move will be determined by the ro~ational speed and the pitch of the screws in conjunction with which the respective support plates operate. The pitch of the thread on the drive screws is selected in such a way that the top and bottom support plates will always move at a lower speed than the two in the middle. In the initial position, the two middle plates will be in close contac-t with each other and the top and bot-~om plates will be in positions which will allow movement to take place towa-rds the ends of the guide pinsb After movement has taken place 7 the middle support plates will have moved closer to the upper and lower support plate respectively.
~he top support plate 50 and the bottom support plate 60 are provided with clamping devices 51 and 61 , each of which holds one end o~ a tubular blank 10 .
The blànk is provided wi-th a preferably central peripheral starting track ~2 ~Fig . 2) in which the thick-ness of the material is approximately lJ3 of its original thickness. The starting track is formed preferably before the blank is positioned in the device by the application - 25 of external pressure to the wall of the material9 for instance by means of a number of interacting rollers, at the same time as the tubular blank is subjected t~
tensile stresses along its axis. When forming the start track, the use of rollers in conjunction with the stretching operation produces a track with a pre-determined axial length which is thus given a profile which is largely identical with the profile in those parts of the draw rings which are introduced into the track (see description of Fig. 2 below) when re-shaping the blank into the object. The tubular blank is caused to lengthen axially when the start track is formed.
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~hc tw~ middle support pl~tes 70 ~nd 80 are each f it ted wi th a draw ring 71 and 81, with the latter draw ring being obscured in the Fi~lre. ~he clamping device 51 of the top support plate and the draw ring~ 71,81 of the two middle support plates consist of two halves 5l a,b , 71 a,b and 81 a~b which are moved by the driving devices 5~,73,83 to and from the closed position shown in the ~igure (the clamping device 81 is obscured in the ~igure).
In ~igure 2, which shows a longtitudinal section through the drawing device in accordance with Figure 1~ the left-hand part of the ~igure portrays the device with the upper clamping device 51 and the two draw rings 71,81 -in their open position, and the right-hand part of the ~igure portrays the device with the upper clamping device 51 and -the two draw rings 71,81 in their closed position (operating position).
The ~igure also shows the blank 10 ~ At its centre is a peripheral start track 12 which is formed in accordance with the a~ove description~
In addition to the details shown in ~igure 1, ~igure 2 shows that the upper and lower clamping devices 51,61 are fitted with sprung support plates 54 and 64 against which the end edges of the tubular blank 10 make contact. ~he required spring function is provided by springs 55,65 around the guiding devices 56 and 66 for the support plates 54 and 64 , with the guiding devices screwed firmly to the support plates.
~he ~igure also shows that the two draw rings 71 and 81 consist of two draw ring halves 71 a,b and 81 a,b.
~ach draw ring is divided into three sections 74,75~76 and 84,85,86 , each of which consists in turn of two ring section halves. ~he ring sections are separated ~rom each other by a cert~in degree of th~rmal insulation.
The rlng sections are held together by means of the rin~ casings 77 a,b and 87 a,b in such a way that they will combine to fo:rm the two halves of -the draw rings. ~ach ring section is provided with channels 1~4~175,176 and 18491859186 to permit the flow of liquid.
The draw ring sections are in the form of a section 74 and 84 with an internal circumference which matches lo the circum~erence o~ the material in the blank ln the areas in which the thickness of the material has not been reduced, another section 76 and 86 with an - internal circ~ference which matches the circumference of the material in the blank in the areas in which the thickness of the material has been reduced, and a further section 75 and 85 which forms contact surfaces with the material in tha transitional zone between material in the blank which has and which has not been reduced in thickness.
~inally, Figure 2 shows a mandrel 20 which fits the internal sur~aee of the blank 10 and which is provided with liquid channels 21 , ~igure 3 shows part of a longtitudinal section which corresponds to central sections of Figure 2 in which the draw rings have moved or are in the course of moving apart along the axis of the blank~ and portrays a central section 11 of a blank in which the thickness of the material in the blank 10l has been reduced. A-t the transitional zone 13 J 14 between material with its original wall thickness and material with reduced wall thickness, contact surfaces are formed between the middle draw rings 75 9 85 and the material in the transitional zone. In this way the draw rings are able to co~trol the shape of the transitional surface between material with its original wall thickness and material with reduced wa:Ll thickness.
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~igure 4 shows the support plate 70 ~iewed from above and with the draw ring 71 in its closed position~ The ~igure also illustrates the locations o~ the bearings for the guide pins 31 and -the openings 78 and for the threaded holes 72 for the drive screws 32 . ~he other support plates which are fitted with the draw ring 81 or with the cla~ping devices 51 or 61 are similarly equipped~ As has already been mentioned 3 the . clamping device 61 is not divided, and has therefore lo nothing ~orresponding to the drivin~ device 73.
res 5 and 6 show a typical application of the present invention in which the wall thickness of a tubular blank 15,15' which is sealed at one end is : reduced, starting a-t the sealed end of the blank~ ~his requires a draw ring 23 to be dimensioned preferably in such a way that both be~ore and at the start of the drawing operation contact will be made be-tween ~the middle ring section and the upper ring section and ~he outer surface of the tubular blank~ Here too the draw ring is made up of three ring sections 24,25j26 with liquid channels 124,125~126 . ~he ring sections are dimensioned in a similar fashion to the ring sections which have already been described and are held together by a ring casing 27 . A mandrel 28 operates in conjunction with the draw ring 2~ in the re-shaping of the blankO ~he mandrel is normally provided with liquid channels, which is not clear from the Figure, however~
~igure 6 shows the manner in which re-shaping is begun and in which a section 16 of the blank with reduced wall thickness is formed in the lower section of the : bla~. Re-shaping normally continues until all the ; material in the cylindrical part of the blank has had ": ~

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its wall thickness reduced. In t:he event of the mouth already having been formed, which may be the case with an injection-moulded blank, the re-shaping of the blank is, of course, interrupted as the draw ring reaches the mouth. The transitional zone between material with its original wall thickness and material with reduced wall thickness is indicated in the Figure by the designation 113.

igures 7 and 8 show an alternative embodiment of the present invention in which a draw ring 29 is composed of only two r.ing ~ec-tions 96,97 with separate liquid ~~ channels 94~95 . In this application too there should preferably be a certain degree of thermal insulation between the ring sectionsO If necessary, the draw ring may be extended by the addition o~ a third ring section wi-th a separate liquid channel and which i~ dimensioned in the manner already described. Here too the draw ring opera-tes in conjunction with an internal mandrel 28 , which is normally provided with liquid channels but which is not clear .from the ~iguresO ~he draw ring re-shapes the mouth of a tubular blank 17 which is sealed at one end. In an a~ea which is usually quite close to the opening in the blank, there ~ill be ~
peripheral st æ t track 19 in which the thickness of the material has been reduced to approximately 1/3 of its ~ original thickness. ~he start track is produced in the manner which has already been described.

In Figure 8 the draw ring 29 has been moved relative to the blank with the help of the mandrel 28 in such a way that a section 18 of the blank with reduced wall thickness is produced adjacent to the opening in the blank 17'.

Figures 9 and 10 show a further alternative embodiment of the present invention in which a central clamping device 41 a,b is located in the area between the draw rings 71 ~ , .
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and 81. The clamping device is positioned on a central support plate 40 with a fixed position in the device.
This fixed position is obtained, for example by attaching the support plate to the guide pins 31. The central support plate is also fitted with driving devices 43 a,b for moving the two parts 41 a,b of the central clamping device to and from the operating position of the respective parts. In certain embodiments, the central clamping device is provided with liquid channels 141 a,b.
Other devices shown in Figures 9 and 10 correspond to devices shown in Figures 1-4, in which case their referenc~
numbers agree with the refexence numbers in those Figures.
An equivalent device to the clamping device 51 is not - present in this embodiment.

Figures 11 and 12 show details of the central areas in Figures 9 and 10, i.e. those areas in which the wall of the material in the blank is provided with a start track or in which the wall of the material has undergone a reduction in thickness in conjunction with the movement of the draw rings. The reference designation 112 is used to indicate an area of contact between the internal surface of the blank 10,10' and the external surface of the mandrel 20 caused by a certain amount of deformation in the wall of the blank produced by the clamping device 41 a when this is in the operating position. The reference designations 115,116 indicate areas of contact with the mandrel by the internal surface of sections of the material in the blank 10' of which the thickness - has been reduced by the drawing operation.

In accordance with the present invention the central clamping device 41 may be designed in acc~rdance with several alternative embodiments. These are characterized by the fact that the clamping device ~1 a,b in its operating position surrounds the wall of the blan~, thus forming contact surfaces with the external surface of the wall of the blank which are distributed at various points around the periphery of the blank. This distribution of the contact surfaces is produced by the clamping device for example by the surfaces of the clamping device which face the blank not being in the form of cylindrical surfaces of circular cross-section, but rather in the form of cylindrical surfaces of, for instance, elliptical or polygonal cross-section.

f~ Figures 13-15 show examples of objects 210', 210", 210'" in accordance with the invention. The object 210' in Figure 13 has at its lower part a cylindrical wall section 213 of amorphous material adjacent to a sealed bottom 211' in the bottom also being of amorphous material. Figure 14 shows an object 210" in which the external cylindrical surface has the same diameter along the entire length of the object. The sealed bottom 211"
of the object is also of amorphous material in this embodiment. Finally, Figure 15 shows an embodiment in which the edge of the mouth 212 of the object consists of material with its original thickness, whereas the remaining parts of the object are similar in design to those in Figure 14.

The blank 10 is positioned over the mandrel 20 in the embodiment of the present invention in accordance with the -typical e~ample shown in Figures 1-4. The clamping device 51 and the draw rings 71 and 81 will then be in their open position, corresponding to the position shown in the left-hand part of Figure 2. The blank which is placed around the mandrel forms the contact surfaces with the mandrel. Once the blank is in place and is in contact with the sprung support plate 64 of the lower clamping device 61 the upper clamping device 51 and the draw ring halves are then moved to their closed position.
The two draw rings 71 and 81 enter the start track 12 and in so doing form contact surfaces with the outer wall o~

~ , .

the blank where the wall thickness has not been reduced, where the wall thickness has been reduced to its minimum value~ and at the transitional zone between the two aforementioned areas.

The material of the blank will preferably be at a high temperature, although preferably below TG, when it is placed on the mandrel. The final temperature of the material is set by the transfer of heat between the ( mandrel and the blank and/or between the draw rings and the blank. The temperature is controlled by means of the liquid which flows through the liquid channels 21 in ; the mandrel and/or through the liguid channels 174,175, 176 and 184,185 r 186 in the draw rings. The thermal insulation which is present between the ring sections of the draw rings generally maintains a certain difference in temperature hetween different areas of material in the blank. The ring sections 74,84 with the largest internal diameter will, when in the position shown in the right-hand part of Figure 2, set the material to a temperature in the range of or just below TG, and preferably to a temperature which is no moxe than 15 C below TG. The ring sections 75,85 have a similar function, whereas the ring sections 76,86 preferably will maintain a temperature well below TG, and preferably at a temperature which is ~5 at least 15 C below TG, in order to cool the material ~once it has undergone the reduction in thickness.

Once the material has reached the specified temperatur~s the driving devices at the base will begin to rotate the driving screws 3~, causing the support plates 50,70 and the associated clamping device 51 and draw ring 71 to move upwards in the Figures, and the support plates 60,80 and the associated clamping device 61 and draw ring 81 to move downwards in the Figures. The thickness of the material in the blank is thus reduced by the draw rings as long as movement continues. At the same , ; ~ ' ' ""' 1 . "

time, the blank will be lellgthened axially and this elongation will be pxoportional to the reduction in the thickness of the material and to the axial movement of the draw rings. The speeds at which the support plates 50 and 60 move are therefore selected in such a way that the positions of the clamping devices 51,61 wlll match the elongation of the blank. Any irregularities which may occur will be absorbed by the sprung support plates 54 and 64.
. ~ ,.
~he middle dra~ rings 75 and 85 are in contact with the transitional zone between material with reduced ; thickness and material with its original thickness. The - profile of the middle ring section is selec-ted in such a way that the material during the re-shaping operation will form contact surfaces with -the internal surfaces of the ring section. In this way the ring section will control the shape o~ the transitional surface between material with reduced thickness and ma-terial with its original thicknessg The ring section also has a temperature regulating function in that the transfer of heat ta~es place at the aforeme~tioned contact surfaces in such a way that the material in the transitional zone is maintained at a temperature close to ~G
throughout the entire drawing operation. It is essential, particularly when drawing takes place at high speed or when the material used is very thick5 that the middle draw ring should have excellent heat conducting properties so that the material in the transitional zone will not reach too high a temperature.
Once the dr~w rings have been moved apart so that the central section 11 of the blank will be given a predetermined length7 the movement of the support plates is stopped. The driving devices 53,73,83 then move the clamping device 51 and the draw rings 71 and 81 to their open position, and the object which has . : ~

~2~

been formed in the man~er described is then removed from the mandrel, whexeupon a new tubular blank is placed on the m~ndrel and the operation is repeated.

The section 11 with reduced wall thickness in the finished object forms the central section at which the ob~ect is cut in ~rder to produce two symmet~ical parts.
~ach part is then sealed at the end with its original wall thickness, thus producing a preform which may be used, for example, to produce a blow-moulded container~
lo ~hose sectio~s of the preform which have reduced wall thickness are subsequently re-shaped to form the basis for the mouth of the future container~
In the application of the embodiment of the present invention shown in ~igures 5 and 6, the function is in principle identical with that described above. The internal mandrel 2~ acts as a dolly which takes up those forces which arise as the draw ring 23 is moved axially along the blanl~. Regulation of the temperature in the dif~erent areas of the material is also important in this typical application. The mandrel 28 is normally pro~ided with liquid channels corresponding to the li~uid channels 21 in the mandrel 20 sho~n in ~igures 2 and 3. In certain typical applications the thickness of all the material in the cylindrical seetion o~ the blank is reduced, whilst the re-shaping st~ps sooner in other typical applications.
:
The embodiment shown in ~igures 7 and 8 is applicable in those eases in which it is required to produce a number of areas of material in wnich the thickness of the material has been reduced. Each such area of material requires a start track in which the reduction in the thickness of the material may begin. ~hen producing the object the draw ring 29 is moved to an initial start track and the halves of the draw ring 35 ~ take up their operating position. ~he draw ring is "' ,;. ' , ., ' .

~%~7~

moYed from the start track over a short distance along the axis of the blank, reducing the thickness of the material un-til the ~irst section of material with reduced wall thickness has been produced. The draw ring halves are then moved apart and the draw ring is moved to the next star-t track~ when -the dra~r ring halves take up their new operating position. ~he draw ring is now moved once more along the axis of -the blank in order to produce a new area of ma~erial with 1 10 reduced wall thickness~ and so on. The operation is repeated until the desired number of ~reas with reduced material thickness have been produced.
~he blank used in conjunction with the unidirectional drawing described in connection with ~igures 5 - 8 is sho~n as being sealed at one end~ In this way the seal ~ill have operated in conjunc~ion with an internal mandrel to absorb the axial forces required during the drawing operation~ It is, of course, poæ~ible to use external clamping devices which replace the func~ion of the mandrel in-this r-espect. ~his alternative is - used when drawing tubular blanks which are open at both ends~

In the application of the present invention which utilizes the embodiment shown in Figures 9-12, the blank lo is slid over the mandrel 20 until it makes '~ contact with the lower clamping device 61. In this case the latter serves as a device for determining the axial position of the blank, thereby ensuring that the track 12 on the blank adopts a position which is suitable for the positioning of the draw rings 71,81 and for the clamping device 41. This situation corresponds to the left-hand half of Figure 9. The driving devices 43,73,83 then move the clamping device 41 and the draw rings 71,81 into contact with the external surface of the blank in and adjacent to .

the track 12. The temperature conditioning of the material in the blank then takes place in the manner which has already been described, in addition to which in certain typical applications liquid is also caused to flow through the channels 141 in the clamping device 41. This situation corresponds to what is shown in the right-hand part of E'igure '9 and in detail in Figure 11.

( In its operating position the central clamping device 41 lo surrounds the blank 10 in the bottom of the track 12.
This forms contact surfaces with the bottom of the track which are divided into a number of areas around the circumference of the blank. The contact pressure present at these surfaces in turn causes the internal surface of the blank and the surface of the mandrel to bear against each other. The bearing surfaces adopt positions which correspond to the distribution of the contact surfaces. The bearing surfaces are produced because the clamping device deforms the shape of the surface defining the internal limits of the blank. The contact pressure of the clamping device is selected in such a way that - in the event of the shape being deformed, the thickness of the material'in the bottom of the track will remain largely unchanged. A bearing surface is shown in detail in Figure 12 and is given the reference designation 112.

The driving devices in the base 30 (Figure 1) then rotate the driving screws 32 causing the draw rinys 71,81 to move apart along the axis of the blank, simultaneously re-shaping the wall of the material and elongating the blank, The friction between the blank and the mandrel at the aforementioned bearing surfaces 112 ixes the position of the blank on the mandrel and ensures that the re--shaping of the blank will take place symmetrically around the track 12. The Ariving of the support plate 60 is selected in such a way that the clamping device 61 will be 2~

away reliably from khe end of the tube so as not to have any effect on the elongation of the tube which occurs in COII j unction with the xeduction in the thickness of the wall of the blank. This operating situation corresponds to Figures 10 and 12. Figure 12 also shows that, in addition to the stretching of the material which occurs during the re-shaping of the wall of the blank, contraction of the blank also takes place, causing its internal surface to be moved into contact with the ( 10 mandrel 20. These contact surfaces are indicated in the Figure by the reference designations 115,116. The formation of these contact surfaces contributes to the ,- fixing of the position of the blank relative to the mandrel which is achieved with the help of the central clamping device 41. It has been found in the majority of typical applications that additional fixing by means of the contact surfaces 115,116 is not essential to achieving the desired symmetrical re-shaping of the blank The description in the previous paragraph indicates that the alternative embodiment of the invention in accordance with Figures 9 12 will permit any desired length of the blank to have the thickness of its material reduced. It is thus possible to reduce the thickness of the material along the entire length of the blank 7 to interrupt the Z5 reduction in thickness immediately before the ends of the blank, or else to reduce the thickness in a number of areas distributed axially along the blank and separated by sections of material in which there has been no reduction in thickness. In each area with reduced material thickness, the reduction of the thickness is begun in a new start track, 5urprisingly, it has been found that when the b]ank is re-shaped at the temperatures indicated above, relatively low contact pressure is produced between the material of the blank and the mandrel, for ~hich reason ~26~

no problems are encountered in removing the moulded object from the mandrel after the moulding operation is complete.

The embodiments of objects shown in Figures 13-15 are examples of objects produced in accordance with the above description. When producing an object in accordance with Figure 13 the thickness is reduced in one preferred embodiment in a tubular blank which is ~- open at both ends, whereby at the end of the blank which will subsequently be sealed an area of amorphous material is left which is then heated and sealed in accordance with the method described above. Figures 14 and 15 relate to embodiments in which an already sealed tubular blank of amorphous material is given lS cylindrical areas of the walls consisting of essentially monoaxially oriented material. In Figure 14 the mono-axially oriented material is present around the object over its entire length, whereas in Figure 15 the edge of the mouth 212 consists of material which has not undergone such orientation.

The idea of invention also contains the possibility of further increasing the crystallinity by heating the material, over and above the crystallinity which is produced in the material in conjunction with the mono-axial orientation. This crystallinity should not be allowed to continue to such a point that the ability of the material to undergo further re-shaping is impaired in the case of an object which is a preform which will be re-shaped in a subsequent operation to produce a finished article. The crystallinity of an object is normally allowed to reach a maximum level of approximately 30 % when the object is to undergo further re-shaping.
Crystallinity is preferably allowed to lie between 10-25 ~ r whereas the crystallinity produced by monoaxial orlentation will achieve a maximum value oE approx. 17 %.

"., ~

,.. . . .

.: ; 3 It has been assumed in the above description that the reduction in the thickness of the material until it reaches its final value takes place iII a single reduction stage. The idea of invention also contains the possibility of reducing the thickness of the material in a number of consecutive reduction stages, before finally reducing the thickness of the material to approvimately 1/3 of its original thickness in a final stage. In this case the draw ring or draw rings will consist of a number of ring sections for the consecutive gradual reduction of the thickness of the material. The embodiment described in this paragraph .~ is used mainly when the material in the blank has a ~ large wall thickness and/or when the draw rings are moved at high speed.

Tubular blanks of circular cross-section have been shown in the above description. The idea of invention may, of course, also be applied to tubular blanks o~
other cross-sections.

The abo~e description relates to the plastic material polyethylene terephthalate. The values indicated in the description for the reductions in thickness and temperature ar~ therefore also related to this material.
A large number of materials of the type polyester or polyamide are known to exist, h~wever, and to have similar characteristics, for which reason the invention as such is also applicable either in whole or in part tc these materials, provided that the reductions in thickness and the temperatures are adjusted to suit the specific requirements of the respective material.
The following are typical materials for which the presen-t invention is suitable, after the indicated adjustments have been made: polyethylene terephthalate, polyhexamethylene adipamide, polycaprolacta~m, poly-hexamethylene sebacamide, polyethylene-2,6- and 1,5-. . .

naphthalate, polytetramethylene-l,2-dioxybenzoate, and copolymers of ethylene teraphthalate, ethylene isophthalate, and other similar plastics polymers.

The crystallinity values stated in the present application relate to the theories disclosed in the publication "Die Makromolekulare Chemiel' 176, 2459-2465 (1975).

- In addition to the above specification, the invention is also described in the following Patant Claims.

This application is a division of application Serial No. 378,503 filed May 28, 1981.

, ~

Claims (12)

The embodiments of the invention in which an exclusive property or privilege is claimed are defined as follows:

1. A tubular object of thermoplastic material formed from a tubular blank consisting of material with a crystallinity of less than 10%, the object having a cylindrical part which consists of material which is oriented along the axis of the object only and has a maximum crystallinity of approximately 30%, the material of the cylindrical part being obtained by reducing the thickness of the blank while substantially maintaining its diameter.

2. An object as claimed in claim 1, wherein said maximum crystallinity is between 10 and 25%.

3. An object as claimed in claim 1, wherein said maximum crystallinity is 17%.

4. An object as claimed in claim 1, wherein the reduction of the thickness of the blank is obtained with the blank at a temperature in the vicinity of the glass transition temperature of the material.

5. An object as claimed in claim 4, wherein said temperature is no more than 30°C. greater than the glass transition temperature.

6. An object as claimed in claim 1, wherein the thickness of the cylindrical part is a multifold reduction of the thickness of the blank.

7. A tubular object of polyethylene terephtha-late formed from a blank consisting of material with a crystallinity of less than 10%, said object having a cylindrical part which consists of material which is oriented along the axis of the object only and has a maximum crystallinity of approximately 30%, the material of said cylindrical part being obtained by forming a transitional zone between a region of thinner material and a region of thicker material and displacing said transitional zone to elongate the region of thinner material and reduce the region of thicker material.

8. An object as claimed in claim 7, wherein the thickness of the cylindrical part is a multifold reduction of the thickness of the blank.

9. An object as claimed in claim 1, wherein said maximum crystallinity is between 10 and 25%.

10. An object as claimed in claim 1, wherein said maximum crystallinity is 17%.

11. An object as claimed in claim 1, wherein the reduction of the thickness of the blank is obtained with the blank at a temperature in the vicinity of the glass transition temperature of the material.

12. An object as claimed in claim 3, wherein said temperature is no more than 30°C. greater than the glass transition temperature.